ZrBr<sub>4</sub>-Mediated Phase Engineering in CsPbBr<sub>3</sub> for Enhanced Operational Stability of White-Light-Emitting Diodes

The persistent operational instability of all-inorganic cesium lead halide (CsPbX<sub>3</sub>) perovskite nanocrystals (NCs) has hindered their integration into white-light-emitting diodes (WLEDs). This study introduces a transformative approach by engineering a phase transition from CsP...

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Main Authors: Muhammad Amin Padhiar, Yongqiang Ji, Jing Wang, Noor Zamin Khan, Mengji Xiong, Shuxin Wang
Format: Article
Language:English
Published: MDPI AG 2025-04-01
Series:Nanomaterials
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Online Access:https://www.mdpi.com/2079-4991/15/9/674
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author Muhammad Amin Padhiar
Yongqiang Ji
Jing Wang
Noor Zamin Khan
Mengji Xiong
Shuxin Wang
author_facet Muhammad Amin Padhiar
Yongqiang Ji
Jing Wang
Noor Zamin Khan
Mengji Xiong
Shuxin Wang
author_sort Muhammad Amin Padhiar
collection DOAJ
description The persistent operational instability of all-inorganic cesium lead halide (CsPbX<sub>3</sub>) perovskite nanocrystals (NCs) has hindered their integration into white-light-emitting diodes (WLEDs). This study introduces a transformative approach by engineering a phase transition from CsPbBr<sub>3</sub> NCs to zirconium bromide (ZrBr<sub>4</sub>)-stabilized hexagonal nanocomposites (HNs) through a modified hot-injection synthesis. Structural analyses revealed that the ZrBr<sub>4</sub>-mediated phase transformation induced a structurally ordered lattice with minimized defects, significantly enhancing charge carrier confinement and radiative recombination efficiency. The resulting HNs achieved an exceptional photoluminescence quantum yield (PLQY) of 92%, prolonged emission lifetimes, and suppressed nonradiative decay, attributed to effective surface passivation. The WLEDs with HNs enabled a breakthrough luminous efficiency of 158 lm/W and a record color rendering index (CRI) of 98, outperforming conventional CsPbX<sub>3</sub>-based devices. The WLEDs exhibited robust thermal stability, retaining over 80% of initial emission intensity at 100 °C, and demonstrated exceptional operational stability with negligible PL degradation during 50 h of continuous operation at 100 mA. Commission Internationale de l’Éclairage (CIE) coordinates of (0.35, 0.32) validated pure white-light emission with high chromatic fidelity. This work establishes ZrBr<sub>4</sub>-mediated HNs as a paradigm-shifting material platform, addressing critical stability and efficiency challenges in perovskite optoelectronics and paving the way for next-generation, high-performance lighting solutions.
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spelling doaj-art-2f04ca1c818f4c9c857746c72707ea9b2025-08-20T02:24:58ZengMDPI AGNanomaterials2079-49912025-04-0115967410.3390/nano15090674ZrBr<sub>4</sub>-Mediated Phase Engineering in CsPbBr<sub>3</sub> for Enhanced Operational Stability of White-Light-Emitting DiodesMuhammad Amin Padhiar0Yongqiang Ji1Jing Wang2Noor Zamin Khan3Mengji Xiong4Shuxin Wang5School of Intelligent Manufacturing, Shanghai Zhongqiao Vocational and Technical University, Shanghai 201205, ChinaInstitute of Physics, Henan Academy of Sciences, Zhengzhou 450046, ChinaSchool of Intelligent Manufacturing, Shanghai Zhongqiao Vocational and Technical University, Shanghai 201205, ChinaSchool of Physics and Materials Science, Guangzhou University, Guangzhou 510006, ChinaSchool of Intelligent Manufacturing, Shanghai Zhongqiao Vocational and Technical University, Shanghai 201205, ChinaSchool of Intelligent Manufacturing, Shanghai Zhongqiao Vocational and Technical University, Shanghai 201205, ChinaThe persistent operational instability of all-inorganic cesium lead halide (CsPbX<sub>3</sub>) perovskite nanocrystals (NCs) has hindered their integration into white-light-emitting diodes (WLEDs). This study introduces a transformative approach by engineering a phase transition from CsPbBr<sub>3</sub> NCs to zirconium bromide (ZrBr<sub>4</sub>)-stabilized hexagonal nanocomposites (HNs) through a modified hot-injection synthesis. Structural analyses revealed that the ZrBr<sub>4</sub>-mediated phase transformation induced a structurally ordered lattice with minimized defects, significantly enhancing charge carrier confinement and radiative recombination efficiency. The resulting HNs achieved an exceptional photoluminescence quantum yield (PLQY) of 92%, prolonged emission lifetimes, and suppressed nonradiative decay, attributed to effective surface passivation. The WLEDs with HNs enabled a breakthrough luminous efficiency of 158 lm/W and a record color rendering index (CRI) of 98, outperforming conventional CsPbX<sub>3</sub>-based devices. The WLEDs exhibited robust thermal stability, retaining over 80% of initial emission intensity at 100 °C, and demonstrated exceptional operational stability with negligible PL degradation during 50 h of continuous operation at 100 mA. Commission Internationale de l’Éclairage (CIE) coordinates of (0.35, 0.32) validated pure white-light emission with high chromatic fidelity. This work establishes ZrBr<sub>4</sub>-mediated HNs as a paradigm-shifting material platform, addressing critical stability and efficiency challenges in perovskite optoelectronics and paving the way for next-generation, high-performance lighting solutions.https://www.mdpi.com/2079-4991/15/9/674all-inorganic perovskite nanocrystalsphase transformationradiative recombinationwhite-light-emitting diodes (WLEDs)luminous efficiencyoperational stability
spellingShingle Muhammad Amin Padhiar
Yongqiang Ji
Jing Wang
Noor Zamin Khan
Mengji Xiong
Shuxin Wang
ZrBr<sub>4</sub>-Mediated Phase Engineering in CsPbBr<sub>3</sub> for Enhanced Operational Stability of White-Light-Emitting Diodes
Nanomaterials
all-inorganic perovskite nanocrystals
phase transformation
radiative recombination
white-light-emitting diodes (WLEDs)
luminous efficiency
operational stability
title ZrBr<sub>4</sub>-Mediated Phase Engineering in CsPbBr<sub>3</sub> for Enhanced Operational Stability of White-Light-Emitting Diodes
title_full ZrBr<sub>4</sub>-Mediated Phase Engineering in CsPbBr<sub>3</sub> for Enhanced Operational Stability of White-Light-Emitting Diodes
title_fullStr ZrBr<sub>4</sub>-Mediated Phase Engineering in CsPbBr<sub>3</sub> for Enhanced Operational Stability of White-Light-Emitting Diodes
title_full_unstemmed ZrBr<sub>4</sub>-Mediated Phase Engineering in CsPbBr<sub>3</sub> for Enhanced Operational Stability of White-Light-Emitting Diodes
title_short ZrBr<sub>4</sub>-Mediated Phase Engineering in CsPbBr<sub>3</sub> for Enhanced Operational Stability of White-Light-Emitting Diodes
title_sort zrbr sub 4 sub mediated phase engineering in cspbbr sub 3 sub for enhanced operational stability of white light emitting diodes
topic all-inorganic perovskite nanocrystals
phase transformation
radiative recombination
white-light-emitting diodes (WLEDs)
luminous efficiency
operational stability
url https://www.mdpi.com/2079-4991/15/9/674
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