A lanthanide MOF with nanostructured node disorder

Abstract Structural disorder can be used to tune the properties of functional materials and is an important tool that can be employed for the development of complex framework materials, such as metal-organic frameworks. Here we show the synthesis and structural characterization of a metal-organic fr...

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Main Authors: Sarah L. Griffin, Emily G. Meekel, Johnathan M. Bulled, Stefano Canossa, Alexander Wahrhaftig-Lewis, Ella M. Schmidt, Neil R. Champness
Format: Article
Language:English
Published: Nature Portfolio 2025-04-01
Series:Nature Communications
Online Access:https://doi.org/10.1038/s41467-025-58402-4
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author Sarah L. Griffin
Emily G. Meekel
Johnathan M. Bulled
Stefano Canossa
Alexander Wahrhaftig-Lewis
Ella M. Schmidt
Neil R. Champness
author_facet Sarah L. Griffin
Emily G. Meekel
Johnathan M. Bulled
Stefano Canossa
Alexander Wahrhaftig-Lewis
Ella M. Schmidt
Neil R. Champness
author_sort Sarah L. Griffin
collection DOAJ
description Abstract Structural disorder can be used to tune the properties of functional materials and is an important tool that can be employed for the development of complex framework materials, such as metal-organic frameworks. Here we show the synthesis and structural characterization of a metal-organic framework, UoB-100(Dy). Average structure refinements indicate that the node is disordered between two orientations of the nonanuclear secondary building unit (SBU). By performing 3D diffuse scattering (DS) analysis and Monte Carlo (MC) simulations, we confirm the presence of strong correlations between the metal clusters of UoB-100(Dy). These nodes assemble into a complex nanodomain structure. Quantum mechanical calculations identify linker strain as the driving force behind the nanodomain structure. The implications of such a nanodomain structure for the magnetic, gas storage, and mechanical properties of lanthanide MOFs are discussed.
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spelling doaj-art-35b16d9bf3d74129b2dcac1ac8371ad72025-08-20T01:54:22ZengNature PortfolioNature Communications2041-17232025-04-011611910.1038/s41467-025-58402-4A lanthanide MOF with nanostructured node disorderSarah L. Griffin0Emily G. Meekel1Johnathan M. Bulled2Stefano Canossa3Alexander Wahrhaftig-Lewis4Ella M. Schmidt5Neil R. Champness6School of Chemistry, University of BirminghamInstitute for Integrated Cell-Material Sciences (WPI-iCeMS), Kyoto UniversityESRFETH Zürich, Anorganische FunktionsmaterialienSchool of Chemistry, University of BirminghamFaculty of Geosciences, MARUM and MAPEX, University of BremenSchool of Chemistry, University of BirminghamAbstract Structural disorder can be used to tune the properties of functional materials and is an important tool that can be employed for the development of complex framework materials, such as metal-organic frameworks. Here we show the synthesis and structural characterization of a metal-organic framework, UoB-100(Dy). Average structure refinements indicate that the node is disordered between two orientations of the nonanuclear secondary building unit (SBU). By performing 3D diffuse scattering (DS) analysis and Monte Carlo (MC) simulations, we confirm the presence of strong correlations between the metal clusters of UoB-100(Dy). These nodes assemble into a complex nanodomain structure. Quantum mechanical calculations identify linker strain as the driving force behind the nanodomain structure. The implications of such a nanodomain structure for the magnetic, gas storage, and mechanical properties of lanthanide MOFs are discussed.https://doi.org/10.1038/s41467-025-58402-4
spellingShingle Sarah L. Griffin
Emily G. Meekel
Johnathan M. Bulled
Stefano Canossa
Alexander Wahrhaftig-Lewis
Ella M. Schmidt
Neil R. Champness
A lanthanide MOF with nanostructured node disorder
Nature Communications
title A lanthanide MOF with nanostructured node disorder
title_full A lanthanide MOF with nanostructured node disorder
title_fullStr A lanthanide MOF with nanostructured node disorder
title_full_unstemmed A lanthanide MOF with nanostructured node disorder
title_short A lanthanide MOF with nanostructured node disorder
title_sort lanthanide mof with nanostructured node disorder
url https://doi.org/10.1038/s41467-025-58402-4
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