A simplified system for the detection of antennal responses to host-borne volatile organic compounds in sand flies

Abstract Background Phlebotomus (Larroussius) perniciosus (Diptera: Psychodidae) is the most common and predominant vector of Leishmania infantum in the Western Mediterranean region. Volatile organic compounds (VOCs) produced by vertebrates are important cues affecting the behaviour of blood-feeding...

Full description

Saved in:
Bibliographic Details
Main Authors: Onofrio Marco Pistillo, Priscilla Farina, Marcos Antonio Bezerra-Santos, Ilaria D’Isita, Petr Volf, Domenico Otranto, Giovanni Benelli, Giacinto Salvatore Germinara
Format: Article
Language:English
Published: BMC 2025-08-01
Series:Parasites & Vectors
Subjects:
Online Access:https://doi.org/10.1186/s13071-025-06998-3
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849226561399554048
author Onofrio Marco Pistillo
Priscilla Farina
Marcos Antonio Bezerra-Santos
Ilaria D’Isita
Petr Volf
Domenico Otranto
Giovanni Benelli
Giacinto Salvatore Germinara
author_facet Onofrio Marco Pistillo
Priscilla Farina
Marcos Antonio Bezerra-Santos
Ilaria D’Isita
Petr Volf
Domenico Otranto
Giovanni Benelli
Giacinto Salvatore Germinara
author_sort Onofrio Marco Pistillo
collection DOAJ
description Abstract Background Phlebotomus (Larroussius) perniciosus (Diptera: Psychodidae) is the most common and predominant vector of Leishmania infantum in the Western Mediterranean region. Volatile organic compounds (VOCs) produced by vertebrates are important cues affecting the behaviour of blood-feeding insects. Generally, the identification of putative behaviourally active VOCs involves three distinct phases: extraction, chemical characterization and chemoreceptivity evaluation using electrophysiological techniques. Here, we present a simplified gas chromatography–mass spectrometry–electroantennographic detection (GC–MS–EAD) setup adapted for screening bioactive compounds in sand flies, in which the chemical identification and antennal responses are recorded simultaneously. Methods The method integrates: (i) a flow-splitter that balances the flow rate of the two outgoing streams, (ii) GC columns with different lengths and diameters in the two sections splitter-MS and splitter-EAD and (iii) an antennal signal amplifier. The GC–MS–EAD analysis was applied to headspace solid-phase microextraction (HS-SPME) extracts from a healthy dog, and antennal responses were recorded in female P. perniciosus sand flies. Results The canine VOC profile was predominantly composed of aldehydes, with hexanal and nonanal eliciting the strongest antennal responses in P. perniciosus. Conclusions This simplified GC–MS-EAD system shows promise for broader application in the study of host–vector interactions. Its use across different host–vector pairs may enhance our understanding of these relationships and inform the development of strategies for integrated vector monitoring and control. Graphical Abstract
format Article
id doaj-art-37a0bfb6bde4457ab67f100686097fd3
institution Kabale University
issn 1756-3305
language English
publishDate 2025-08-01
publisher BMC
record_format Article
series Parasites & Vectors
spelling doaj-art-37a0bfb6bde4457ab67f100686097fd32025-08-24T11:10:30ZengBMCParasites & Vectors1756-33052025-08-011811810.1186/s13071-025-06998-3A simplified system for the detection of antennal responses to host-borne volatile organic compounds in sand fliesOnofrio Marco Pistillo0Priscilla Farina1Marcos Antonio Bezerra-Santos2Ilaria D’Isita3Petr Volf4Domenico Otranto5Giovanni Benelli6Giacinto Salvatore Germinara7Department of Agricultural Sciences, Food, Natural Resources and Engineering, University of FoggiaDepartment of Agriculture, Food and Environment, University of PisaDepartment of Veterinary Medicine, University of BariDepartment of Agricultural Sciences, Food, Natural Resources and Engineering, University of FoggiaDepartment of Parasitology, Faculty of Science, Charles UniversityDepartment of Veterinary Medicine, University of BariDepartment of Agriculture, Food and Environment, University of PisaDepartment of Agricultural Sciences, Food, Natural Resources and Engineering, University of FoggiaAbstract Background Phlebotomus (Larroussius) perniciosus (Diptera: Psychodidae) is the most common and predominant vector of Leishmania infantum in the Western Mediterranean region. Volatile organic compounds (VOCs) produced by vertebrates are important cues affecting the behaviour of blood-feeding insects. Generally, the identification of putative behaviourally active VOCs involves three distinct phases: extraction, chemical characterization and chemoreceptivity evaluation using electrophysiological techniques. Here, we present a simplified gas chromatography–mass spectrometry–electroantennographic detection (GC–MS–EAD) setup adapted for screening bioactive compounds in sand flies, in which the chemical identification and antennal responses are recorded simultaneously. Methods The method integrates: (i) a flow-splitter that balances the flow rate of the two outgoing streams, (ii) GC columns with different lengths and diameters in the two sections splitter-MS and splitter-EAD and (iii) an antennal signal amplifier. The GC–MS–EAD analysis was applied to headspace solid-phase microextraction (HS-SPME) extracts from a healthy dog, and antennal responses were recorded in female P. perniciosus sand flies. Results The canine VOC profile was predominantly composed of aldehydes, with hexanal and nonanal eliciting the strongest antennal responses in P. perniciosus. Conclusions This simplified GC–MS-EAD system shows promise for broader application in the study of host–vector interactions. Its use across different host–vector pairs may enhance our understanding of these relationships and inform the development of strategies for integrated vector monitoring and control. Graphical Abstracthttps://doi.org/10.1186/s13071-025-06998-3ElectroantennographyHS-SPMEPsychodidaePhlebotominaeLeishmania infantumLeishmaniasis
spellingShingle Onofrio Marco Pistillo
Priscilla Farina
Marcos Antonio Bezerra-Santos
Ilaria D’Isita
Petr Volf
Domenico Otranto
Giovanni Benelli
Giacinto Salvatore Germinara
A simplified system for the detection of antennal responses to host-borne volatile organic compounds in sand flies
Parasites & Vectors
Electroantennography
HS-SPME
Psychodidae
Phlebotominae
Leishmania infantum
Leishmaniasis
title A simplified system for the detection of antennal responses to host-borne volatile organic compounds in sand flies
title_full A simplified system for the detection of antennal responses to host-borne volatile organic compounds in sand flies
title_fullStr A simplified system for the detection of antennal responses to host-borne volatile organic compounds in sand flies
title_full_unstemmed A simplified system for the detection of antennal responses to host-borne volatile organic compounds in sand flies
title_short A simplified system for the detection of antennal responses to host-borne volatile organic compounds in sand flies
title_sort simplified system for the detection of antennal responses to host borne volatile organic compounds in sand flies
topic Electroantennography
HS-SPME
Psychodidae
Phlebotominae
Leishmania infantum
Leishmaniasis
url https://doi.org/10.1186/s13071-025-06998-3
work_keys_str_mv AT onofriomarcopistillo asimplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT priscillafarina asimplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT marcosantoniobezerrasantos asimplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT ilariadisita asimplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT petrvolf asimplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT domenicootranto asimplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT giovannibenelli asimplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT giacintosalvatoregerminara asimplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT onofriomarcopistillo simplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT priscillafarina simplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT marcosantoniobezerrasantos simplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT ilariadisita simplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT petrvolf simplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT domenicootranto simplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT giovannibenelli simplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies
AT giacintosalvatoregerminara simplifiedsystemforthedetectionofantennalresponsestohostbornevolatileorganiccompoundsinsandflies