Modified QuEChERS method combined with ultra-high performance liquid chromatography-tandem mass spectrometry for simultaneous determination of 19 quinolones and sulfonamides in aquatic products
<b>Objective:</b> A simultaneous determination method was established for detecting 19 kinds of quinolones and sulfonamides in aquatic products simultaneously, by using QuEChERS combined with UPLC-MS/MS. <b>Methods:</b> Samples were extracted with 1.0% formic acid acetonitril...
Saved in:
| Main Authors: | , , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
The Editorial Office of Food and Machinery
2023-10-01
|
| Series: | Shipin yu jixie |
| Subjects: | |
| Online Access: | http://www.ifoodmm.com/spyjxen/article/abstract/20230706 |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| _version_ | 1850159409798316032 |
|---|---|
| author | SUN Juan YANG Jing ZHAO Chun-hui SHEN Yuan LI Ying FANG Fang |
| author_facet | SUN Juan YANG Jing ZHAO Chun-hui SHEN Yuan LI Ying FANG Fang |
| author_sort | SUN Juan |
| collection | DOAJ |
| description | <b>Objective:</b> A simultaneous determination method was established for detecting 19 kinds of quinolones and sulfonamides in aquatic products simultaneously, by using QuEChERS combined with UPLC-MS/MS. <b>Methods:</b> Samples were extracted with 1.0% formic acid acetonitrile solution, ultrasonic for 1 min, and purified by QuEChERS multi-function needle filter. The sample purification and filtering were performed simultaneously. The Mass spectrometry was conducted by using positive (ESI+) electrospray ionization and multi-reactions monitoring (MRM) models, with external standard method. <b>Results:</b> The detection limit of 19 kinds of sulfonamides and quinolones is from 0.5 to 1.0 μg/kg. Compared with the national standard method, the detection sensitivity is improved. The added recoveries were from 81.0% to 113.0%, and the relative standard deviation (RSD) were from 0.2% to 11.7%. <b>Conclusion:</b> This method assisted ultrasonic extraction and QuEChERS, enhanced the efficiency of measuring quinolones and sulfonamides in aquatic products. It is a simple, rapid, sensitivity, accurate method, which provides an efficient technical means for daily monitoring of sulfonamides and quinolones in large quantities of aquatic product samples. |
| format | Article |
| id | doaj-art-2fe432909027401da76a6ff55869f382 |
| institution | OA Journals |
| issn | 1003-5788 |
| language | English |
| publishDate | 2023-10-01 |
| publisher | The Editorial Office of Food and Machinery |
| record_format | Article |
| series | Shipin yu jixie |
| spelling | doaj-art-2fe432909027401da76a6ff55869f3822025-08-20T02:23:32ZengThe Editorial Office of Food and MachineryShipin yu jixie1003-57882023-10-013974047,24010.13652/j.spjx.1003.5788.2022.81147Modified QuEChERS method combined with ultra-high performance liquid chromatography-tandem mass spectrometry for simultaneous determination of 19 quinolones and sulfonamides in aquatic productsSUN Juan0YANG Jing1ZHAO Chun-hui2SHEN Yuan3LI Ying4FANG Fang5 Beijing Agricultural Product Quality and Safety Center, Beijing 102629 , China Beijing Agricultural Product Quality and Safety Center, Beijing 102629 , China Aquatic Product Technology Promotion of Beijing, Beijing 100176 , China Beijing Agricultural Product Quality and Safety Center, Beijing 102629 , China Beijing Agricultural Product Quality and Safety Center, Beijing 102629 , China Beijing Agricultural Product Quality and Safety Center, Beijing 102629 , China <b>Objective:</b> A simultaneous determination method was established for detecting 19 kinds of quinolones and sulfonamides in aquatic products simultaneously, by using QuEChERS combined with UPLC-MS/MS. <b>Methods:</b> Samples were extracted with 1.0% formic acid acetonitrile solution, ultrasonic for 1 min, and purified by QuEChERS multi-function needle filter. The sample purification and filtering were performed simultaneously. The Mass spectrometry was conducted by using positive (ESI+) electrospray ionization and multi-reactions monitoring (MRM) models, with external standard method. <b>Results:</b> The detection limit of 19 kinds of sulfonamides and quinolones is from 0.5 to 1.0 μg/kg. Compared with the national standard method, the detection sensitivity is improved. The added recoveries were from 81.0% to 113.0%, and the relative standard deviation (RSD) were from 0.2% to 11.7%. <b>Conclusion:</b> This method assisted ultrasonic extraction and QuEChERS, enhanced the efficiency of measuring quinolones and sulfonamides in aquatic products. It is a simple, rapid, sensitivity, accurate method, which provides an efficient technical means for daily monitoring of sulfonamides and quinolones in large quantities of aquatic product samples.http://www.ifoodmm.com/spyjxen/article/abstract/20230706 uplc-ms/ms quechers aquatic products quinolones sulfonamides |
| spellingShingle | SUN Juan YANG Jing ZHAO Chun-hui SHEN Yuan LI Ying FANG Fang Modified QuEChERS method combined with ultra-high performance liquid chromatography-tandem mass spectrometry for simultaneous determination of 19 quinolones and sulfonamides in aquatic products Shipin yu jixie uplc-ms/ms quechers aquatic products quinolones sulfonamides |
| title | Modified QuEChERS method combined with ultra-high performance liquid chromatography-tandem mass spectrometry for simultaneous determination of 19 quinolones and sulfonamides in aquatic products |
| title_full | Modified QuEChERS method combined with ultra-high performance liquid chromatography-tandem mass spectrometry for simultaneous determination of 19 quinolones and sulfonamides in aquatic products |
| title_fullStr | Modified QuEChERS method combined with ultra-high performance liquid chromatography-tandem mass spectrometry for simultaneous determination of 19 quinolones and sulfonamides in aquatic products |
| title_full_unstemmed | Modified QuEChERS method combined with ultra-high performance liquid chromatography-tandem mass spectrometry for simultaneous determination of 19 quinolones and sulfonamides in aquatic products |
| title_short | Modified QuEChERS method combined with ultra-high performance liquid chromatography-tandem mass spectrometry for simultaneous determination of 19 quinolones and sulfonamides in aquatic products |
| title_sort | modified quechers method combined with ultra high performance liquid chromatography tandem mass spectrometry for simultaneous determination of 19 quinolones and sulfonamides in aquatic products |
| topic | uplc-ms/ms quechers aquatic products quinolones sulfonamides |
| url | http://www.ifoodmm.com/spyjxen/article/abstract/20230706 |
| work_keys_str_mv | AT sunjuan modifiedquechersmethodcombinedwithultrahighperformanceliquidchromatographytandemmassspectrometryforsimultaneousdeterminationof19quinolonesandsulfonamidesinaquaticproducts AT yangjing modifiedquechersmethodcombinedwithultrahighperformanceliquidchromatographytandemmassspectrometryforsimultaneousdeterminationof19quinolonesandsulfonamidesinaquaticproducts AT zhaochunhui modifiedquechersmethodcombinedwithultrahighperformanceliquidchromatographytandemmassspectrometryforsimultaneousdeterminationof19quinolonesandsulfonamidesinaquaticproducts AT shenyuan modifiedquechersmethodcombinedwithultrahighperformanceliquidchromatographytandemmassspectrometryforsimultaneousdeterminationof19quinolonesandsulfonamidesinaquaticproducts AT liying modifiedquechersmethodcombinedwithultrahighperformanceliquidchromatographytandemmassspectrometryforsimultaneousdeterminationof19quinolonesandsulfonamidesinaquaticproducts AT fangfang modifiedquechersmethodcombinedwithultrahighperformanceliquidchromatographytandemmassspectrometryforsimultaneousdeterminationof19quinolonesandsulfonamidesinaquaticproducts |