Using QCM‐D for Real‐Time Analysis of Cell Adhesion Dynamics at Biointerfaces

Abstract Efficient cell adhesion is crucial for host tissue attachment and improving implant integration. This study aims at investigating adhesion of human gingival fibroblasts to functionalized biomaterial surfaces using quartz crystal microbalance with dissipation (QCM‐D) and analyzing the dynami...

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Main Authors: Agnes Rogala, Hanna Tiainen, Daria Zaytseva‐Zotova
Format: Article
Language:English
Published: Wiley-VCH 2025-05-01
Series:Advanced Materials Interfaces
Subjects:
Online Access:https://doi.org/10.1002/admi.202400811
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author Agnes Rogala
Hanna Tiainen
Daria Zaytseva‐Zotova
author_facet Agnes Rogala
Hanna Tiainen
Daria Zaytseva‐Zotova
author_sort Agnes Rogala
collection DOAJ
description Abstract Efficient cell adhesion is crucial for host tissue attachment and improving implant integration. This study aims at investigating adhesion of human gingival fibroblasts to functionalized biomaterial surfaces using quartz crystal microbalance with dissipation (QCM‐D) and analyzing the dynamics of focal adhesion (FA) formation during this process. The QCM‐D responses are correlated with changes in cell morphology and activation of focal adhesion kinase (FAK) in the absence or presence of serum proteins. As model surfaces, this work uses polystyrene oxidized by UV/ozone treatment (PSox) and tannic acid nanocoating formed on polystyrene (TA60). Compared to PSox, reduced cell adhesion on TA60 with fibroblast establishing fewer FAs is observed in this work. The addition of serum promotes more stable cell adhesion, although the adsorbed protein corona slows initial cell spreading and FAK activation. Further, this work examines whether there is a relationship between QCM‐D responses and FAK activation. The data shows a positive correlation between the energy dissipation and temporal changes in phosphorylated FAK (pY397FAK), although the absolute value of pY397FAK cannot be derived from the QCM‐D response. Thus, this study demonstrates the usefulness of the QCM‐D as a technique for quantitative non‐invasive analysis of cell adhesion to functionalized surfaces.
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spelling doaj-art-3bc0686ea6be4dcd84379ebcfd65c7a12025-08-20T01:48:16ZengWiley-VCHAdvanced Materials Interfaces2196-73502025-05-01129n/an/a10.1002/admi.202400811Using QCM‐D for Real‐Time Analysis of Cell Adhesion Dynamics at BiointerfacesAgnes Rogala0Hanna Tiainen1Daria Zaytseva‐Zotova2Department of Biomaterials Institute of Clinical Dentistry University of Oslo Postboks 1109 Blindern Oslo 0317 NorwayDepartment of Biomaterials Institute of Clinical Dentistry University of Oslo Postboks 1109 Blindern Oslo 0317 NorwayDepartment of Biomaterials Institute of Clinical Dentistry University of Oslo Postboks 1109 Blindern Oslo 0317 NorwayAbstract Efficient cell adhesion is crucial for host tissue attachment and improving implant integration. This study aims at investigating adhesion of human gingival fibroblasts to functionalized biomaterial surfaces using quartz crystal microbalance with dissipation (QCM‐D) and analyzing the dynamics of focal adhesion (FA) formation during this process. The QCM‐D responses are correlated with changes in cell morphology and activation of focal adhesion kinase (FAK) in the absence or presence of serum proteins. As model surfaces, this work uses polystyrene oxidized by UV/ozone treatment (PSox) and tannic acid nanocoating formed on polystyrene (TA60). Compared to PSox, reduced cell adhesion on TA60 with fibroblast establishing fewer FAs is observed in this work. The addition of serum promotes more stable cell adhesion, although the adsorbed protein corona slows initial cell spreading and FAK activation. Further, this work examines whether there is a relationship between QCM‐D responses and FAK activation. The data shows a positive correlation between the energy dissipation and temporal changes in phosphorylated FAK (pY397FAK), although the absolute value of pY397FAK cannot be derived from the QCM‐D response. Thus, this study demonstrates the usefulness of the QCM‐D as a technique for quantitative non‐invasive analysis of cell adhesion to functionalized surfaces.https://doi.org/10.1002/admi.202400811FAKfocal adhesionsQCM‐Dsurface functionalizationtannic acid
spellingShingle Agnes Rogala
Hanna Tiainen
Daria Zaytseva‐Zotova
Using QCM‐D for Real‐Time Analysis of Cell Adhesion Dynamics at Biointerfaces
Advanced Materials Interfaces
FAK
focal adhesions
QCM‐D
surface functionalization
tannic acid
title Using QCM‐D for Real‐Time Analysis of Cell Adhesion Dynamics at Biointerfaces
title_full Using QCM‐D for Real‐Time Analysis of Cell Adhesion Dynamics at Biointerfaces
title_fullStr Using QCM‐D for Real‐Time Analysis of Cell Adhesion Dynamics at Biointerfaces
title_full_unstemmed Using QCM‐D for Real‐Time Analysis of Cell Adhesion Dynamics at Biointerfaces
title_short Using QCM‐D for Real‐Time Analysis of Cell Adhesion Dynamics at Biointerfaces
title_sort using qcm d for real time analysis of cell adhesion dynamics at biointerfaces
topic FAK
focal adhesions
QCM‐D
surface functionalization
tannic acid
url https://doi.org/10.1002/admi.202400811
work_keys_str_mv AT agnesrogala usingqcmdforrealtimeanalysisofcelladhesiondynamicsatbiointerfaces
AT hannatiainen usingqcmdforrealtimeanalysisofcelladhesiondynamicsatbiointerfaces
AT dariazaytsevazotova usingqcmdforrealtimeanalysisofcelladhesiondynamicsatbiointerfaces