Transformation of 3D Metal–Organic Frameworks into Nanosheets with Enhanced Memristive Behavior for Electronic Data Processing

Abstract The transition from three‐dimensional (3D) to two‐dimensional (2D) semiconducting and insulating materials for micro‐ and opto‐electronics is driven by an energy efficiency and device miniaturization. Herein, the simplicity of growth and stacking of 2D metal–organic framework (MOF) with suc...

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Main Authors: Yuri A. Mezenov, Semyon V. Bachinin, Yuliya A. Kenzhebayeva, Anastasiia S. Efimova, Pavel V. Alekseevskiy, Daria Poloneeva, Anastasia Lubimova, Svyatoslav A. Povarov, Vladimir Shirobokov, Mikhail S. Dunaevskiy, Aleksandra S. Falchevskaya, Andrei S. Potapov, Alexander Novikov, Artem A. Selyutin, Pascal Boulet, Alena N. Kulakova, Valentin A. Milichko
Format: Article
Language:English
Published: Wiley 2025-04-01
Series:Advanced Science
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Online Access:https://doi.org/10.1002/advs.202405989
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author Yuri A. Mezenov
Semyon V. Bachinin
Yuliya A. Kenzhebayeva
Anastasiia S. Efimova
Pavel V. Alekseevskiy
Daria Poloneeva
Anastasia Lubimova
Svyatoslav A. Povarov
Vladimir Shirobokov
Mikhail S. Dunaevskiy
Aleksandra S. Falchevskaya
Andrei S. Potapov
Alexander Novikov
Artem A. Selyutin
Pascal Boulet
Alena N. Kulakova
Valentin A. Milichko
author_facet Yuri A. Mezenov
Semyon V. Bachinin
Yuliya A. Kenzhebayeva
Anastasiia S. Efimova
Pavel V. Alekseevskiy
Daria Poloneeva
Anastasia Lubimova
Svyatoslav A. Povarov
Vladimir Shirobokov
Mikhail S. Dunaevskiy
Aleksandra S. Falchevskaya
Andrei S. Potapov
Alexander Novikov
Artem A. Selyutin
Pascal Boulet
Alena N. Kulakova
Valentin A. Milichko
author_sort Yuri A. Mezenov
collection DOAJ
description Abstract The transition from three‐dimensional (3D) to two‐dimensional (2D) semiconducting and insulating materials for micro‐ and opto‐electronics is driven by an energy efficiency and device miniaturization. Herein, the simplicity of growth and stacking of 2D metal–organic framework (MOF) with such planar devices opens up new perspectives in controlling their efficiency and operating parameters. Here, the study reports on 3D to 2D MOF’ structural transformation to achieve ultrathin nanosheets with enhanced insulating properties. Based on neutral N‐donor ligands, the study designs and solvothermally synthesizes 3D MOFs followed by their thermal and solvent treatment to implement the transformation. A set of single crystal and powder X‐ray diffraction, electron microscopy, Raman spectroscopy, numerical modeling, and mechanical exfoliation confirm the nature of the transformation. Compared with initial 3D MOF, its nanosheets demonstrate sufficient changes in electronic properties, expressed as tuning their absorption, photoluminescence, and resistivity. The latter allows to demonstrate the prototype of ultrathin memristive element based on a 4 to 32 nm MOF nanosheet with enhanced functionality (150 to 1400 ON/OFF ratio, retention time exceeding 7300 s, and 100 cycles of switching), thereby, extending the list of scalable and insulating 2D MOFs for micro‐ and opto‐electronics.
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spelling doaj-art-303bb83207f745a69f6ba9eeedea66722025-08-20T02:18:32ZengWileyAdvanced Science2198-38442025-04-011216n/an/a10.1002/advs.202405989Transformation of 3D Metal–Organic Frameworks into Nanosheets with Enhanced Memristive Behavior for Electronic Data ProcessingYuri A. Mezenov0Semyon V. Bachinin1Yuliya A. Kenzhebayeva2Anastasiia S. Efimova3Pavel V. Alekseevskiy4Daria Poloneeva5Anastasia Lubimova6Svyatoslav A. Povarov7Vladimir Shirobokov8Mikhail S. Dunaevskiy9Aleksandra S. Falchevskaya10Andrei S. Potapov11Alexander Novikov12Artem A. Selyutin13Pascal Boulet14Alena N. Kulakova15Valentin A. Milichko16Qingdao Innovation and Development Center Harbin Engineering University Qingdao Shandong 266000 ChinaSchool of Physics and Engineering ITMO University St. Petersburg 197101 RussiaSchool of Physics and Engineering ITMO University St. Petersburg 197101 RussiaSchool of Physics and Engineering ITMO University St. Petersburg 197101 RussiaSchool of Physics and Engineering ITMO University St. Petersburg 197101 RussiaAdvanced Catalytic Materials (ACM) KAUST Catalysis Center (KCC) Division of Physical Sciences and Engineering King Abdullah University of Science and Technology Thuwal 23955 Saudi ArabiaSchool of Physics and Engineering ITMO University St. Petersburg 197101 RussiaSchool of Physics and Engineering ITMO University St. Petersburg 197101 RussiaSchool of Physics and Engineering ITMO University St. Petersburg 197101 RussiaSchool of Physics and Engineering ITMO University St. Petersburg 197101 RussiaITMO University “Solution Chemistry of Advanced Materials and Technologies” (SCAMT) International Institute Saint Petersburg 191002 RussiaNikolaev Institute of Inorganic Chemistry Siberian Branch of the Russian Academy of Sciences Laboratory of Metal‐Organic Coordination Polymers Novosibirsk 630090 RussiaSaint Petersburg State University Saint Petersburg 199034 RussiaSaint Petersburg State University Saint Petersburg 199034 RussiaInstitut Jean Lamour Universit de Lorraine UMR CNRS 7198 Nancy 54011 FranceSchool of Physics and Engineering ITMO University St. Petersburg 197101 RussiaSchool of Physics and Engineering ITMO University St. Petersburg 197101 RussiaAbstract The transition from three‐dimensional (3D) to two‐dimensional (2D) semiconducting and insulating materials for micro‐ and opto‐electronics is driven by an energy efficiency and device miniaturization. Herein, the simplicity of growth and stacking of 2D metal–organic framework (MOF) with such planar devices opens up new perspectives in controlling their efficiency and operating parameters. Here, the study reports on 3D to 2D MOF’ structural transformation to achieve ultrathin nanosheets with enhanced insulating properties. Based on neutral N‐donor ligands, the study designs and solvothermally synthesizes 3D MOFs followed by their thermal and solvent treatment to implement the transformation. A set of single crystal and powder X‐ray diffraction, electron microscopy, Raman spectroscopy, numerical modeling, and mechanical exfoliation confirm the nature of the transformation. Compared with initial 3D MOF, its nanosheets demonstrate sufficient changes in electronic properties, expressed as tuning their absorption, photoluminescence, and resistivity. The latter allows to demonstrate the prototype of ultrathin memristive element based on a 4 to 32 nm MOF nanosheet with enhanced functionality (150 to 1400 ON/OFF ratio, retention time exceeding 7300 s, and 100 cycles of switching), thereby, extending the list of scalable and insulating 2D MOFs for micro‐ and opto‐electronics.https://doi.org/10.1002/advs.202405989memristive behaviormetal–organic frameworksnanosheetsstructural transformation
spellingShingle Yuri A. Mezenov
Semyon V. Bachinin
Yuliya A. Kenzhebayeva
Anastasiia S. Efimova
Pavel V. Alekseevskiy
Daria Poloneeva
Anastasia Lubimova
Svyatoslav A. Povarov
Vladimir Shirobokov
Mikhail S. Dunaevskiy
Aleksandra S. Falchevskaya
Andrei S. Potapov
Alexander Novikov
Artem A. Selyutin
Pascal Boulet
Alena N. Kulakova
Valentin A. Milichko
Transformation of 3D Metal–Organic Frameworks into Nanosheets with Enhanced Memristive Behavior for Electronic Data Processing
Advanced Science
memristive behavior
metal–organic frameworks
nanosheets
structural transformation
title Transformation of 3D Metal–Organic Frameworks into Nanosheets with Enhanced Memristive Behavior for Electronic Data Processing
title_full Transformation of 3D Metal–Organic Frameworks into Nanosheets with Enhanced Memristive Behavior for Electronic Data Processing
title_fullStr Transformation of 3D Metal–Organic Frameworks into Nanosheets with Enhanced Memristive Behavior for Electronic Data Processing
title_full_unstemmed Transformation of 3D Metal–Organic Frameworks into Nanosheets with Enhanced Memristive Behavior for Electronic Data Processing
title_short Transformation of 3D Metal–Organic Frameworks into Nanosheets with Enhanced Memristive Behavior for Electronic Data Processing
title_sort transformation of 3d metal organic frameworks into nanosheets with enhanced memristive behavior for electronic data processing
topic memristive behavior
metal–organic frameworks
nanosheets
structural transformation
url https://doi.org/10.1002/advs.202405989
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