Impregnation of ZnO onto a Vegetal Activated Carbon from Algerian Olive Waste: A Sustainable Photocatalyst for Degradation of Ethyl Violet Dye

This study is aimed at developing a simple and low-cost method to fabricate ZnO-loaded porous activated carbon (AC-ZnO) prepared from the Algerian olive-waste cakes and utilize it as a photocatalyst for the degradation of Ethyl Violet dye. The synthesized AC-ZnO material was characterized using powd...

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Main Authors: Ala Abdessemed, Shivatharsiny Rasalingam, Sanna Abdessemed, Kamel El Zin Djebbar, Ranjit Koodali
Format: Article
Language:English
Published: Wiley 2019-01-01
Series:International Journal of Photoenergy
Online Access:http://dx.doi.org/10.1155/2019/4714107
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author Ala Abdessemed
Shivatharsiny Rasalingam
Sanna Abdessemed
Kamel El Zin Djebbar
Ranjit Koodali
author_facet Ala Abdessemed
Shivatharsiny Rasalingam
Sanna Abdessemed
Kamel El Zin Djebbar
Ranjit Koodali
author_sort Ala Abdessemed
collection DOAJ
description This study is aimed at developing a simple and low-cost method to fabricate ZnO-loaded porous activated carbon (AC-ZnO) prepared from the Algerian olive-waste cakes and utilize it as a photocatalyst for the degradation of Ethyl Violet dye. The synthesized AC-ZnO material was characterized using powder X-ray diffraction, BET surface area measurements, Raman microscopy, thermogravimetric analysis, UV-visible diffuse reflectance spectroscopy, and zeta potential measurements. The degradation efficiency was evaluated with Ethyl Violet (EV) dye in aqueous solution under UV irradiation supplied by a Xenon arc lamp through a Pyrex glass filter (cutoff 280 nm), and the degraded products were identified by using electrospray ionization mass spectroscopy. Additional experiments were carried out under N2 flow and with isopropyl alcohol to examine the role of superoxide and hydroxyl radicals, respectively. The amount of ●OH radical formed on irradiated AC-ZnO was tested with terephthalic acid which can act as a chemical trap for the ●OH radicals. The results from this study indicate that the AC-ZnO is a potential catalyst for the pollutant removal and the ●OH radicals are the key species for the degradation of EV. Further, this study opens up an opportunity to produce cheaper activated carbon support from olive wastes for environmental remediation applications.
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issn 1110-662X
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publishDate 2019-01-01
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series International Journal of Photoenergy
spelling doaj-art-377323c6547c4fbfbd38d4f7a78b6f862025-08-20T03:20:30ZengWileyInternational Journal of Photoenergy1110-662X1687-529X2019-01-01201910.1155/2019/47141074714107Impregnation of ZnO onto a Vegetal Activated Carbon from Algerian Olive Waste: A Sustainable Photocatalyst for Degradation of Ethyl Violet DyeAla Abdessemed0Shivatharsiny Rasalingam1Sanna Abdessemed2Kamel El Zin Djebbar3Ranjit Koodali4Biotechnology Research Centre, BPE 73, Ali Mendjeli, Nouvelle Ville, 25000 Constantine, AlgeriaDepartment of Chemistry, University of Jaffna, 40000, Sri LankaBiotechnology Research Centre, BPE 73, Ali Mendjeli, Nouvelle Ville, 25000 Constantine, AlgeriaLaboratory of Science and Technology of the Environment, University Mentouri Constantine, Chaabat Errassas, Constantine, 25000, AlgeriaDepartment of Chemistry, University of South Dakota, Vermillion, SD 50679, USAThis study is aimed at developing a simple and low-cost method to fabricate ZnO-loaded porous activated carbon (AC-ZnO) prepared from the Algerian olive-waste cakes and utilize it as a photocatalyst for the degradation of Ethyl Violet dye. The synthesized AC-ZnO material was characterized using powder X-ray diffraction, BET surface area measurements, Raman microscopy, thermogravimetric analysis, UV-visible diffuse reflectance spectroscopy, and zeta potential measurements. The degradation efficiency was evaluated with Ethyl Violet (EV) dye in aqueous solution under UV irradiation supplied by a Xenon arc lamp through a Pyrex glass filter (cutoff 280 nm), and the degraded products were identified by using electrospray ionization mass spectroscopy. Additional experiments were carried out under N2 flow and with isopropyl alcohol to examine the role of superoxide and hydroxyl radicals, respectively. The amount of ●OH radical formed on irradiated AC-ZnO was tested with terephthalic acid which can act as a chemical trap for the ●OH radicals. The results from this study indicate that the AC-ZnO is a potential catalyst for the pollutant removal and the ●OH radicals are the key species for the degradation of EV. Further, this study opens up an opportunity to produce cheaper activated carbon support from olive wastes for environmental remediation applications.http://dx.doi.org/10.1155/2019/4714107
spellingShingle Ala Abdessemed
Shivatharsiny Rasalingam
Sanna Abdessemed
Kamel El Zin Djebbar
Ranjit Koodali
Impregnation of ZnO onto a Vegetal Activated Carbon from Algerian Olive Waste: A Sustainable Photocatalyst for Degradation of Ethyl Violet Dye
International Journal of Photoenergy
title Impregnation of ZnO onto a Vegetal Activated Carbon from Algerian Olive Waste: A Sustainable Photocatalyst for Degradation of Ethyl Violet Dye
title_full Impregnation of ZnO onto a Vegetal Activated Carbon from Algerian Olive Waste: A Sustainable Photocatalyst for Degradation of Ethyl Violet Dye
title_fullStr Impregnation of ZnO onto a Vegetal Activated Carbon from Algerian Olive Waste: A Sustainable Photocatalyst for Degradation of Ethyl Violet Dye
title_full_unstemmed Impregnation of ZnO onto a Vegetal Activated Carbon from Algerian Olive Waste: A Sustainable Photocatalyst for Degradation of Ethyl Violet Dye
title_short Impregnation of ZnO onto a Vegetal Activated Carbon from Algerian Olive Waste: A Sustainable Photocatalyst for Degradation of Ethyl Violet Dye
title_sort impregnation of zno onto a vegetal activated carbon from algerian olive waste a sustainable photocatalyst for degradation of ethyl violet dye
url http://dx.doi.org/10.1155/2019/4714107
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