Barleria extracts containing barlerin and verbascoside boost immunity and regulate CYP450 gene in prostate cancer

Abstract Barleria species have been traditionally utilized for medicinal purposes. This study provides a comprehensive analysis of six Barleria leaf extracts, namely B. cristata, B. lupulina, B. prionitis, B. repens, B. siamensis, and B. strigosa, to elucidate their metabolite composition, toxicity,...

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Main Authors: Sanit Kaewdaungdee, Zi Wei Sham, Hao Xuan Ho, Shiou Yih Lee, Tawatchai Tanee, Yannick D. Benoit, Thomas Liehr, Sakda Daduang, Runglawan Sudmoon, Arunrat Chaveerach
Format: Article
Language:English
Published: Nature Portfolio 2025-07-01
Series:Scientific Reports
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Online Access:https://doi.org/10.1038/s41598-025-07397-5
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author Sanit Kaewdaungdee
Zi Wei Sham
Hao Xuan Ho
Shiou Yih Lee
Tawatchai Tanee
Yannick D. Benoit
Thomas Liehr
Sakda Daduang
Runglawan Sudmoon
Arunrat Chaveerach
author_facet Sanit Kaewdaungdee
Zi Wei Sham
Hao Xuan Ho
Shiou Yih Lee
Tawatchai Tanee
Yannick D. Benoit
Thomas Liehr
Sakda Daduang
Runglawan Sudmoon
Arunrat Chaveerach
author_sort Sanit Kaewdaungdee
collection DOAJ
description Abstract Barleria species have been traditionally utilized for medicinal purposes. This study provides a comprehensive analysis of six Barleria leaf extracts, namely B. cristata, B. lupulina, B. prionitis, B. repens, B. siamensis, and B. strigosa, to elucidate their metabolite composition, toxicity, immunomodulatory functions, and roles in cytochrome P450 (CYP) gene expression. The findings indicate that two key metabolites, barlerin and verbascoside, are present in all six Barleria extracts, with B. siamensis exhibiting the highest amount of these compounds at 0.43 mg/g (barlerin) and 1.02 mg/g (verbascoside) of dried leaf, respectively. In terms of toxicological effects, B. cristata and B. siamensis demonstrated significant anti-proliferative activity against PC-3 cells by inducing DNA damage, enhancing apoptosis, and obstructing the cell cycle. However, these extracts did not exert cytotoxic effects on PBMCs, HPrEC, and THLE-3. Conversely, B. strigosa extract exhibited mild toxicity towards HPrECs and moderate toxicity towards THLE-3 cells. Furthermore, treatment with these extracts activated PBMCs, leading to the upregulation of cytokine genes, including IL-2, IL-10, IL-12, IL-15, IL-21, and IFN-γ, which promoted cytotoxicity for PC-3 cells. Additionally, B. siamensis extract significantly suppressed the expression of CYP450 genes, including CYP1A2, CYP3A4, CYP2D6, and CYP2E1, whereas B. strigosa extract induced the overexpression of CYP2E1. In conclusion, Barleria extracts containing barlerin and verbascoside exhibit immunomodulatory properties by activating immune cells to target cancer cells. Moreover, these extracts influence the expression of CYP450 genes, potentially impacting their bioavailability and therapeutic efficacy.
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spelling doaj-art-3618074befd64c889e9458a2c8a97f1e2025-08-20T04:01:34ZengNature PortfolioScientific Reports2045-23222025-07-0115111710.1038/s41598-025-07397-5Barleria extracts containing barlerin and verbascoside boost immunity and regulate CYP450 gene in prostate cancerSanit Kaewdaungdee0Zi Wei Sham1Hao Xuan Ho2Shiou Yih Lee3Tawatchai Tanee4Yannick D. Benoit5Thomas Liehr6Sakda Daduang7Runglawan Sudmoon8Arunrat Chaveerach9Department of Biology, Faculty of Science, Khon Kaen UniversityFaculty of Health and Life Sciences, INTI International UniversityFaculty of Health and Life Sciences, INTI International UniversityFaculty of Health and Life Sciences, INTI International UniversityFaculty of Environment and Resource Studies, Mahasarakham UniversityDepartment of Cellular and Molecular Medicine, Faculty of Medicine, University of OttawaInstitute of Human Genetics, Jena University HospitalDivision of Pharmacognosy and Toxicology, Faculty of Pharmaceutical Sciences, Khon Kaen UniversityFaculty of Law, Khon Kaen UniversityDepartment of Biology, Faculty of Science, Khon Kaen UniversityAbstract Barleria species have been traditionally utilized for medicinal purposes. This study provides a comprehensive analysis of six Barleria leaf extracts, namely B. cristata, B. lupulina, B. prionitis, B. repens, B. siamensis, and B. strigosa, to elucidate their metabolite composition, toxicity, immunomodulatory functions, and roles in cytochrome P450 (CYP) gene expression. The findings indicate that two key metabolites, barlerin and verbascoside, are present in all six Barleria extracts, with B. siamensis exhibiting the highest amount of these compounds at 0.43 mg/g (barlerin) and 1.02 mg/g (verbascoside) of dried leaf, respectively. In terms of toxicological effects, B. cristata and B. siamensis demonstrated significant anti-proliferative activity against PC-3 cells by inducing DNA damage, enhancing apoptosis, and obstructing the cell cycle. However, these extracts did not exert cytotoxic effects on PBMCs, HPrEC, and THLE-3. Conversely, B. strigosa extract exhibited mild toxicity towards HPrECs and moderate toxicity towards THLE-3 cells. Furthermore, treatment with these extracts activated PBMCs, leading to the upregulation of cytokine genes, including IL-2, IL-10, IL-12, IL-15, IL-21, and IFN-γ, which promoted cytotoxicity for PC-3 cells. Additionally, B. siamensis extract significantly suppressed the expression of CYP450 genes, including CYP1A2, CYP3A4, CYP2D6, and CYP2E1, whereas B. strigosa extract induced the overexpression of CYP2E1. In conclusion, Barleria extracts containing barlerin and verbascoside exhibit immunomodulatory properties by activating immune cells to target cancer cells. Moreover, these extracts influence the expression of CYP450 genes, potentially impacting their bioavailability and therapeutic efficacy.https://doi.org/10.1038/s41598-025-07397-5Anticancer activityBarleriaBarlerinCytochrome P450Immunomodulatory activityVerbascoside
spellingShingle Sanit Kaewdaungdee
Zi Wei Sham
Hao Xuan Ho
Shiou Yih Lee
Tawatchai Tanee
Yannick D. Benoit
Thomas Liehr
Sakda Daduang
Runglawan Sudmoon
Arunrat Chaveerach
Barleria extracts containing barlerin and verbascoside boost immunity and regulate CYP450 gene in prostate cancer
Scientific Reports
Anticancer activity
Barleria
Barlerin
Cytochrome P450
Immunomodulatory activity
Verbascoside
title Barleria extracts containing barlerin and verbascoside boost immunity and regulate CYP450 gene in prostate cancer
title_full Barleria extracts containing barlerin and verbascoside boost immunity and regulate CYP450 gene in prostate cancer
title_fullStr Barleria extracts containing barlerin and verbascoside boost immunity and regulate CYP450 gene in prostate cancer
title_full_unstemmed Barleria extracts containing barlerin and verbascoside boost immunity and regulate CYP450 gene in prostate cancer
title_short Barleria extracts containing barlerin and verbascoside boost immunity and regulate CYP450 gene in prostate cancer
title_sort barleria extracts containing barlerin and verbascoside boost immunity and regulate cyp450 gene in prostate cancer
topic Anticancer activity
Barleria
Barlerin
Cytochrome P450
Immunomodulatory activity
Verbascoside
url https://doi.org/10.1038/s41598-025-07397-5
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