Preparation and Characterization of Double-Layered Microcapsules Containing Nano-SiO2
The double-layered microencapsulation technology has been used in many fields. In this study, the double-layered microencapsulated anthocyanin of Passiflora edulis shells (APESs) was prepared via complex coacervation using gelatin and gum Arabic as the first wall materials (single-layered microcapsu...
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| Format: | Article |
| Language: | English |
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Wiley
2021-01-01
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| Series: | International Journal of Polymer Science |
| Online Access: | http://dx.doi.org/10.1155/2021/6675278 |
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| author | Xue Sun Jingcheng Su Rui Zhang Fangyu Fan |
| author_facet | Xue Sun Jingcheng Su Rui Zhang Fangyu Fan |
| author_sort | Xue Sun |
| collection | DOAJ |
| description | The double-layered microencapsulation technology has been used in many fields. In this study, the double-layered microencapsulated anthocyanin of Passiflora edulis shells (APESs) was prepared via complex coacervation using gelatin and gum Arabic as the first wall materials (single-layered microcapsules (SMs)) and using gum Arabic containing nano-SiO2 as the second wall material (double-layered microcapsules (DMs)/nano-SiO2) to enhance the stability of the core material. Properties of microcapsules were analyzed on the basis of EE, morphology, scanning electron microscopy (SEM), droplet size, moisture content, and differential scanning calorimetry (DSC). The results showed that the EE values of SMs, DMs, and DMs/nano-SiO2 were 96.12%, 97.24%, and 97.85%, respectively. DMs/nano-SiO2 had the lowest moisture content (2.17%). The average droplet size of DMs/nano-SiO2 (34.93 μm) was higher than those of SMs and DMs. DSC indicated that the melting temperature of DMs/nano-SiO2 was 73.61°C and 45.33°C higher than those of SMs and DMs, respectively. SEM demonstrated that DMs/nano-SiO2 had the smoothest surface compared with the other two kinds of microcapsules. The storage stability of APESs and their microcapsules indicated that the stability of the microcapsules was improved by adding DMs/nano-SiO2 into the wall material of microcapsules. These results indicated double-layered microcapsules containing silica nanoparticles contribute to the stability of the core material. |
| format | Article |
| id | doaj-art-2f564765fb71436ebce9c882f0de6458 |
| institution | Kabale University |
| issn | 1687-9422 1687-9430 |
| language | English |
| publishDate | 2021-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | International Journal of Polymer Science |
| spelling | doaj-art-2f564765fb71436ebce9c882f0de64582025-02-03T01:20:32ZengWileyInternational Journal of Polymer Science1687-94221687-94302021-01-01202110.1155/2021/66752786675278Preparation and Characterization of Double-Layered Microcapsules Containing Nano-SiO2Xue Sun0Jingcheng Su1Rui Zhang2Fangyu Fan3Key Laboratory for Forest Resources Conservation and Utilisation in the Southwest Mountains of China, Ministry of Education, and College of Life Sciences, Southwest Forestry University, Kunming, Yunnan 650224, ChinaKey Laboratory for Forest Resources Conservation and Utilisation in the Southwest Mountains of China, Ministry of Education, and College of Life Sciences, Southwest Forestry University, Kunming, Yunnan 650224, ChinaKey Laboratory for Forest Resources Conservation and Utilisation in the Southwest Mountains of China, Ministry of Education, and College of Life Sciences, Southwest Forestry University, Kunming, Yunnan 650224, ChinaKey Laboratory for Forest Resources Conservation and Utilisation in the Southwest Mountains of China, Ministry of Education, and College of Life Sciences, Southwest Forestry University, Kunming, Yunnan 650224, ChinaThe double-layered microencapsulation technology has been used in many fields. In this study, the double-layered microencapsulated anthocyanin of Passiflora edulis shells (APESs) was prepared via complex coacervation using gelatin and gum Arabic as the first wall materials (single-layered microcapsules (SMs)) and using gum Arabic containing nano-SiO2 as the second wall material (double-layered microcapsules (DMs)/nano-SiO2) to enhance the stability of the core material. Properties of microcapsules were analyzed on the basis of EE, morphology, scanning electron microscopy (SEM), droplet size, moisture content, and differential scanning calorimetry (DSC). The results showed that the EE values of SMs, DMs, and DMs/nano-SiO2 were 96.12%, 97.24%, and 97.85%, respectively. DMs/nano-SiO2 had the lowest moisture content (2.17%). The average droplet size of DMs/nano-SiO2 (34.93 μm) was higher than those of SMs and DMs. DSC indicated that the melting temperature of DMs/nano-SiO2 was 73.61°C and 45.33°C higher than those of SMs and DMs, respectively. SEM demonstrated that DMs/nano-SiO2 had the smoothest surface compared with the other two kinds of microcapsules. The storage stability of APESs and their microcapsules indicated that the stability of the microcapsules was improved by adding DMs/nano-SiO2 into the wall material of microcapsules. These results indicated double-layered microcapsules containing silica nanoparticles contribute to the stability of the core material.http://dx.doi.org/10.1155/2021/6675278 |
| spellingShingle | Xue Sun Jingcheng Su Rui Zhang Fangyu Fan Preparation and Characterization of Double-Layered Microcapsules Containing Nano-SiO2 International Journal of Polymer Science |
| title | Preparation and Characterization of Double-Layered Microcapsules Containing Nano-SiO2 |
| title_full | Preparation and Characterization of Double-Layered Microcapsules Containing Nano-SiO2 |
| title_fullStr | Preparation and Characterization of Double-Layered Microcapsules Containing Nano-SiO2 |
| title_full_unstemmed | Preparation and Characterization of Double-Layered Microcapsules Containing Nano-SiO2 |
| title_short | Preparation and Characterization of Double-Layered Microcapsules Containing Nano-SiO2 |
| title_sort | preparation and characterization of double layered microcapsules containing nano sio2 |
| url | http://dx.doi.org/10.1155/2021/6675278 |
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