Micro-nanojauges design to monitor surface mechanical state during high temperature oxidation of metals with application to 17-4PH stainless steel
Determination of mechanical state of thermal oxide growing during high temperature oxidation is a challenge. Fabrication of nanogauges for monitoring during high temperature oxidation was presently investigated up to 1000 °C. Several materials were tested in terms of mechanical behaviour and maximum...
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Elsevier
2024-10-01
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| Series: | Materials & Design |
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| Online Access: | http://www.sciencedirect.com/science/article/pii/S0264127524007160 |
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| author | Abdelhamid Hmima Malak Kheir Al Din Claire Gong Benoit Panicaud Akram Alhussein Guillaume Geandier Florimonde Lebel Jean-Luc Grosseau-Poussard Joseph Marae Djouda Thomas Maurer Hind Kadiri |
| author_facet | Abdelhamid Hmima Malak Kheir Al Din Claire Gong Benoit Panicaud Akram Alhussein Guillaume Geandier Florimonde Lebel Jean-Luc Grosseau-Poussard Joseph Marae Djouda Thomas Maurer Hind Kadiri |
| author_sort | Abdelhamid Hmima |
| collection | DOAJ |
| description | Determination of mechanical state of thermal oxide growing during high temperature oxidation is a challenge. Fabrication of nanogauges for monitoring during high temperature oxidation was presently investigated up to 1000 °C. Several materials were tested in terms of mechanical behaviour and maximum working temperature for gauges used as markers during thermal loading under air. The experimental determination of the optimized gauges material for high temperature oxidation was validated. SiO2 offers particularly interesting features for gauges to determine the mechanical state of metal/oxide system. In this article, a special attention has also been paid to two nano-fabrication processes, as well as their limits. The standard electron beam lithography process is well suited to build gauges for oxidation applications, and can be improved by use of reactive ion etching process. The gauges can eventually reach several micrometers height such that the oxidation layer does not cover the gauges during thermal loading for relevant monitoring at short oxidation times. To illustrate, an application to a 17-4PH stainless steel oxidized at 480 °C is proposed and stress kinetics are deduced and related to an advanced thermomechano-chemical model, as well as identification of the numerical values of different thermomechano-chemical parameters associated to mechanisms of growth or relaxation. |
| format | Article |
| id | doaj-art-3470aed6800a45819a17e6d997f8657d |
| institution | OA Journals |
| issn | 0264-1275 |
| language | English |
| publishDate | 2024-10-01 |
| publisher | Elsevier |
| record_format | Article |
| series | Materials & Design |
| spelling | doaj-art-3470aed6800a45819a17e6d997f8657d2025-08-20T01:54:15ZengElsevierMaterials & Design0264-12752024-10-0124611334110.1016/j.matdes.2024.113341Micro-nanojauges design to monitor surface mechanical state during high temperature oxidation of metals with application to 17-4PH stainless steelAbdelhamid Hmima0Malak Kheir Al Din1Claire Gong2Benoit Panicaud3Akram Alhussein4Guillaume Geandier5Florimonde Lebel6Jean-Luc Grosseau-Poussard7Joseph Marae Djouda8Thomas Maurer9Hind Kadiri10Light, Nanomaterials, Nanotechnologies (L2n) CNRS EMR 7004, UTT, 12 rue Marie Curie 10000, Troyes, FranceLife Assessment of Structures, Materials, Mechanics and Integrated Systems (LASMIS), UTT, 12 rue Marie Curie 10000, Troyes, FranceLight, Nanomaterials, Nanotechnologies (L2n) CNRS EMR 7004, UTT, 12 rue Marie Curie 10000, Troyes, FranceLife Assessment of Structures, Materials, Mechanics and Integrated Systems (LASMIS), UTT, 12 rue Marie Curie 10000, Troyes, France; Corresponding author.Life Assessment of Structures, Materials, Mechanics and Integrated Systems (LASMIS), UTT, Pôle Technologique Sud Champagne, 26 Rue Lavoisier 52800, Nogent, FranceInstitut Jean Lamour, Université de Lorraine, CNRS, IJL, F-54000, Nancy, FranceInstitut Jean Lamour, Université de Lorraine, CNRS, IJL, F-54000, Nancy, FranceLaboratoire des Sciences de l’Ingénieur pour l’Environnement (LaSIE), CNRS UMR 7356, Université de La Rochelle, Avenue Michel Crépeau 17042, La Rochelle Cedex 1, FranceEPF, Ecole d’ingénieurs, 3 bis rue Lakanal 92 330, Sceaux, FranceLight, Nanomaterials, Nanotechnologies (L2n) CNRS EMR 7004, UTT, 12 rue Marie Curie 10000, Troyes, FranceLight, Nanomaterials, Nanotechnologies (L2n) CNRS EMR 7004, UTT, 12 rue Marie Curie 10000, Troyes, FranceDetermination of mechanical state of thermal oxide growing during high temperature oxidation is a challenge. Fabrication of nanogauges for monitoring during high temperature oxidation was presently investigated up to 1000 °C. Several materials were tested in terms of mechanical behaviour and maximum working temperature for gauges used as markers during thermal loading under air. The experimental determination of the optimized gauges material for high temperature oxidation was validated. SiO2 offers particularly interesting features for gauges to determine the mechanical state of metal/oxide system. In this article, a special attention has also been paid to two nano-fabrication processes, as well as their limits. The standard electron beam lithography process is well suited to build gauges for oxidation applications, and can be improved by use of reactive ion etching process. The gauges can eventually reach several micrometers height such that the oxidation layer does not cover the gauges during thermal loading for relevant monitoring at short oxidation times. To illustrate, an application to a 17-4PH stainless steel oxidized at 480 °C is proposed and stress kinetics are deduced and related to an advanced thermomechano-chemical model, as well as identification of the numerical values of different thermomechano-chemical parameters associated to mechanisms of growth or relaxation.http://www.sciencedirect.com/science/article/pii/S0264127524007160Short oxidation timeHigh-temperature oxidationElectron beam lithography processNanogaugesStress determinationStainless steel |
| spellingShingle | Abdelhamid Hmima Malak Kheir Al Din Claire Gong Benoit Panicaud Akram Alhussein Guillaume Geandier Florimonde Lebel Jean-Luc Grosseau-Poussard Joseph Marae Djouda Thomas Maurer Hind Kadiri Micro-nanojauges design to monitor surface mechanical state during high temperature oxidation of metals with application to 17-4PH stainless steel Materials & Design Short oxidation time High-temperature oxidation Electron beam lithography process Nanogauges Stress determination Stainless steel |
| title | Micro-nanojauges design to monitor surface mechanical state during high temperature oxidation of metals with application to 17-4PH stainless steel |
| title_full | Micro-nanojauges design to monitor surface mechanical state during high temperature oxidation of metals with application to 17-4PH stainless steel |
| title_fullStr | Micro-nanojauges design to monitor surface mechanical state during high temperature oxidation of metals with application to 17-4PH stainless steel |
| title_full_unstemmed | Micro-nanojauges design to monitor surface mechanical state during high temperature oxidation of metals with application to 17-4PH stainless steel |
| title_short | Micro-nanojauges design to monitor surface mechanical state during high temperature oxidation of metals with application to 17-4PH stainless steel |
| title_sort | micro nanojauges design to monitor surface mechanical state during high temperature oxidation of metals with application to 17 4ph stainless steel |
| topic | Short oxidation time High-temperature oxidation Electron beam lithography process Nanogauges Stress determination Stainless steel |
| url | http://www.sciencedirect.com/science/article/pii/S0264127524007160 |
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