Mitigating microstructural heterogeneity in laser-directed energy deposition Ni-based superalloys by heat accumulation in-situ heat treatment

The microstructure and mechanical properties of additively manufactured (AM) components often exhibit inherent heterogeneity due to their complex thermal histories. Building on conventional heat treatment strategies to mitigate microstructural heterogeneity, this study employed a continuous laser fo...

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Bibliographic Details
Main Authors: Chen Yang, Haibo Tang, Zhuo Li, Ziheng Zeng, Shujing Shi, Yansong Zhang, Chunjie Shen
Format: Article
Language:English
Published: Taylor & Francis Group 2025-12-01
Series:Virtual and Physical Prototyping
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Online Access:https://www.tandfonline.com/doi/10.1080/17452759.2025.2509614
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Summary:The microstructure and mechanical properties of additively manufactured (AM) components often exhibit inherent heterogeneity due to their complex thermal histories. Building on conventional heat treatment strategies to mitigate microstructural heterogeneity, this study employed a continuous laser forming method coupled with enhanced heat accumulation and the resulting in-situ heat treatment (IHT) to homogenise AM DD98 m samples. Results demonstrate that heat accumulation stabilises cooling rates at ∼65 K/s and maintains primary dendrite arm spacing (PDAS) at ∼55 μm. By promoting solid-state elemental diffusion, IHT significantly reduces elemental segregation, leading to extensive dissolution of γ-γ′ eutectic phases. Due to the IHT, the γ’ phase exhibits consistent volume fractions and comparable precipitate size distribution across specimens, yielding relatively homogeneous microhardness throughout the samples. Notably, the layered γ′ phase, previously underexplored in literature, is attributed to IHT-induced local Ostwald ripening, driven by aluminium (Al) diffusion gradients. This work successfully utilises IHT to control solid-state phase transformations, thereby reducing AM component heterogeneity. The findings advance strategies for tailoring microstructural uniformity in additive manufacturing, offering a novel pathway to mitigate microstructural heterogeneity in superalloys.
ISSN:1745-2759
1745-2767