Synthesis, spectral investigation and antimicrobial assay of 2-ethoxy-6-(((3-nitrophenyl)imino)methyl)phenol and its Co(II) and Cu(II) complexes

Abstract In the present work, [Co2(EN-H)2Cl2] and [Cu2(EN-H)2Cl2] were synthesized using Schiff base, 2-ethoxy-6-(((3-nitrophenyl)imino)methyl)phenol [EN(3)], which is derived from 3-nitroaniline and 3-ethoxysalicylaldehyde. The nature of bonding and the structural features of the Schiff base and it...

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Bibliographic Details
Main Authors: V. Gomathi, Rajendran Rajaram, K. Kayathri Devi, M. Gayathri, P. Ishwarya, P. Jagatheeshwari, R. Karthika, D. Keerthana
Format: Article
Language:English
Published: Springer 2025-05-01
Series:Discover Chemistry
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Online Access:https://doi.org/10.1007/s44371-025-00185-0
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Summary:Abstract In the present work, [Co2(EN-H)2Cl2] and [Cu2(EN-H)2Cl2] were synthesized using Schiff base, 2-ethoxy-6-(((3-nitrophenyl)imino)methyl)phenol [EN(3)], which is derived from 3-nitroaniline and 3-ethoxysalicylaldehyde. The nature of bonding and the structural features of the Schiff base and its complexes have been deduced using molar conductance, Fourier Transfrom Infra-Red (FT-IR), electronic, 1H NMR, mass, and fluorescence spectra. The antimicrobial activities of Schiff base, and its Co(II) and Cu(II) complexes were investigated against Staphylococcus aureus, Escherichia coli, and Aspergillus niger by agar-well diffusion method. Both the Schiff base and complexes exhibit substantial activities. The [Cu2(EN-H)2Cl2] displays significant antimicrobial activity compared to the standard drug oxytetracycline and amphotericin B, which suggests the potential antimicrobial activity. The efficiency order towards Staphylococcus aureus is EN(3) < [Co2(EN-H)2Cl2] < standard drug < [Cu2(EN-H)2Cl2]. In case of E. coli, the order is EN(3) < standard drug < [Co2(EN-H)2Cl2] < [Cu2(EN-H)2Cl2].The efficacy order against Aspergillus niger is standard drug < EN(3) < [Co2(EN-H)2Cl2] < [Cu2(EN-H)2Cl2]. From the obtained results, it is arrived that the proposed complexes possess antimicrobial, as well as antifungal activities.
ISSN:3005-1193