Transparent Al-Doped ZnO Thin Films for High-Sensitivity NO<sub>2</sub> Gas Sensing

This study developed a transparent NO<sub>2</sub> gas sensor with enhanced sensing performance and high optical transmittance. Al-doped ZnO thin films were deposited by atomic layer deposition, which was chosen for its capability to precisely control surface chemistry at the atomic scale...

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Main Authors: So-Young Bak, Se-Hyeong Lee, Hyeongrok Jang, Minseong Kim, Sungjae Kim, Moonsuk Yi
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Sensors
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Online Access:https://www.mdpi.com/1424-8220/25/12/3622
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author So-Young Bak
Se-Hyeong Lee
Hyeongrok Jang
Minseong Kim
Sungjae Kim
Moonsuk Yi
author_facet So-Young Bak
Se-Hyeong Lee
Hyeongrok Jang
Minseong Kim
Sungjae Kim
Moonsuk Yi
author_sort So-Young Bak
collection DOAJ
description This study developed a transparent NO<sub>2</sub> gas sensor with enhanced sensing performance and high optical transmittance. Al-doped ZnO thin films were deposited by atomic layer deposition, which was chosen for its capability to precisely control surface chemistry at the atomic scale. Oxygen vacancies were effectively introduced by utilizing trimethylaluminum, a strongly reducing Al<sub>2</sub>O<sub>3</sub> precursor, thereby increasing carrier concentration and enhancing gas-sensing performance. By adjusting the Al doping level, the optimized device achieved a 50 °C reduction in operating temperature, a 66.2-fold increase in sensitivity at 150 °C, and shortened response and recovery times. The morphology, crystallinity, and elemental distribution were analyzed using transmission electron microscopy, selected area electron diffraction, and energy-dispersive X-ray spectroscopy, while chemical bonding states were investigated via X-ray photoelectron spectroscopy. Optical properties were characterized using UV–visible spectroscopy, confirming an average transmittance of approximately 80% in the visible range. These results demonstrate the promise of transparent oxide gas sensors for integration into next-generation electronics and Internet of Things-based environmental monitoring systems.
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institution Kabale University
issn 1424-8220
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publisher MDPI AG
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series Sensors
spelling doaj-art-39b71fd2893e4d5fa2b648ac4e64225c2025-08-20T03:27:39ZengMDPI AGSensors1424-82202025-06-012512362210.3390/s25123622Transparent Al-Doped ZnO Thin Films for High-Sensitivity NO<sub>2</sub> Gas SensingSo-Young Bak0Se-Hyeong Lee1Hyeongrok Jang2Minseong Kim3Sungjae Kim4Moonsuk Yi5Department of Electrical and Electronics Engineering, Pusan National University, Busan 46241, Republic of KoreaDepartment of Electrical and Electronics Engineering, Pusan National University, Busan 46241, Republic of KoreaDepartment of Electrical and Electronics Engineering, Pusan National University, Busan 46241, Republic of KoreaDepartment of Electrical and Electronics Engineering, Pusan National University, Busan 46241, Republic of KoreaDepartment of Electrical and Electronics Engineering, Pusan National University, Busan 46241, Republic of KoreaDepartment of Electrical and Electronics Engineering, Pusan National University, Busan 46241, Republic of KoreaThis study developed a transparent NO<sub>2</sub> gas sensor with enhanced sensing performance and high optical transmittance. Al-doped ZnO thin films were deposited by atomic layer deposition, which was chosen for its capability to precisely control surface chemistry at the atomic scale. Oxygen vacancies were effectively introduced by utilizing trimethylaluminum, a strongly reducing Al<sub>2</sub>O<sub>3</sub> precursor, thereby increasing carrier concentration and enhancing gas-sensing performance. By adjusting the Al doping level, the optimized device achieved a 50 °C reduction in operating temperature, a 66.2-fold increase in sensitivity at 150 °C, and shortened response and recovery times. The morphology, crystallinity, and elemental distribution were analyzed using transmission electron microscopy, selected area electron diffraction, and energy-dispersive X-ray spectroscopy, while chemical bonding states were investigated via X-ray photoelectron spectroscopy. Optical properties were characterized using UV–visible spectroscopy, confirming an average transmittance of approximately 80% in the visible range. These results demonstrate the promise of transparent oxide gas sensors for integration into next-generation electronics and Internet of Things-based environmental monitoring systems.https://www.mdpi.com/1424-8220/25/12/3622Al-doped ZnOoxygen vacanciesgas sensorNO<sub>2</sub>Trimethylaluminum
spellingShingle So-Young Bak
Se-Hyeong Lee
Hyeongrok Jang
Minseong Kim
Sungjae Kim
Moonsuk Yi
Transparent Al-Doped ZnO Thin Films for High-Sensitivity NO<sub>2</sub> Gas Sensing
Sensors
Al-doped ZnO
oxygen vacancies
gas sensor
NO<sub>2</sub>
Trimethylaluminum
title Transparent Al-Doped ZnO Thin Films for High-Sensitivity NO<sub>2</sub> Gas Sensing
title_full Transparent Al-Doped ZnO Thin Films for High-Sensitivity NO<sub>2</sub> Gas Sensing
title_fullStr Transparent Al-Doped ZnO Thin Films for High-Sensitivity NO<sub>2</sub> Gas Sensing
title_full_unstemmed Transparent Al-Doped ZnO Thin Films for High-Sensitivity NO<sub>2</sub> Gas Sensing
title_short Transparent Al-Doped ZnO Thin Films for High-Sensitivity NO<sub>2</sub> Gas Sensing
title_sort transparent al doped zno thin films for high sensitivity no sub 2 sub gas sensing
topic Al-doped ZnO
oxygen vacancies
gas sensor
NO<sub>2</sub>
Trimethylaluminum
url https://www.mdpi.com/1424-8220/25/12/3622
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