Growth Kinetics of Ni<sub>3</sub>Ga<sub>7</sub> in Ni/Ga System During Interfacial Reaction Diffusion

In order to apply Ga alloys to flexible and wearable electronic devices, it is crucial to verify the mechanical reliability of interconnections between Ga and various metal electrodes. This study investigated the phase transformation kinetics and microstructural evolution in the Ni/Ga couple. The di...

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Main Authors: Jun Peng, Tao Wang, Shuai Zhang
Format: Article
Language:English
Published: MDPI AG 2025-05-01
Series:Crystals
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Online Access:https://www.mdpi.com/2073-4352/15/6/520
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author Jun Peng
Tao Wang
Shuai Zhang
author_facet Jun Peng
Tao Wang
Shuai Zhang
author_sort Jun Peng
collection DOAJ
description In order to apply Ga alloys to flexible and wearable electronic devices, it is crucial to verify the mechanical reliability of interconnections between Ga and various metal electrodes. This study investigated the phase transformation kinetics and microstructural evolution in the Ni/Ga couple. The diffusion reaction behavior between nickel and gallium was characterized from 323 K to 623 K for different annealing times. At temperatures lower than 323 K, no obvious intermetallic compound was identified after annealing, according to SEM observation. For reactions at temperatures higher than 423 K, the Ni<sub>3</sub>Ga<sub>7</sub> phase was identified as the only reaction product formed, occurring in a planar morphology along the Ni/Ga interface. The activation energy for the growth of Ni<sub>3</sub>Ga<sub>7</sub> was determined as 58.58 kJ/mol. The kinetic equation expressing the relationship between the thickness of interfacial intermetallic compound, annealing temperature, and time, is the following: <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mi>d</mi><mo>=</mo><mn>417174.55</mn><mrow><mrow><mi mathvariant="normal">exp</mi></mrow><mo>⁡</mo><mrow><mfenced separators="|"><mrow><mo>−</mo><mstyle scriptlevel="0" displaystyle="true"><mfrac><mrow><mn>58579</mn></mrow><mrow><mi>R</mi><mi>T</mi></mrow></mfrac></mstyle></mrow></mfenced><msup><mrow><mi>t</mi></mrow><mrow><mn>2.04</mn><mo>−</mo><mn>0.0024</mn><mi>T</mi></mrow></msup></mrow></mrow></mrow></semantics></math></inline-formula>.
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spelling doaj-art-3dfda28644144d8ea4ee07107ef31c192025-08-20T03:24:36ZengMDPI AGCrystals2073-43522025-05-0115652010.3390/cryst15060520Growth Kinetics of Ni<sub>3</sub>Ga<sub>7</sub> in Ni/Ga System During Interfacial Reaction DiffusionJun Peng0Tao Wang1Shuai Zhang2College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, ChinaCollege of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, ChinaCollege of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, ChinaIn order to apply Ga alloys to flexible and wearable electronic devices, it is crucial to verify the mechanical reliability of interconnections between Ga and various metal electrodes. This study investigated the phase transformation kinetics and microstructural evolution in the Ni/Ga couple. The diffusion reaction behavior between nickel and gallium was characterized from 323 K to 623 K for different annealing times. At temperatures lower than 323 K, no obvious intermetallic compound was identified after annealing, according to SEM observation. For reactions at temperatures higher than 423 K, the Ni<sub>3</sub>Ga<sub>7</sub> phase was identified as the only reaction product formed, occurring in a planar morphology along the Ni/Ga interface. The activation energy for the growth of Ni<sub>3</sub>Ga<sub>7</sub> was determined as 58.58 kJ/mol. The kinetic equation expressing the relationship between the thickness of interfacial intermetallic compound, annealing temperature, and time, is the following: <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mi>d</mi><mo>=</mo><mn>417174.55</mn><mrow><mrow><mi mathvariant="normal">exp</mi></mrow><mo>⁡</mo><mrow><mfenced separators="|"><mrow><mo>−</mo><mstyle scriptlevel="0" displaystyle="true"><mfrac><mrow><mn>58579</mn></mrow><mrow><mi>R</mi><mi>T</mi></mrow></mfrac></mstyle></mrow></mfenced><msup><mrow><mi>t</mi></mrow><mrow><mn>2.04</mn><mo>−</mo><mn>0.0024</mn><mi>T</mi></mrow></msup></mrow></mrow></mrow></semantics></math></inline-formula>.https://www.mdpi.com/2073-4352/15/6/520galliumintermetallic compoundinterfacial diffusionkineticsnickel
spellingShingle Jun Peng
Tao Wang
Shuai Zhang
Growth Kinetics of Ni<sub>3</sub>Ga<sub>7</sub> in Ni/Ga System During Interfacial Reaction Diffusion
Crystals
gallium
intermetallic compound
interfacial diffusion
kinetics
nickel
title Growth Kinetics of Ni<sub>3</sub>Ga<sub>7</sub> in Ni/Ga System During Interfacial Reaction Diffusion
title_full Growth Kinetics of Ni<sub>3</sub>Ga<sub>7</sub> in Ni/Ga System During Interfacial Reaction Diffusion
title_fullStr Growth Kinetics of Ni<sub>3</sub>Ga<sub>7</sub> in Ni/Ga System During Interfacial Reaction Diffusion
title_full_unstemmed Growth Kinetics of Ni<sub>3</sub>Ga<sub>7</sub> in Ni/Ga System During Interfacial Reaction Diffusion
title_short Growth Kinetics of Ni<sub>3</sub>Ga<sub>7</sub> in Ni/Ga System During Interfacial Reaction Diffusion
title_sort growth kinetics of ni sub 3 sub ga sub 7 sub in ni ga system during interfacial reaction diffusion
topic gallium
intermetallic compound
interfacial diffusion
kinetics
nickel
url https://www.mdpi.com/2073-4352/15/6/520
work_keys_str_mv AT junpeng growthkineticsofnisub3subgasub7subinnigasystemduringinterfacialreactiondiffusion
AT taowang growthkineticsofnisub3subgasub7subinnigasystemduringinterfacialreactiondiffusion
AT shuaizhang growthkineticsofnisub3subgasub7subinnigasystemduringinterfacialreactiondiffusion