Compressibility of single-crystal zircon up to 19 GPa: implications for the partitioning coefficient of trace elements

<p>Zircon is a widely studied accessory mineral that helps us understand the evolution of the Earth. The unique nature of zircon is due to its chemical and physical strength and the characteristic crystallographic zirconium site, which is compatible with rare Earth elements and actinoids. Acco...

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Main Authors: S. Maitani, R. Sinmyo, H. Higuchi, T. Ikeda-Fukazawa, S. Kawaguchi-Imada
Format: Article
Language:English
Published: Copernicus Publications 2025-04-01
Series:European Journal of Mineralogy
Online Access:https://ejm.copernicus.org/articles/37/257/2025/ejm-37-257-2025.pdf
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author S. Maitani
R. Sinmyo
H. Higuchi
T. Ikeda-Fukazawa
S. Kawaguchi-Imada
author_facet S. Maitani
R. Sinmyo
H. Higuchi
T. Ikeda-Fukazawa
S. Kawaguchi-Imada
author_sort S. Maitani
collection DOAJ
description <p>Zircon is a widely studied accessory mineral that helps us understand the evolution of the Earth. The unique nature of zircon is due to its chemical and physical strength and the characteristic crystallographic zirconium site, which is compatible with rare Earth elements and actinoids. According to the lattice strain model, trace element partitioning coefficients can be predicted by zircon's compressibility of the cation site. However, the crystal structure of zircon has been precisely determined at less than 5 GPa by single-crystal X-ray diffraction measurements. Here, we have precisely determined the crystal structure of zircon under high-pressure conditions of up to 19 GPa, covering the whole stability field of zircon using a diamond anvil cell. We have also theoretically calculated the unit cell parameters of zircon at high pressure by molecular dynamics simulations. The unit cell parameters and the bond length showed abnormal trends above the high-pressure stability limit of zircon. The previous discrepancy in the compressibility is likely due to the non-hydrostatic condition and instability of the sample. We determined the compressibility of the Zr–O bond and ZrO<span class="inline-formula"><sub>8</sub></span> polyhedra based on the determined crystal structure. The averaged length of the Zr–O bond showed a consistent modulus, with the partitioning coefficients predicted by the lattice strain model. On the contrary, the model with a Poisson solid assumption is inconsistent with the partitioning coefficients. The averaged lengths of the cation–anion bonds under high pressure can help in understanding the partitioning coefficient between minerals and melt.</p>
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spelling doaj-art-2f19e467c14b4fa3a0bb5878ba6ceca42025-08-20T02:15:51ZengCopernicus PublicationsEuropean Journal of Mineralogy0935-12211617-40112025-04-013725726710.5194/ejm-37-257-2025Compressibility of single-crystal zircon up to 19&thinsp;GPa: implications for the partitioning coefficient of trace elementsS. Maitani0R. Sinmyo1H. Higuchi2T. Ikeda-Fukazawa3S. Kawaguchi-Imada4Department of Physics, School of Science and Technology, Meiji University, 1-1-1 Higashi Mita, Tama-ku, Kawasaki, Kanagawa 214-8571, JapanDepartment of Physics, School of Science and Technology, Meiji University, 1-1-1 Higashi Mita, Tama-ku, Kawasaki, Kanagawa 214-8571, JapanDepartment of Applied Chemistry, School of Science and Technology, Meiji University, 1-1-1 Higashi Mita, Tama-ku, Kawasaki, Kanagawa 214-8571, JapanDepartment of Applied Chemistry, School of Science and Technology, Meiji University, 1-1-1 Higashi Mita, Tama-ku, Kawasaki, Kanagawa 214-8571, JapanJapan Synchrotron Radiation Research Institute, 1-1-1 Koto, Sayo, Hyogo 679-5198, Japan<p>Zircon is a widely studied accessory mineral that helps us understand the evolution of the Earth. The unique nature of zircon is due to its chemical and physical strength and the characteristic crystallographic zirconium site, which is compatible with rare Earth elements and actinoids. According to the lattice strain model, trace element partitioning coefficients can be predicted by zircon's compressibility of the cation site. However, the crystal structure of zircon has been precisely determined at less than 5 GPa by single-crystal X-ray diffraction measurements. Here, we have precisely determined the crystal structure of zircon under high-pressure conditions of up to 19 GPa, covering the whole stability field of zircon using a diamond anvil cell. We have also theoretically calculated the unit cell parameters of zircon at high pressure by molecular dynamics simulations. The unit cell parameters and the bond length showed abnormal trends above the high-pressure stability limit of zircon. The previous discrepancy in the compressibility is likely due to the non-hydrostatic condition and instability of the sample. We determined the compressibility of the Zr–O bond and ZrO<span class="inline-formula"><sub>8</sub></span> polyhedra based on the determined crystal structure. The averaged length of the Zr–O bond showed a consistent modulus, with the partitioning coefficients predicted by the lattice strain model. On the contrary, the model with a Poisson solid assumption is inconsistent with the partitioning coefficients. The averaged lengths of the cation–anion bonds under high pressure can help in understanding the partitioning coefficient between minerals and melt.</p>https://ejm.copernicus.org/articles/37/257/2025/ejm-37-257-2025.pdf
spellingShingle S. Maitani
R. Sinmyo
H. Higuchi
T. Ikeda-Fukazawa
S. Kawaguchi-Imada
Compressibility of single-crystal zircon up to 19&thinsp;GPa: implications for the partitioning coefficient of trace elements
European Journal of Mineralogy
title Compressibility of single-crystal zircon up to 19&thinsp;GPa: implications for the partitioning coefficient of trace elements
title_full Compressibility of single-crystal zircon up to 19&thinsp;GPa: implications for the partitioning coefficient of trace elements
title_fullStr Compressibility of single-crystal zircon up to 19&thinsp;GPa: implications for the partitioning coefficient of trace elements
title_full_unstemmed Compressibility of single-crystal zircon up to 19&thinsp;GPa: implications for the partitioning coefficient of trace elements
title_short Compressibility of single-crystal zircon up to 19&thinsp;GPa: implications for the partitioning coefficient of trace elements
title_sort compressibility of single crystal zircon up to 19 thinsp gpa implications for the partitioning coefficient of trace elements
url https://ejm.copernicus.org/articles/37/257/2025/ejm-37-257-2025.pdf
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AT rsinmyo compressibilityofsinglecrystalzirconupto19thinspgpaimplicationsforthepartitioningcoefficientoftraceelements
AT hhiguchi compressibilityofsinglecrystalzirconupto19thinspgpaimplicationsforthepartitioningcoefficientoftraceelements
AT tikedafukazawa compressibilityofsinglecrystalzirconupto19thinspgpaimplicationsforthepartitioningcoefficientoftraceelements
AT skawaguchiimada compressibilityofsinglecrystalzirconupto19thinspgpaimplicationsforthepartitioningcoefficientoftraceelements