Proton-coupled electron transfer controls peroxide activation initiated by a solid-water interface

Abstract Decentralized water treatment technologies, designed to align with the specific characteristics of the water source and the requirements of the user, are gaining prominence due to their cost and energy-saving advantages over traditional centralized systems. The application of chemical water...

Full description

Saved in:
Bibliographic Details
Main Authors: Jian-Hua Chen, Wan-Ting Li, Kun-Yu Cai, Hui-Jie Tu, Zi-Tong Long, Shoaib Akhtar, Lin-Dong Liu
Format: Article
Language:English
Published: Nature Portfolio 2025-04-01
Series:Nature Communications
Online Access:https://doi.org/10.1038/s41467-025-58917-w
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849311082489839616
author Jian-Hua Chen
Wan-Ting Li
Kun-Yu Cai
Hui-Jie Tu
Zi-Tong Long
Shoaib Akhtar
Lin-Dong Liu
author_facet Jian-Hua Chen
Wan-Ting Li
Kun-Yu Cai
Hui-Jie Tu
Zi-Tong Long
Shoaib Akhtar
Lin-Dong Liu
author_sort Jian-Hua Chen
collection DOAJ
description Abstract Decentralized water treatment technologies, designed to align with the specific characteristics of the water source and the requirements of the user, are gaining prominence due to their cost and energy-saving advantages over traditional centralized systems. The application of chemical water treatment via heterogeneous advanced oxidation processes using peroxide (O–O) represents a potentially attractive treatment option. These processes serve to initiate redox processes at the solid-water interface. Nevertheless, the oxidation mechanism exemplified by the typical Fenton-like persulfate-based heterogeneous oxidation, in which electron transfer dominates, is almost universally accepted. Here, we present experimental results that challenge this view. At the solid-liquid interface, it is demonstrated that protons are thermodynamically coupled to electrons. In situ quantitative titration provides direct experimental evidence that the coupling ratio of protons to transferred electrons is almost 1:1. Comprehensive thermodynamic analyses further demonstrate that a net proton-coupled electron transfer occurs, with both protons and electrons entering the redox cycle. These findings will inform future developments in O–O activation technologies, enabling more efficient redox activity via the tight coupling of protons and electrons.
format Article
id doaj-art-3bf6fb2a4dba4a2983285a4fc2662e87
institution Kabale University
issn 2041-1723
language English
publishDate 2025-04-01
publisher Nature Portfolio
record_format Article
series Nature Communications
spelling doaj-art-3bf6fb2a4dba4a2983285a4fc2662e872025-08-20T03:53:32ZengNature PortfolioNature Communications2041-17232025-04-0116111110.1038/s41467-025-58917-wProton-coupled electron transfer controls peroxide activation initiated by a solid-water interfaceJian-Hua Chen0Wan-Ting Li1Kun-Yu Cai2Hui-Jie Tu3Zi-Tong Long4Shoaib Akhtar5Lin-Dong Liu6Interdisciplinary Research Centre for Agriculture Green Development in Yangtze River Basin, Department of Environmental Sciences and Engineering, College of Resources and Environment, Southwest UniversityInterdisciplinary Research Centre for Agriculture Green Development in Yangtze River Basin, Department of Environmental Sciences and Engineering, College of Resources and Environment, Southwest UniversityInterdisciplinary Research Centre for Agriculture Green Development in Yangtze River Basin, Department of Environmental Sciences and Engineering, College of Resources and Environment, Southwest UniversityInterdisciplinary Research Centre for Agriculture Green Development in Yangtze River Basin, Department of Environmental Sciences and Engineering, College of Resources and Environment, Southwest UniversityInterdisciplinary Research Centre for Agriculture Green Development in Yangtze River Basin, Department of Environmental Sciences and Engineering, College of Resources and Environment, Southwest UniversityInterdisciplinary Research Centre for Agriculture Green Development in Yangtze River Basin, Department of Environmental Sciences and Engineering, College of Resources and Environment, Southwest UniversityInterdisciplinary Research Centre for Agriculture Green Development in Yangtze River Basin, Department of Environmental Sciences and Engineering, College of Resources and Environment, Southwest UniversityAbstract Decentralized water treatment technologies, designed to align with the specific characteristics of the water source and the requirements of the user, are gaining prominence due to their cost and energy-saving advantages over traditional centralized systems. The application of chemical water treatment via heterogeneous advanced oxidation processes using peroxide (O–O) represents a potentially attractive treatment option. These processes serve to initiate redox processes at the solid-water interface. Nevertheless, the oxidation mechanism exemplified by the typical Fenton-like persulfate-based heterogeneous oxidation, in which electron transfer dominates, is almost universally accepted. Here, we present experimental results that challenge this view. At the solid-liquid interface, it is demonstrated that protons are thermodynamically coupled to electrons. In situ quantitative titration provides direct experimental evidence that the coupling ratio of protons to transferred electrons is almost 1:1. Comprehensive thermodynamic analyses further demonstrate that a net proton-coupled electron transfer occurs, with both protons and electrons entering the redox cycle. These findings will inform future developments in O–O activation technologies, enabling more efficient redox activity via the tight coupling of protons and electrons.https://doi.org/10.1038/s41467-025-58917-w
spellingShingle Jian-Hua Chen
Wan-Ting Li
Kun-Yu Cai
Hui-Jie Tu
Zi-Tong Long
Shoaib Akhtar
Lin-Dong Liu
Proton-coupled electron transfer controls peroxide activation initiated by a solid-water interface
Nature Communications
title Proton-coupled electron transfer controls peroxide activation initiated by a solid-water interface
title_full Proton-coupled electron transfer controls peroxide activation initiated by a solid-water interface
title_fullStr Proton-coupled electron transfer controls peroxide activation initiated by a solid-water interface
title_full_unstemmed Proton-coupled electron transfer controls peroxide activation initiated by a solid-water interface
title_short Proton-coupled electron transfer controls peroxide activation initiated by a solid-water interface
title_sort proton coupled electron transfer controls peroxide activation initiated by a solid water interface
url https://doi.org/10.1038/s41467-025-58917-w
work_keys_str_mv AT jianhuachen protoncoupledelectrontransfercontrolsperoxideactivationinitiatedbyasolidwaterinterface
AT wantingli protoncoupledelectrontransfercontrolsperoxideactivationinitiatedbyasolidwaterinterface
AT kunyucai protoncoupledelectrontransfercontrolsperoxideactivationinitiatedbyasolidwaterinterface
AT huijietu protoncoupledelectrontransfercontrolsperoxideactivationinitiatedbyasolidwaterinterface
AT zitonglong protoncoupledelectrontransfercontrolsperoxideactivationinitiatedbyasolidwaterinterface
AT shoaibakhtar protoncoupledelectrontransfercontrolsperoxideactivationinitiatedbyasolidwaterinterface
AT lindongliu protoncoupledelectrontransfercontrolsperoxideactivationinitiatedbyasolidwaterinterface