ZINC OXIDE - SINTERED CALCIUM PHOSPHATE CATALYZED GREEN SYNTHESIS OF ESTERS AND AMIDES

Herein, the application of zinc oxide supported on sintered calcium phosphate (SCaP) as a catalyst in acylation reaction is described. This catalyst was found to be highly effective in solvent free acylation of various phenols, alcohols and amines. Reaction at room temperature, with very less qu...

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Main Authors: S. Sumathi, B.R. Saikishore Kumar
Format: Article
Language:English
Published: Alma Mater Publishing House "Vasile Alecsandri" University of Bacau 2020-06-01
Series:Scientific Study & Research: Chemistry & Chemical Engineering, Biotechnology, Food Industry
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Online Access:http://pubs.ub.ro/?pg=revues&rev=cscc6&num=202002&vol=2&aid=5105
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author S. Sumathi
B.R. Saikishore Kumar
author_facet S. Sumathi
B.R. Saikishore Kumar
author_sort S. Sumathi
collection DOAJ
description Herein, the application of zinc oxide supported on sintered calcium phosphate (SCaP) as a catalyst in acylation reaction is described. This catalyst was found to be highly effective in solvent free acylation of various phenols, alcohols and amines. Reaction at room temperature, with very less quantity of the catalyst, high yield in shorter reaction time, easy separation of the catalyst and isolation of the desired product in good purity are the merits of this reaction. In addition, the recovered catalyst could be reused for four successive runs without significant deterioration in catalytic activity.
format Article
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institution OA Journals
issn 1582-540X
1582-540X
language English
publishDate 2020-06-01
publisher Alma Mater Publishing House "Vasile Alecsandri" University of Bacau
record_format Article
series Scientific Study & Research: Chemistry & Chemical Engineering, Biotechnology, Food Industry
spelling doaj-art-31640ae0680c4dfbbe16db37b2c94e7a2025-08-20T02:38:53ZengAlma Mater Publishing House "Vasile Alecsandri" University of BacauScientific Study & Research: Chemistry & Chemical Engineering, Biotechnology, Food Industry1582-540X1582-540X2020-06-01212207216ZINC OXIDE - SINTERED CALCIUM PHOSPHATE CATALYZED GREEN SYNTHESIS OF ESTERS AND AMIDESS. Sumathi0 B.R. Saikishore Kumar1Hindustan Institute of Technology & Science, Department of Chemistry, Padur, Chennai 603 103, India ATGC Biotech Private Limited, Kompally, Hyderabad, Telengana 500014, India Herein, the application of zinc oxide supported on sintered calcium phosphate (SCaP) as a catalyst in acylation reaction is described. This catalyst was found to be highly effective in solvent free acylation of various phenols, alcohols and amines. Reaction at room temperature, with very less quantity of the catalyst, high yield in shorter reaction time, easy separation of the catalyst and isolation of the desired product in good purity are the merits of this reaction. In addition, the recovered catalyst could be reused for four successive runs without significant deterioration in catalytic activity.http://pubs.ub.ro/?pg=revues&rev=cscc6&num=202002&vol=2&aid=5105acylationalcoholsaminescalcium phosphatecatalystphenolszinc oxide
spellingShingle S. Sumathi
B.R. Saikishore Kumar
ZINC OXIDE - SINTERED CALCIUM PHOSPHATE CATALYZED GREEN SYNTHESIS OF ESTERS AND AMIDES
Scientific Study & Research: Chemistry & Chemical Engineering, Biotechnology, Food Industry
acylation
alcohols
amines
calcium phosphate
catalyst
phenols
zinc oxide
title ZINC OXIDE - SINTERED CALCIUM PHOSPHATE CATALYZED GREEN SYNTHESIS OF ESTERS AND AMIDES
title_full ZINC OXIDE - SINTERED CALCIUM PHOSPHATE CATALYZED GREEN SYNTHESIS OF ESTERS AND AMIDES
title_fullStr ZINC OXIDE - SINTERED CALCIUM PHOSPHATE CATALYZED GREEN SYNTHESIS OF ESTERS AND AMIDES
title_full_unstemmed ZINC OXIDE - SINTERED CALCIUM PHOSPHATE CATALYZED GREEN SYNTHESIS OF ESTERS AND AMIDES
title_short ZINC OXIDE - SINTERED CALCIUM PHOSPHATE CATALYZED GREEN SYNTHESIS OF ESTERS AND AMIDES
title_sort zinc oxide sintered calcium phosphate catalyzed green synthesis of esters and amides
topic acylation
alcohols
amines
calcium phosphate
catalyst
phenols
zinc oxide
url http://pubs.ub.ro/?pg=revues&rev=cscc6&num=202002&vol=2&aid=5105
work_keys_str_mv AT ssumathi zincoxidesinteredcalciumphosphatecatalyzedgreensynthesisofestersandamides
AT brsaikishorekumar zincoxidesinteredcalciumphosphatecatalyzedgreensynthesisofestersandamides