Effect of hot press sintering parameters on microstructure and mechanical properties of Ti35421

The Ti‒3Al‒5Mo‒4Cr‒2Zr‒1Fe (Ti-35421, mass fraction) titanium alloys were prepared by hot pressing sintering in this paper. The influences of sintering temperature, sintering pressure, and holding time on the microstructure and mechanical properties of Ti-35421 alloys were explored by orthogonal exp...

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Main Authors: JIA Guorong, LU Leiyi, MIN Jin, CAO Xihao, GUO Yanhua, SUN Zhonggang, CHANG Hui
Format: Article
Language:zho
Published: Editorial Office of Powder Metallurgy Technology 2025-04-01
Series:Fenmo yejin jishu
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Online Access:https://pmt.ustb.edu.cn/article/doi/10.19591/j.cnki.cn11-1974/tf.2023120008
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author JIA Guorong
LU Leiyi
MIN Jin
CAO Xihao
GUO Yanhua
SUN Zhonggang
CHANG Hui
author_facet JIA Guorong
LU Leiyi
MIN Jin
CAO Xihao
GUO Yanhua
SUN Zhonggang
CHANG Hui
author_sort JIA Guorong
collection DOAJ
description The Ti‒3Al‒5Mo‒4Cr‒2Zr‒1Fe (Ti-35421, mass fraction) titanium alloys were prepared by hot pressing sintering in this paper. The influences of sintering temperature, sintering pressure, and holding time on the microstructure and mechanical properties of Ti-35421 alloys were explored by orthogonal experiments and characterized by relative density, secondary α phase dimension, hardness, and compression properties. The results show that the sintering temperature is the most important parameter affecting the properties of Ti-35421 alloys. As the sintering temperature increases, the yield strength first increases and then decreases, the fracture strain first decreases and then becomes stable. At the same time, the high sintering temperature causes the grain growth, which reduces the compressive properties of the Ti-35421 alloys. The optimal sintering parameters are followed as the temperature of 900 ℃, the sintering pressure of 45 MPa, and the sintering time of 2 h, and the corresponding yield strength and fracture strain of the Ti-35421 alloys reach 1248 MPa and 23.03%, respectively. The Ti-35421 alloys obtained by hot pressing sintering are mainly composed of the original β grains and secondary α phase within the grains. As the sintering temperature increases, the size of β grains in the sintered body increases significantly, and the aspect ratio of the secondary α phase also increases.
format Article
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institution OA Journals
issn 1001-3784
language zho
publishDate 2025-04-01
publisher Editorial Office of Powder Metallurgy Technology
record_format Article
series Fenmo yejin jishu
spelling doaj-art-36140e54560a4e00bd5ad4c0fde0ca222025-08-20T02:26:30ZzhoEditorial Office of Powder Metallurgy TechnologyFenmo yejin jishu1001-37842025-04-0143215316210.19591/j.cnki.cn11-1974/tf.2023120008Effect of hot press sintering parameters on microstructure and mechanical properties of Ti35421JIA Guorong0LU Leiyi1MIN Jin2CAO Xihao3GUO Yanhua4SUN Zhonggang5CHANG Hui6College of Materials Science and Engineering, Nanjing Tech University, Nanjing 210037, ChinaCollege of Materials Science and Engineering, Nanjing Tech University, Nanjing 210037, ChinaCollege of Materials Science and Engineering, Nanjing Tech University, Nanjing 210037, ChinaCollege of Materials Science and Engineering, Nanjing Tech University, Nanjing 210037, ChinaCollege of Materials Science and Engineering, Nanjing Tech University, Nanjing 210037, ChinaCollege of Materials Science and Engineering, Nanjing Tech University, Nanjing 210037, ChinaCollege of Materials Science and Engineering, Nanjing Tech University, Nanjing 210037, ChinaThe Ti‒3Al‒5Mo‒4Cr‒2Zr‒1Fe (Ti-35421, mass fraction) titanium alloys were prepared by hot pressing sintering in this paper. The influences of sintering temperature, sintering pressure, and holding time on the microstructure and mechanical properties of Ti-35421 alloys were explored by orthogonal experiments and characterized by relative density, secondary α phase dimension, hardness, and compression properties. The results show that the sintering temperature is the most important parameter affecting the properties of Ti-35421 alloys. As the sintering temperature increases, the yield strength first increases and then decreases, the fracture strain first decreases and then becomes stable. At the same time, the high sintering temperature causes the grain growth, which reduces the compressive properties of the Ti-35421 alloys. The optimal sintering parameters are followed as the temperature of 900 ℃, the sintering pressure of 45 MPa, and the sintering time of 2 h, and the corresponding yield strength and fracture strain of the Ti-35421 alloys reach 1248 MPa and 23.03%, respectively. The Ti-35421 alloys obtained by hot pressing sintering are mainly composed of the original β grains and secondary α phase within the grains. As the sintering temperature increases, the size of β grains in the sintered body increases significantly, and the aspect ratio of the secondary α phase also increases.https://pmt.ustb.edu.cn/article/doi/10.19591/j.cnki.cn11-1974/tf.2023120008titanium alloyspowder metallurgyhot pressing sinteringmicrostructuremechanical properties
spellingShingle JIA Guorong
LU Leiyi
MIN Jin
CAO Xihao
GUO Yanhua
SUN Zhonggang
CHANG Hui
Effect of hot press sintering parameters on microstructure and mechanical properties of Ti35421
Fenmo yejin jishu
titanium alloys
powder metallurgy
hot pressing sintering
microstructure
mechanical properties
title Effect of hot press sintering parameters on microstructure and mechanical properties of Ti35421
title_full Effect of hot press sintering parameters on microstructure and mechanical properties of Ti35421
title_fullStr Effect of hot press sintering parameters on microstructure and mechanical properties of Ti35421
title_full_unstemmed Effect of hot press sintering parameters on microstructure and mechanical properties of Ti35421
title_short Effect of hot press sintering parameters on microstructure and mechanical properties of Ti35421
title_sort effect of hot press sintering parameters on microstructure and mechanical properties of ti35421
topic titanium alloys
powder metallurgy
hot pressing sintering
microstructure
mechanical properties
url https://pmt.ustb.edu.cn/article/doi/10.19591/j.cnki.cn11-1974/tf.2023120008
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AT minjin effectofhotpresssinteringparametersonmicrostructureandmechanicalpropertiesofti35421
AT caoxihao effectofhotpresssinteringparametersonmicrostructureandmechanicalpropertiesofti35421
AT guoyanhua effectofhotpresssinteringparametersonmicrostructureandmechanicalpropertiesofti35421
AT sunzhonggang effectofhotpresssinteringparametersonmicrostructureandmechanicalpropertiesofti35421
AT changhui effectofhotpresssinteringparametersonmicrostructureandmechanicalpropertiesofti35421