Synthesis and Characterization of 1,2,3- Triazole Derivatives from D-Mannitol
This research included the use of azido D-Mannitol (3) to synthesize 1,2,3 triazole derivatives. Azido D – Mannitol (3) itself used as an intermediate which was prepared from reaction of 1, 2:5, 6-Di-o-isopropylidene-3,4-di-p-tosyl-D-Mannitol (2) with sodium azide. The prepared compound (3) was a...
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| Language: | English |
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Tikrit University
2023-02-01
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| Series: | Tikrit Journal of Pure Science |
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| Online Access: | https://tjpsj.org/index.php/tjps/article/view/876 |
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| author | Ihmood Kh. Juber |
| author_facet | Ihmood Kh. Juber |
| author_sort | Ihmood Kh. Juber |
| collection | DOAJ |
| description |
This research included the use of azido D-Mannitol (3) to synthesize 1,2,3 triazole derivatives. Azido D – Mannitol (3) itself used as an intermediate which was prepared from reaction of 1, 2:5, 6-Di-o-isopropylidene-3,4-di-p-tosyl-D-Mannitol (2) with sodium azide. The prepared compound (3) was allowed to react with alkenes for the formation of corresponding 1,2,3 triazole (4a-e ).
The structures of some prepared compounds were confirmed by physical properties and spectroscopic methods FT-IR , 1H-NMR , 13C-NMR and Mass spectra in addition to use TLC.
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| format | Article |
| id | doaj-art-30fa6db400ed4b5291eea338190e3974 |
| institution | OA Journals |
| issn | 1813-1662 2415-1726 |
| language | English |
| publishDate | 2023-02-01 |
| publisher | Tikrit University |
| record_format | Article |
| series | Tikrit Journal of Pure Science |
| spelling | doaj-art-30fa6db400ed4b5291eea338190e39742025-08-20T02:36:31ZengTikrit UniversityTikrit Journal of Pure Science1813-16622415-17262023-02-0122910.25130/tjps.v22i9.876Synthesis and Characterization of 1,2,3- Triazole Derivatives from D-MannitolIhmood Kh. Juber This research included the use of azido D-Mannitol (3) to synthesize 1,2,3 triazole derivatives. Azido D – Mannitol (3) itself used as an intermediate which was prepared from reaction of 1, 2:5, 6-Di-o-isopropylidene-3,4-di-p-tosyl-D-Mannitol (2) with sodium azide. The prepared compound (3) was allowed to react with alkenes for the formation of corresponding 1,2,3 triazole (4a-e ). The structures of some prepared compounds were confirmed by physical properties and spectroscopic methods FT-IR , 1H-NMR , 13C-NMR and Mass spectra in addition to use TLC. https://tjpsj.org/index.php/tjps/article/view/876D-Mannitol1,2,3-triazoleazideisopropylidene |
| spellingShingle | Ihmood Kh. Juber Synthesis and Characterization of 1,2,3- Triazole Derivatives from D-Mannitol Tikrit Journal of Pure Science D-Mannitol 1,2,3-triazole azide isopropylidene |
| title | Synthesis and Characterization of 1,2,3- Triazole Derivatives from D-Mannitol |
| title_full | Synthesis and Characterization of 1,2,3- Triazole Derivatives from D-Mannitol |
| title_fullStr | Synthesis and Characterization of 1,2,3- Triazole Derivatives from D-Mannitol |
| title_full_unstemmed | Synthesis and Characterization of 1,2,3- Triazole Derivatives from D-Mannitol |
| title_short | Synthesis and Characterization of 1,2,3- Triazole Derivatives from D-Mannitol |
| title_sort | synthesis and characterization of 1 2 3 triazole derivatives from d mannitol |
| topic | D-Mannitol 1,2,3-triazole azide isopropylidene |
| url | https://tjpsj.org/index.php/tjps/article/view/876 |
| work_keys_str_mv | AT ihmoodkhjuber synthesisandcharacterizationof123triazolederivativesfromdmannitol |