Heat protective coatings on niobium alloys

The article shows that during plasma-diffusion deposition, a multilayer coating was formed on the surface of the niobium alloy. A highly porous plasma-sprayed layer of molybdenum silicide has a significant spread in thickness (h=100...350 μm, Hμ20=6880 MPa). When studying the microstructure of sampl...

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Main Authors: Vitaliy Babak, Boris Lyashenko, Vitaliy Shchepetov, Sergei Kharchenko
Format: Article
Language:English
Published: National Technical University of Ukraine "Igor Sikorsky Kyiv Polytechnic Institute" 2020-12-01
Series:Mechanics and Advanced Technologies
Subjects:
Online Access:http://journal.mmi.kpi.ua/article/view/219550
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author Vitaliy Babak
Boris Lyashenko
Vitaliy Shchepetov
Sergei Kharchenko
author_facet Vitaliy Babak
Boris Lyashenko
Vitaliy Shchepetov
Sergei Kharchenko
author_sort Vitaliy Babak
collection DOAJ
description The article shows that during plasma-diffusion deposition, a multilayer coating was formed on the surface of the niobium alloy. A highly porous plasma-sprayed layer of molybdenum silicide has a significant spread in thickness (h=100...350 μm, Hμ20=6880 MPa). When studying the microstructure of samples with a plasma-diffusion coating after testing, it was found that cracks in the coating originate in the process of creep, mostly at the interface between the plasma and diffusion layers of the coating. The source of their origin is individual discontinuities in the diffusion layer as delivered. Crack propagation occurs both into the plasma and diffusion layers of the coating. Crack growth in the plasma layer is inhibited due to the rounded nature of the pores and the increased plasticity of this layer. The growth of cracks deep into the sample is, as a rule, inhibited by a boride sublayer. The advantage of plasma-diffusion technology provided an increased plasticity of the coating, the presence of thin barrier sublayers, a discontinuous coating structure, the presence of low-melting compounds that contribute to the healing of defects in the coating, an increase in its corrosion resistance and resistance to thermal fatigue destruction. The combination of these properties made it possible to provide an increase in durability compared to silicide and borosilicide coatings under conditions of isothermal creep in air (1400°C, 50 MPa) 1.9...3.7 times and under conditions of thermal cyclic creep (1400-250°C, 50 MPa) in 6.8...8.5 times. It has been determined that the use of a discrete structure will increase the thickness of the coating layer and ensure an increase in their working properties.
format Article
id doaj-art-32533de7a41d4fcbb18e82d54e25c626
institution DOAJ
issn 2521-1943
2522-4255
language English
publishDate 2020-12-01
publisher National Technical University of Ukraine "Igor Sikorsky Kyiv Polytechnic Institute"
record_format Article
series Mechanics and Advanced Technologies
spelling doaj-art-32533de7a41d4fcbb18e82d54e25c6262025-08-20T03:15:42ZengNational Technical University of Ukraine "Igor Sikorsky Kyiv Polytechnic Institute"Mechanics and Advanced Technologies2521-19432522-42552020-12-013(90)10.20535/2521-1943.2020.0.219550Heat protective coatings on niobium alloysVitaliy Babak0Boris Lyashenko1Vitaliy Shchepetov2Sergei Kharchenko3Institute of Engineering Thermophysics of the National Academy of Sciences of UkraineG.S. Pisarenko Institute for Problems of Strength of the National Academy of Sciences of UkraineInstitute of Engineering Thermophysics of the National Academy of Sciences of UkraineInstitute of Engineering Thermophysics of the National Academy of Sciences of UkraineThe article shows that during plasma-diffusion deposition, a multilayer coating was formed on the surface of the niobium alloy. A highly porous plasma-sprayed layer of molybdenum silicide has a significant spread in thickness (h=100...350 μm, Hμ20=6880 MPa). When studying the microstructure of samples with a plasma-diffusion coating after testing, it was found that cracks in the coating originate in the process of creep, mostly at the interface between the plasma and diffusion layers of the coating. The source of their origin is individual discontinuities in the diffusion layer as delivered. Crack propagation occurs both into the plasma and diffusion layers of the coating. Crack growth in the plasma layer is inhibited due to the rounded nature of the pores and the increased plasticity of this layer. The growth of cracks deep into the sample is, as a rule, inhibited by a boride sublayer. The advantage of plasma-diffusion technology provided an increased plasticity of the coating, the presence of thin barrier sublayers, a discontinuous coating structure, the presence of low-melting compounds that contribute to the healing of defects in the coating, an increase in its corrosion resistance and resistance to thermal fatigue destruction. The combination of these properties made it possible to provide an increase in durability compared to silicide and borosilicide coatings under conditions of isothermal creep in air (1400°C, 50 MPa) 1.9...3.7 times and under conditions of thermal cyclic creep (1400-250°C, 50 MPa) in 6.8...8.5 times. It has been determined that the use of a discrete structure will increase the thickness of the coating layer and ensure an increase in their working properties.http://journal.mmi.kpi.ua/article/view/219550alloymulticomponent coatingsplasma-diffusion coatingsheat strengthheat resistance
spellingShingle Vitaliy Babak
Boris Lyashenko
Vitaliy Shchepetov
Sergei Kharchenko
Heat protective coatings on niobium alloys
Mechanics and Advanced Technologies
alloy
multicomponent coatings
plasma-diffusion coatings
heat strength
heat resistance
title Heat protective coatings on niobium alloys
title_full Heat protective coatings on niobium alloys
title_fullStr Heat protective coatings on niobium alloys
title_full_unstemmed Heat protective coatings on niobium alloys
title_short Heat protective coatings on niobium alloys
title_sort heat protective coatings on niobium alloys
topic alloy
multicomponent coatings
plasma-diffusion coatings
heat strength
heat resistance
url http://journal.mmi.kpi.ua/article/view/219550
work_keys_str_mv AT vitaliybabak heatprotectivecoatingsonniobiumalloys
AT borislyashenko heatprotectivecoatingsonniobiumalloys
AT vitaliyshchepetov heatprotectivecoatingsonniobiumalloys
AT sergeikharchenko heatprotectivecoatingsonniobiumalloys