Assessment of surface treatment methods for strengthening the interfacial adhesion in CARALL fiber metal laminates

Abstract Metal and polymer interface bonding significantly influences the mechanical performance of fiber metal laminates (FMLs). Therefore, the effect of surface treatments (mechanical abrasion, nitric acid etching, P2 etching, sulfuric acid anodizing (SAA), and electric discharge machine (EDM) tex...

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Main Authors: Madhusudhan Balkundhi, Satish Shenoy Baloor, Gururaj Bolar
Format: Article
Language:English
Published: Nature Portfolio 2024-12-01
Series:Scientific Reports
Subjects:
Online Access:https://doi.org/10.1038/s41598-024-81777-1
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author Madhusudhan Balkundhi
Satish Shenoy Baloor
Gururaj Bolar
author_facet Madhusudhan Balkundhi
Satish Shenoy Baloor
Gururaj Bolar
author_sort Madhusudhan Balkundhi
collection DOAJ
description Abstract Metal and polymer interface bonding significantly influences the mechanical performance of fiber metal laminates (FMLs). Therefore, the effect of surface treatments (mechanical abrasion, nitric acid etching, P2 etching, sulfuric acid anodizing (SAA), and electric discharge machine (EDM) texturing) carried on aluminum 2024-T3 alloy sheets was evaluated considering surface morphology, surface topography, and surface roughness. Further, the influence of surface treatments on interfacial adhesion strength and failure mode between the aluminum alloy and carbon fiber prepreg was investigated. The surface treatments increased the surface roughness of the aluminum substrates. Surfaces treated using SAA, nitric acid, and P2 etchant showed improved wettability, while mechanically abraded and EDM textured substrates showcased hydrophobic behavior. The selected surface treatments significantly affected interfacial adhesion between the epoxy polymer and aluminum alloy. SAA and EDM texturing greatly enhanced the interfacial peel strength of FMLs. In the case of interfacial shear strength, EDM textured substrate showed superior performance, followed by SAA. Moreover, untreated and mechanically abraded specimens exhibited weaker bonding and adhesive failure at the aluminum-epoxy interface, whilst chemical treatments resulted in mixed model failure. EDM textured surface underwent cohesive failure, while a dominant mixed mode failure and fiber adhesion were observed in the SAA-treated specimen.
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spelling doaj-art-3f511631d8ef4ce6a3097fbf8d37c2082025-08-20T02:43:32ZengNature PortfolioScientific Reports2045-23222024-12-0114111310.1038/s41598-024-81777-1Assessment of surface treatment methods for strengthening the interfacial adhesion in CARALL fiber metal laminatesMadhusudhan Balkundhi0Satish Shenoy Baloor1Gururaj Bolar2Department of Mechanical and Industrial Engineering, Manipal Institute of Technology, Manipal Academy of Higher EducationDepartment of Aeronautical and Automobile Engineering, Manipal Institute of Technology, Manipal Academy of Higher EducationDepartment of Mechanical and Industrial Engineering, Manipal Institute of Technology, Manipal Academy of Higher EducationAbstract Metal and polymer interface bonding significantly influences the mechanical performance of fiber metal laminates (FMLs). Therefore, the effect of surface treatments (mechanical abrasion, nitric acid etching, P2 etching, sulfuric acid anodizing (SAA), and electric discharge machine (EDM) texturing) carried on aluminum 2024-T3 alloy sheets was evaluated considering surface morphology, surface topography, and surface roughness. Further, the influence of surface treatments on interfacial adhesion strength and failure mode between the aluminum alloy and carbon fiber prepreg was investigated. The surface treatments increased the surface roughness of the aluminum substrates. Surfaces treated using SAA, nitric acid, and P2 etchant showed improved wettability, while mechanically abraded and EDM textured substrates showcased hydrophobic behavior. The selected surface treatments significantly affected interfacial adhesion between the epoxy polymer and aluminum alloy. SAA and EDM texturing greatly enhanced the interfacial peel strength of FMLs. In the case of interfacial shear strength, EDM textured substrate showed superior performance, followed by SAA. Moreover, untreated and mechanically abraded specimens exhibited weaker bonding and adhesive failure at the aluminum-epoxy interface, whilst chemical treatments resulted in mixed model failure. EDM textured surface underwent cohesive failure, while a dominant mixed mode failure and fiber adhesion were observed in the SAA-treated specimen.https://doi.org/10.1038/s41598-024-81777-1Fiber metal laminatesSurface treatmentInterfacial adhesionPeel strengthShear strengthSurface characterization
spellingShingle Madhusudhan Balkundhi
Satish Shenoy Baloor
Gururaj Bolar
Assessment of surface treatment methods for strengthening the interfacial adhesion in CARALL fiber metal laminates
Scientific Reports
Fiber metal laminates
Surface treatment
Interfacial adhesion
Peel strength
Shear strength
Surface characterization
title Assessment of surface treatment methods for strengthening the interfacial adhesion in CARALL fiber metal laminates
title_full Assessment of surface treatment methods for strengthening the interfacial adhesion in CARALL fiber metal laminates
title_fullStr Assessment of surface treatment methods for strengthening the interfacial adhesion in CARALL fiber metal laminates
title_full_unstemmed Assessment of surface treatment methods for strengthening the interfacial adhesion in CARALL fiber metal laminates
title_short Assessment of surface treatment methods for strengthening the interfacial adhesion in CARALL fiber metal laminates
title_sort assessment of surface treatment methods for strengthening the interfacial adhesion in carall fiber metal laminates
topic Fiber metal laminates
Surface treatment
Interfacial adhesion
Peel strength
Shear strength
Surface characterization
url https://doi.org/10.1038/s41598-024-81777-1
work_keys_str_mv AT madhusudhanbalkundhi assessmentofsurfacetreatmentmethodsforstrengtheningtheinterfacialadhesionincarallfibermetallaminates
AT satishshenoybaloor assessmentofsurfacetreatmentmethodsforstrengtheningtheinterfacialadhesionincarallfibermetallaminates
AT gururajbolar assessmentofsurfacetreatmentmethodsforstrengtheningtheinterfacialadhesionincarallfibermetallaminates