Preparation, Rheological Behavior, and Redispersibility of Bamboo‐Derived Holocellulose Nanofibers

ABSTRACT With the demand for sustainable preparation of nanocellulose, the extraction of holocellulose nanofibers with surface‐coated hemicellulose from various biomass is drawing more and more attention. However, detailed preparation processes and some fundamental properties of holocellulose nanofi...

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Main Authors: Chong‐Han Yin, Xin‐Zhi Wang, Zi‐Meng Han, Huai‐Bin Yang, Kun‐Peng Yang, Wen‐Pei Zheng, Qing‐Fang Guan, Shu‐Hong Yu
Format: Article
Language:English
Published: Wiley 2025-04-01
Series:SmartMat
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Online Access:https://doi.org/10.1002/smm2.70001
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author Chong‐Han Yin
Xin‐Zhi Wang
Zi‐Meng Han
Huai‐Bin Yang
Kun‐Peng Yang
Wen‐Pei Zheng
Qing‐Fang Guan
Shu‐Hong Yu
author_facet Chong‐Han Yin
Xin‐Zhi Wang
Zi‐Meng Han
Huai‐Bin Yang
Kun‐Peng Yang
Wen‐Pei Zheng
Qing‐Fang Guan
Shu‐Hong Yu
author_sort Chong‐Han Yin
collection DOAJ
description ABSTRACT With the demand for sustainable preparation of nanocellulose, the extraction of holocellulose nanofibers with surface‐coated hemicellulose from various biomass is drawing more and more attention. However, detailed preparation processes and some fundamental properties of holocellulose nanofibers, such as rheological behavior and redispersibility, still need systematic investigation. An in‐depth understanding of these processes and properties plays a crucial role in guiding the preparation and subsequent material design of holocellulose nanofibers. Herein, a concise method is reported to prepare bamboo‐derived holocellulose nanofibers (BHCNFs) from bamboo residue and has been characterized in detail. To facilitate subsequent application, comprehensive exploration and understanding of the rheological behavior of BHCNF were conducted, along with an investigation into the redispersibility after freeze‐drying. The presence of hemicellulose significantly affects the rheological behavior and gives BHCNF a certain redispersibility. To achieve better redispersibility, aerogel powder was prepared via spray freeze‐drying, offering new insights into the drying and practical application of BHCNF.
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issn 2688-819X
language English
publishDate 2025-04-01
publisher Wiley
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series SmartMat
spelling doaj-art-35c8c69262e3485f9c4e1c99193566682025-08-20T02:20:12ZengWileySmartMat2688-819X2025-04-0162n/an/a10.1002/smm2.70001Preparation, Rheological Behavior, and Redispersibility of Bamboo‐Derived Holocellulose NanofibersChong‐Han Yin0Xin‐Zhi Wang1Zi‐Meng Han2Huai‐Bin Yang3Kun‐Peng Yang4Wen‐Pei Zheng5Qing‐Fang Guan6Shu‐Hong Yu7Department of Chemistry, New Cornerstone Science Laboratory, Institute of Biomimetic Materials & Chemistry, Anhui Engineering Laboratory of Biomimetic Materials, Division of Nanomaterials & Chemistry, Hefei National Research Center for Physical Sciences at the Microscale University of Science and Technology of China Hefei ChinaDepartment of Chemistry, New Cornerstone Science Laboratory, Institute of Biomimetic Materials & Chemistry, Anhui Engineering Laboratory of Biomimetic Materials, Division of Nanomaterials & Chemistry, Hefei National Research Center for Physical Sciences at the Microscale University of Science and Technology of China Hefei ChinaDepartment of Chemistry, New Cornerstone Science Laboratory, Institute of Biomimetic Materials & Chemistry, Anhui Engineering Laboratory of Biomimetic Materials, Division of Nanomaterials & Chemistry, Hefei National Research Center for Physical Sciences at the Microscale University of Science and Technology of China Hefei ChinaDepartment of Chemistry, New Cornerstone Science Laboratory, Institute of Biomimetic Materials & Chemistry, Anhui Engineering Laboratory of Biomimetic Materials, Division of Nanomaterials & Chemistry, Hefei National Research Center for Physical Sciences at the Microscale University of Science and Technology of China Hefei ChinaDepartment of Chemistry, New Cornerstone Science Laboratory, Institute of Biomimetic Materials & Chemistry, Anhui Engineering Laboratory of Biomimetic Materials, Division of Nanomaterials & Chemistry, Hefei National Research Center for Physical Sciences at the Microscale University of Science and Technology of China Hefei ChinaDepartment of Chemistry, New Cornerstone Science Laboratory, Institute of Biomimetic Materials & Chemistry, Anhui Engineering Laboratory of Biomimetic Materials, Division of Nanomaterials & Chemistry, Hefei National Research Center for Physical Sciences at the Microscale University of Science and Technology of China Hefei ChinaDepartment of Chemistry, New Cornerstone Science Laboratory, Institute of Biomimetic Materials & Chemistry, Anhui Engineering Laboratory of Biomimetic Materials, Division of Nanomaterials & Chemistry, Hefei National Research Center for Physical Sciences at the Microscale University of Science and Technology of China Hefei ChinaDepartment of Chemistry, New Cornerstone Science Laboratory, Institute of Biomimetic Materials & Chemistry, Anhui Engineering Laboratory of Biomimetic Materials, Division of Nanomaterials & Chemistry, Hefei National Research Center for Physical Sciences at the Microscale University of Science and Technology of China Hefei ChinaABSTRACT With the demand for sustainable preparation of nanocellulose, the extraction of holocellulose nanofibers with surface‐coated hemicellulose from various biomass is drawing more and more attention. However, detailed preparation processes and some fundamental properties of holocellulose nanofibers, such as rheological behavior and redispersibility, still need systematic investigation. An in‐depth understanding of these processes and properties plays a crucial role in guiding the preparation and subsequent material design of holocellulose nanofibers. Herein, a concise method is reported to prepare bamboo‐derived holocellulose nanofibers (BHCNFs) from bamboo residue and has been characterized in detail. To facilitate subsequent application, comprehensive exploration and understanding of the rheological behavior of BHCNF were conducted, along with an investigation into the redispersibility after freeze‐drying. The presence of hemicellulose significantly affects the rheological behavior and gives BHCNF a certain redispersibility. To achieve better redispersibility, aerogel powder was prepared via spray freeze‐drying, offering new insights into the drying and practical application of BHCNF.https://doi.org/10.1002/smm2.70001bamboo residuefreeze dryingholocellulose nanofiberredispersibilityrheological behavior
spellingShingle Chong‐Han Yin
Xin‐Zhi Wang
Zi‐Meng Han
Huai‐Bin Yang
Kun‐Peng Yang
Wen‐Pei Zheng
Qing‐Fang Guan
Shu‐Hong Yu
Preparation, Rheological Behavior, and Redispersibility of Bamboo‐Derived Holocellulose Nanofibers
SmartMat
bamboo residue
freeze drying
holocellulose nanofiber
redispersibility
rheological behavior
title Preparation, Rheological Behavior, and Redispersibility of Bamboo‐Derived Holocellulose Nanofibers
title_full Preparation, Rheological Behavior, and Redispersibility of Bamboo‐Derived Holocellulose Nanofibers
title_fullStr Preparation, Rheological Behavior, and Redispersibility of Bamboo‐Derived Holocellulose Nanofibers
title_full_unstemmed Preparation, Rheological Behavior, and Redispersibility of Bamboo‐Derived Holocellulose Nanofibers
title_short Preparation, Rheological Behavior, and Redispersibility of Bamboo‐Derived Holocellulose Nanofibers
title_sort preparation rheological behavior and redispersibility of bamboo derived holocellulose nanofibers
topic bamboo residue
freeze drying
holocellulose nanofiber
redispersibility
rheological behavior
url https://doi.org/10.1002/smm2.70001
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