Purification of Biodiesel from Waste Cooking Oil Using Bentonite as Dry Washing Agent

The process of biodiesel purification is an important step in getting biodiesel products that meet specifications as a substitute for fossil-based fuels. Dry washing method has been developed to achieve an effective purification strategy in order to produce high-quality biodiesel. Bentonite can be us...

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Main Authors: Nanda Suriaini, Tika Thalia Febriana, Andesta Yulanda, Adisalamun Adisalamun, Yanna Syamsuddin, Muhammad Dani Supardan
Format: Article
Language:English
Published: Universitas Syiah Kuala, Chemical Engineering Department 2019-12-01
Series:Jurnal Rekayasa Kimia & Lingkungan
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Online Access:https://jurnal.usk.ac.id/RKL/article/view/13165
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author Nanda Suriaini
Tika Thalia Febriana
Andesta Yulanda
Adisalamun Adisalamun
Yanna Syamsuddin
Muhammad Dani Supardan
author_facet Nanda Suriaini
Tika Thalia Febriana
Andesta Yulanda
Adisalamun Adisalamun
Yanna Syamsuddin
Muhammad Dani Supardan
author_sort Nanda Suriaini
collection DOAJ
description The process of biodiesel purification is an important step in getting biodiesel products that meet specifications as a substitute for fossil-based fuels. Dry washing method has been developed to achieve an effective purification strategy in order to produce high-quality biodiesel. Bentonite can be used as dry washing agent because it has a good adsorbing properties as well as a large pore and surface area therefore can attract polar substances such as glycerol and methanol. The purpose of this research is to know the capability of activated bentonite as dry washing agent for purification of biodiesel produced from waste cooking oil. The activation process of bentonite was carried out using sulfuric acid with concentration 1.5 M. Characterization of the bentonite was conducted using X-Ray Diffraction (XRD) for minerals content and Brunauer–Emmett–Teller (BET) method for surface area. Bentonite was used as dry washing agent for biodiesel purification by varying washing time (10, 20, 30, 40 and 50 minutes) and adsorbent amount (1, 2, 3, 4 and 5%). The experimental results showed that purification of biodiesel by dry washing using activated bentonite resulted in a better yield and quality than wet washing and dry washing using non-activated bentonite, except the acid number. The best operation condition resulted from this research is at 10 minutes washing time and 1% adsorbent with yield of 94.1%; acid number of 0.4208 mg KOH/gram; density of 0.8838 gram/cm3, viscosity of 3.0617 mm2/s and water content of 1.17%.
format Article
id doaj-art-3c8b610e17e04859a676df3492f6d73d
institution Kabale University
issn 1412-5064
2356-1661
language English
publishDate 2019-12-01
publisher Universitas Syiah Kuala, Chemical Engineering Department
record_format Article
series Jurnal Rekayasa Kimia & Lingkungan
spelling doaj-art-3c8b610e17e04859a676df3492f6d73d2025-08-20T03:25:15ZengUniversitas Syiah Kuala, Chemical Engineering DepartmentJurnal Rekayasa Kimia & Lingkungan1412-50642356-16612019-12-0114215516210.23955/rkl.v14i2.1316510517Purification of Biodiesel from Waste Cooking Oil Using Bentonite as Dry Washing AgentNanda Suriaini0Tika Thalia Febriana1Andesta Yulanda2Adisalamun Adisalamun3Yanna Syamsuddin4Muhammad Dani Supardan5Program Studi Magister Teknik Kimia, Fakultas Teknik, Universitas Syiah Kuala, Jln. Syech Abdurrauf, Darussalam, Banda Aceh 23111Jurusan Teknik Kimia, Fakultas Teknik, Universitas Syiah Kuala, Jln. Syech Abdurrauf, Darussalam, Banda Aceh 23111Jurusan Teknik Kimia, Fakultas Teknik, Universitas Syiah Kuala, Jln. Syech Abdurrauf, Darussalam, Banda Aceh 23111Jurusan Teknik Kimia, Fakultas Teknik, Universitas Syiah Kuala, Jln. Syech Abdurrauf, Darussalam, Banda Aceh 23111Jurusan Teknik Kimia, Fakultas Teknik, Universitas Syiah Kuala, Jln. Syech Abdurrauf, Darussalam, Banda Aceh 23111Jurusan Teknik Kimia, Fakultas Teknik, Universitas Syiah Kuala, Jln. Syech Abdurrauf, Darussalam, Banda Aceh 23111The process of biodiesel purification is an important step in getting biodiesel products that meet specifications as a substitute for fossil-based fuels. Dry washing method has been developed to achieve an effective purification strategy in order to produce high-quality biodiesel. Bentonite can be used as dry washing agent because it has a good adsorbing properties as well as a large pore and surface area therefore can attract polar substances such as glycerol and methanol. The purpose of this research is to know the capability of activated bentonite as dry washing agent for purification of biodiesel produced from waste cooking oil. The activation process of bentonite was carried out using sulfuric acid with concentration 1.5 M. Characterization of the bentonite was conducted using X-Ray Diffraction (XRD) for minerals content and Brunauer–Emmett–Teller (BET) method for surface area. Bentonite was used as dry washing agent for biodiesel purification by varying washing time (10, 20, 30, 40 and 50 minutes) and adsorbent amount (1, 2, 3, 4 and 5%). The experimental results showed that purification of biodiesel by dry washing using activated bentonite resulted in a better yield and quality than wet washing and dry washing using non-activated bentonite, except the acid number. The best operation condition resulted from this research is at 10 minutes washing time and 1% adsorbent with yield of 94.1%; acid number of 0.4208 mg KOH/gram; density of 0.8838 gram/cm3, viscosity of 3.0617 mm2/s and water content of 1.17%.https://jurnal.usk.ac.id/RKL/article/view/13165bentonitdry washing agentbiodieselwaste cooking oil
spellingShingle Nanda Suriaini
Tika Thalia Febriana
Andesta Yulanda
Adisalamun Adisalamun
Yanna Syamsuddin
Muhammad Dani Supardan
Purification of Biodiesel from Waste Cooking Oil Using Bentonite as Dry Washing Agent
Jurnal Rekayasa Kimia & Lingkungan
bentonit
dry washing agent
biodiesel
waste cooking oil
title Purification of Biodiesel from Waste Cooking Oil Using Bentonite as Dry Washing Agent
title_full Purification of Biodiesel from Waste Cooking Oil Using Bentonite as Dry Washing Agent
title_fullStr Purification of Biodiesel from Waste Cooking Oil Using Bentonite as Dry Washing Agent
title_full_unstemmed Purification of Biodiesel from Waste Cooking Oil Using Bentonite as Dry Washing Agent
title_short Purification of Biodiesel from Waste Cooking Oil Using Bentonite as Dry Washing Agent
title_sort purification of biodiesel from waste cooking oil using bentonite as dry washing agent
topic bentonit
dry washing agent
biodiesel
waste cooking oil
url https://jurnal.usk.ac.id/RKL/article/view/13165
work_keys_str_mv AT nandasuriaini purificationofbiodieselfromwastecookingoilusingbentoniteasdrywashingagent
AT tikathaliafebriana purificationofbiodieselfromwastecookingoilusingbentoniteasdrywashingagent
AT andestayulanda purificationofbiodieselfromwastecookingoilusingbentoniteasdrywashingagent
AT adisalamunadisalamun purificationofbiodieselfromwastecookingoilusingbentoniteasdrywashingagent
AT yannasyamsuddin purificationofbiodieselfromwastecookingoilusingbentoniteasdrywashingagent
AT muhammaddanisupardan purificationofbiodieselfromwastecookingoilusingbentoniteasdrywashingagent