Dual-feedback healing mechanism redefining anti-oxidation coatings in fiber-reinforced composites

This study introduces a pioneering design concept termed the “dual-feedback healing mechanism”, which investigates the relationship between oxidation products and protective coatings. Specifically, it focuses on channeling oxidation products generated at exposed cracks in the substrate to interact w...

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Main Authors: Yuanshuai Wang, Xinyu Wang, Pianpian Zhang, Anqi Lun, Yuewei Li, Yi Wang, Lizhe Xing, Zhengyang Fu, Ya’nan Yang, Long Xia
Format: Article
Language:English
Published: Tsinghua University Press 2024-10-01
Series:Journal of Advanced Ceramics
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Online Access:https://www.sciopen.com/article/10.26599/JAC.2024.9220966
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author Yuanshuai Wang
Xinyu Wang
Pianpian Zhang
Anqi Lun
Yuewei Li
Yi Wang
Lizhe Xing
Zhengyang Fu
Ya’nan Yang
Long Xia
author_facet Yuanshuai Wang
Xinyu Wang
Pianpian Zhang
Anqi Lun
Yuewei Li
Yi Wang
Lizhe Xing
Zhengyang Fu
Ya’nan Yang
Long Xia
author_sort Yuanshuai Wang
collection DOAJ
description This study introduces a pioneering design concept termed the “dual-feedback healing mechanism”, which investigates the relationship between oxidation products and protective coatings. Specifically, it focuses on channeling oxidation products generated at exposed cracks in the substrate to interact with the antioxidant coatings, enabling a self-repair mechanism for cracks. BNf/SiBN was chosen as the ceramic matrix, while the Si‒O‒Al system served as the antioxidant coating. The dynamic process of obtaining Si–O–Al (SOAC) coating involving the pyrolysis of organic precursors and the dual-feedback healing mechanism were systematically investigated. These findings indicate that when the temperature surpasses 1150 °C, the exposed BN fibers at the cracks are oxidized, transforming into B2O3(g). Subsequently, B2O3(g) reacts with SiO2, forming a SiBO mixture. The mixture effectively diminishes the viscosity of the coating, enabling it to flow and form a fresh protective layer that effectively blocks O2 infiltration. Consequently, after oxidation at 1500 °C, the coated samples experience a mere 3% weight loss. This technology emphasizes the interconnectivity during material transformation, utilizing matrix oxidation products as a driving force for self-healing of the coating. This approach achieves intelligent-like, targeted closure of oxygen pathways, thereby pioneering a novel concept and direction for the advancement of antioxidant coatings. Consequently, this approach not only enhances our understanding of the fundamental nature of “self-healing” but also holds significant potential in the development of reparable antioxidant coatings.
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issn 2226-4108
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publishDate 2024-10-01
publisher Tsinghua University Press
record_format Article
series Journal of Advanced Ceramics
spelling doaj-art-3c70d6238eba4213b58237eeac9dcfce2025-08-20T02:13:56ZengTsinghua University PressJournal of Advanced Ceramics2226-41082227-85082024-10-0113101643165410.26599/JAC.2024.9220966Dual-feedback healing mechanism redefining anti-oxidation coatings in fiber-reinforced compositesYuanshuai Wang0Xinyu Wang1Pianpian Zhang2Anqi Lun3Yuewei Li4Yi Wang5Lizhe Xing6Zhengyang Fu7Ya’nan Yang8Long Xia9School of Materials Science and Engineering, Harbin Institute of Technology (Weihai), Weihai 264209, ChinaSchool of Materials Science and Engineering, Harbin Institute of Technology (Weihai), Weihai 264209, ChinaSchool of Materials Science and Engineering, Harbin Institute of Technology (Weihai), Weihai 264209, ChinaSchool of Materials Science and Engineering, Harbin Institute of Technology (Weihai), Weihai 264209, ChinaSchool of Materials Science and Engineering, Harbin Institute of Technology (Weihai), Weihai 264209, ChinaSchool of Materials Science and Engineering, Harbin Institute of Technology (Weihai), Weihai 264209, ChinaSchool of Materials Science and Engineering, Harbin Institute of Technology (Weihai), Weihai 264209, ChinaSchool of Materials Science and Engineering, Harbin Institute of Technology (Weihai), Weihai 264209, ChinaSchool of Materials Science and Engineering, Harbin Institute of Technology (Weihai), Weihai 264209, ChinaSchool of Materials Science and Engineering, Harbin Institute of Technology (Weihai), Weihai 264209, ChinaThis study introduces a pioneering design concept termed the “dual-feedback healing mechanism”, which investigates the relationship between oxidation products and protective coatings. Specifically, it focuses on channeling oxidation products generated at exposed cracks in the substrate to interact with the antioxidant coatings, enabling a self-repair mechanism for cracks. BNf/SiBN was chosen as the ceramic matrix, while the Si‒O‒Al system served as the antioxidant coating. The dynamic process of obtaining Si–O–Al (SOAC) coating involving the pyrolysis of organic precursors and the dual-feedback healing mechanism were systematically investigated. These findings indicate that when the temperature surpasses 1150 °C, the exposed BN fibers at the cracks are oxidized, transforming into B2O3(g). Subsequently, B2O3(g) reacts with SiO2, forming a SiBO mixture. The mixture effectively diminishes the viscosity of the coating, enabling it to flow and form a fresh protective layer that effectively blocks O2 infiltration. Consequently, after oxidation at 1500 °C, the coated samples experience a mere 3% weight loss. This technology emphasizes the interconnectivity during material transformation, utilizing matrix oxidation products as a driving force for self-healing of the coating. This approach achieves intelligent-like, targeted closure of oxygen pathways, thereby pioneering a novel concept and direction for the advancement of antioxidant coatings. Consequently, this approach not only enhances our understanding of the fundamental nature of “self-healing” but also holds significant potential in the development of reparable antioxidant coatings.https://www.sciopen.com/article/10.26599/JAC.2024.9220966antioxidant coatingdual-feedbackbnf/sibn compositesi–o–al coatingself-healing
spellingShingle Yuanshuai Wang
Xinyu Wang
Pianpian Zhang
Anqi Lun
Yuewei Li
Yi Wang
Lizhe Xing
Zhengyang Fu
Ya’nan Yang
Long Xia
Dual-feedback healing mechanism redefining anti-oxidation coatings in fiber-reinforced composites
Journal of Advanced Ceramics
antioxidant coating
dual-feedback
bnf/sibn composite
si–o–al coating
self-healing
title Dual-feedback healing mechanism redefining anti-oxidation coatings in fiber-reinforced composites
title_full Dual-feedback healing mechanism redefining anti-oxidation coatings in fiber-reinforced composites
title_fullStr Dual-feedback healing mechanism redefining anti-oxidation coatings in fiber-reinforced composites
title_full_unstemmed Dual-feedback healing mechanism redefining anti-oxidation coatings in fiber-reinforced composites
title_short Dual-feedback healing mechanism redefining anti-oxidation coatings in fiber-reinforced composites
title_sort dual feedback healing mechanism redefining anti oxidation coatings in fiber reinforced composites
topic antioxidant coating
dual-feedback
bnf/sibn composite
si–o–al coating
self-healing
url https://www.sciopen.com/article/10.26599/JAC.2024.9220966
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AT anqilun dualfeedbackhealingmechanismredefiningantioxidationcoatingsinfiberreinforcedcomposites
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