Metal Sulfide Nanoparticles as Sphalerite Surface Activators to Improve Zinc Recovery Through Flotation Process

CuS nanoparticles (<b>Np</b>) were synthesized and deposited on synthetic sphalerite (<b>S<sub>P</sub></b>) using two different methods. Two nanoparticle products were obtained on the surface of S<sub>P</sub>, <b>Np1</b> and <b>Np2<...

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Main Authors: Delia Monserrat Ávila-Márquez, Alien Blanco-Flores, Helen Paola Toledo-Jaldin, Maribel González Torres, Alfredo Rafael Vilchis-Nestor, Iván Alejandro Reyes Domínguez, Ramiro de Aquino García
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Language:English
Published: MDPI AG 2024-12-01
Series:Separations
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Online Access:https://www.mdpi.com/2297-8739/11/12/358
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author Delia Monserrat Ávila-Márquez
Alien Blanco-Flores
Helen Paola Toledo-Jaldin
Maribel González Torres
Alfredo Rafael Vilchis-Nestor
Iván Alejandro Reyes Domínguez
Ramiro de Aquino García
author_facet Delia Monserrat Ávila-Márquez
Alien Blanco-Flores
Helen Paola Toledo-Jaldin
Maribel González Torres
Alfredo Rafael Vilchis-Nestor
Iván Alejandro Reyes Domínguez
Ramiro de Aquino García
author_sort Delia Monserrat Ávila-Márquez
collection DOAJ
description CuS nanoparticles (<b>Np</b>) were synthesized and deposited on synthetic sphalerite (<b>S<sub>P</sub></b>) using two different methods. Two nanoparticle products were obtained on the surface of S<sub>P</sub>, <b>Np1</b> and <b>Np2</b>, resulting in two active materials (<b>Np1-S<sub>P</sub></b> and <b>Np2-S<sub>P</sub></b>) with specific characteristics. Nanoparticles and active materials were characterized by TEM, XRD, SEM, and XPS. The collectors PAX and SIPX were adsorbed on <b>Np1-S<sub>P</sub></b> and <b>Np2-S<sub>P</sub></b> to determine the adsorption capacity. Method 1 provides a higher quantity of nanoparticles on <b>S<sub>P</sub></b>, which allows for the adsorption of a higher amount of SIPX. Method 1 was used to deposit nanoparticles on two natural sphalerites (<b>S<sub>N</sub></b>) with different iron contents. <b>S<sub>N</sub></b>, unlike <b>S<sub>P</sub></b>, can be used to test nanoparticle activation results in microflotation experiments. <b>S<sub>N</sub></b> was activated with nanoparticles (<b>Np1-S<sub>N</sub></b>) and using the traditional method (<b>Cu-S<sub>N</sub></b>). The recovery of 75% of zinc using the microflotation process suggests that the hydrophobicity of <b>Np1-S<sub>N</sub></b> is higher than that of <b>Cu-S<sub>N</sub></b>. Nanoparticles improve the hydrophobicity of <b>S<sub>N</sub></b> compared to the traditional activation used in the mining industry. These results suggest that using nanoparticles is an excellent option to activate minerals in flotation processes, decreasing the consumption of reagents and helping to mitigate negative impacts on the environment.
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spelling doaj-art-2fee8549ce4d451fb5596a34d31274322025-08-20T02:43:54ZengMDPI AGSeparations2297-87392024-12-01111235810.3390/separations11120358Metal Sulfide Nanoparticles as Sphalerite Surface Activators to Improve Zinc Recovery Through Flotation ProcessDelia Monserrat Ávila-Márquez0Alien Blanco-Flores1Helen Paola Toledo-Jaldin2Maribel González Torres3Alfredo Rafael Vilchis-Nestor4Iván Alejandro Reyes Domínguez5Ramiro de Aquino García6Institute of Metallurgy, Autonomous University of San Luis Potosi, Av. Sierra Leona 550, Lomas 2a Sección, San Luis Potosí 78210, MexicoMechanical Engineering Division, Technological of Superior Studies of Tianguistenco, National Technological of Mexico, Carretera Tenango-Marquesa Km 22, Santiago Tilapa, Santiago Tianguistenco 52650, MexicoInstitute of Metallurgy, Autonomous University of San Luis Potosi, Av. Sierra Leona 550, Lomas 2a Sección, San Luis Potosí 78210, MexicoMechanical Engineering Division, Technological of Superior Studies of Tianguistenco, National Technological of Mexico, Carretera Tenango-Marquesa Km 22, Santiago Tilapa, Santiago Tianguistenco 52650, MexicoJoint Center for Research in Sustainable Chemistry UAEM-UNAM, Toluca 50200, MexicoInstitute of Metallurgy, Autonomous University of San Luis Potosi, Av. Sierra Leona 550, Lomas 2a Sección, San Luis Potosí 78210, MexicoMechanical Engineering Division, Technological of Superior Studies of Tianguistenco, National Technological of Mexico, Carretera Tenango-Marquesa Km 22, Santiago Tilapa, Santiago Tianguistenco 52650, MexicoCuS nanoparticles (<b>Np</b>) were synthesized and deposited on synthetic sphalerite (<b>S<sub>P</sub></b>) using two different methods. Two nanoparticle products were obtained on the surface of S<sub>P</sub>, <b>Np1</b> and <b>Np2</b>, resulting in two active materials (<b>Np1-S<sub>P</sub></b> and <b>Np2-S<sub>P</sub></b>) with specific characteristics. Nanoparticles and active materials were characterized by TEM, XRD, SEM, and XPS. The collectors PAX and SIPX were adsorbed on <b>Np1-S<sub>P</sub></b> and <b>Np2-S<sub>P</sub></b> to determine the adsorption capacity. Method 1 provides a higher quantity of nanoparticles on <b>S<sub>P</sub></b>, which allows for the adsorption of a higher amount of SIPX. Method 1 was used to deposit nanoparticles on two natural sphalerites (<b>S<sub>N</sub></b>) with different iron contents. <b>S<sub>N</sub></b>, unlike <b>S<sub>P</sub></b>, can be used to test nanoparticle activation results in microflotation experiments. <b>S<sub>N</sub></b> was activated with nanoparticles (<b>Np1-S<sub>N</sub></b>) and using the traditional method (<b>Cu-S<sub>N</sub></b>). The recovery of 75% of zinc using the microflotation process suggests that the hydrophobicity of <b>Np1-S<sub>N</sub></b> is higher than that of <b>Cu-S<sub>N</sub></b>. Nanoparticles improve the hydrophobicity of <b>S<sub>N</sub></b> compared to the traditional activation used in the mining industry. These results suggest that using nanoparticles is an excellent option to activate minerals in flotation processes, decreasing the consumption of reagents and helping to mitigate negative impacts on the environment.https://www.mdpi.com/2297-8739/11/12/358CuS nanoparticlessodium isopropyl xanthatepotassium amyl xanthatekinetics adsorption modelsmicroflotation
spellingShingle Delia Monserrat Ávila-Márquez
Alien Blanco-Flores
Helen Paola Toledo-Jaldin
Maribel González Torres
Alfredo Rafael Vilchis-Nestor
Iván Alejandro Reyes Domínguez
Ramiro de Aquino García
Metal Sulfide Nanoparticles as Sphalerite Surface Activators to Improve Zinc Recovery Through Flotation Process
Separations
CuS nanoparticles
sodium isopropyl xanthate
potassium amyl xanthate
kinetics adsorption models
microflotation
title Metal Sulfide Nanoparticles as Sphalerite Surface Activators to Improve Zinc Recovery Through Flotation Process
title_full Metal Sulfide Nanoparticles as Sphalerite Surface Activators to Improve Zinc Recovery Through Flotation Process
title_fullStr Metal Sulfide Nanoparticles as Sphalerite Surface Activators to Improve Zinc Recovery Through Flotation Process
title_full_unstemmed Metal Sulfide Nanoparticles as Sphalerite Surface Activators to Improve Zinc Recovery Through Flotation Process
title_short Metal Sulfide Nanoparticles as Sphalerite Surface Activators to Improve Zinc Recovery Through Flotation Process
title_sort metal sulfide nanoparticles as sphalerite surface activators to improve zinc recovery through flotation process
topic CuS nanoparticles
sodium isopropyl xanthate
potassium amyl xanthate
kinetics adsorption models
microflotation
url https://www.mdpi.com/2297-8739/11/12/358
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