Development of Spectrophotometric method for quantitative determination of dexamethasone in pharmaceutical preparations

This Study is concerned a fast, easy, sensitive, accurate and economical spectrophotometric method for the determination of Dexamethasone. This method based on the use of UV- spectra measurements at 242 nm.  The linearity of the method is performed between (3 - 65) μg.ml-1, the  coefficient of ...

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Main Authors: Rafal Abdulraheem Abdullah, Khalaf F. AL-Samarraee
Format: Article
Language:English
Published: Tikrit University 2023-01-01
Series:Tikrit Journal of Pure Science
Subjects:
Online Access:https://tjpsj.org/index.php/tjps/article/view/777
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author Rafal Abdulraheem Abdullah
Khalaf F. AL-Samarraee
author_facet Rafal Abdulraheem Abdullah
Khalaf F. AL-Samarraee
author_sort Rafal Abdulraheem Abdullah
collection DOAJ
description This Study is concerned a fast, easy, sensitive, accurate and economical spectrophotometric method for the determination of Dexamethasone. This method based on the use of UV- spectra measurements at 242 nm.  The linearity of the method is performed between (3 - 65) μg.ml-1, the  coefficient of  correlation was = 0.9998. The value of Rec% and RSD% are found at the range (95.28 -102.86)% and (0 - 0.272 )% respectively, The LOD and LOQ were (0.024and 0.081) μg.ml-1, respectively . The method was successfully applied to the determination of DMT in Bulk and pharmaceutical preparations
format Article
id doaj-art-35b0b0d410ad49f2aa0ac5b1b730e8dd
institution DOAJ
issn 1813-1662
2415-1726
language English
publishDate 2023-01-01
publisher Tikrit University
record_format Article
series Tikrit Journal of Pure Science
spelling doaj-art-35b0b0d410ad49f2aa0ac5b1b730e8dd2025-08-20T03:16:51ZengTikrit UniversityTikrit Journal of Pure Science1813-16622415-17262023-01-0122510.25130/tjps.v22i5.777Development of Spectrophotometric method for quantitative determination of dexamethasone in pharmaceutical preparationsRafal Abdulraheem AbdullahKhalaf F. AL-Samarraee This Study is concerned a fast, easy, sensitive, accurate and economical spectrophotometric method for the determination of Dexamethasone. This method based on the use of UV- spectra measurements at 242 nm.  The linearity of the method is performed between (3 - 65) μg.ml-1, the  coefficient of  correlation was = 0.9998. The value of Rec% and RSD% are found at the range (95.28 -102.86)% and (0 - 0.272 )% respectively, The LOD and LOQ were (0.024and 0.081) μg.ml-1, respectively . The method was successfully applied to the determination of DMT in Bulk and pharmaceutical preparations https://tjpsj.org/index.php/tjps/article/view/777Spectrophotometric methoddexamethasonepharmaceutical preparations
spellingShingle Rafal Abdulraheem Abdullah
Khalaf F. AL-Samarraee
Development of Spectrophotometric method for quantitative determination of dexamethasone in pharmaceutical preparations
Tikrit Journal of Pure Science
Spectrophotometric method
dexamethasone
pharmaceutical preparations
title Development of Spectrophotometric method for quantitative determination of dexamethasone in pharmaceutical preparations
title_full Development of Spectrophotometric method for quantitative determination of dexamethasone in pharmaceutical preparations
title_fullStr Development of Spectrophotometric method for quantitative determination of dexamethasone in pharmaceutical preparations
title_full_unstemmed Development of Spectrophotometric method for quantitative determination of dexamethasone in pharmaceutical preparations
title_short Development of Spectrophotometric method for quantitative determination of dexamethasone in pharmaceutical preparations
title_sort development of spectrophotometric method for quantitative determination of dexamethasone in pharmaceutical preparations
topic Spectrophotometric method
dexamethasone
pharmaceutical preparations
url https://tjpsj.org/index.php/tjps/article/view/777
work_keys_str_mv AT rafalabdulraheemabdullah developmentofspectrophotometricmethodforquantitativedeterminationofdexamethasoneinpharmaceuticalpreparations
AT khalaffalsamarraee developmentofspectrophotometricmethodforquantitativedeterminationofdexamethasoneinpharmaceuticalpreparations