Advancements in Understanding Catalyst Reconstruction During Electrochemical CO2 Reduction

ABSTRACT Electrochemical CO2 reduction reaction (CO2RR) has received great attention to solve CO2‐ induced global warming and carbon neutrality. It is essential to enhance the electrochemical CO2RR selectivity, activity, and long‐term stability for sustainable manufacturing of specific chemicals via...

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Main Authors: Woosuck Kwon, Dohun Kim, Yujin Lee, Jinoh Jung, Dae‐Hyun Nam
Format: Article
Language:English
Published: Wiley 2025-08-01
Series:Exploration
Subjects:
Online Access:https://doi.org/10.1002/EXP.20240019
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author Woosuck Kwon
Dohun Kim
Yujin Lee
Jinoh Jung
Dae‐Hyun Nam
author_facet Woosuck Kwon
Dohun Kim
Yujin Lee
Jinoh Jung
Dae‐Hyun Nam
author_sort Woosuck Kwon
collection DOAJ
description ABSTRACT Electrochemical CO2 reduction reaction (CO2RR) has received great attention to solve CO2‐ induced global warming and carbon neutrality. It is essential to enhance the electrochemical CO2RR selectivity, activity, and long‐term stability for sustainable manufacturing of specific chemicals via CO2RR. To produce multi‐carbon (C2+) chemicals, Cu‐based heterogeneous catalysts have been developed in terms of defect engineering, morphological design, and facet control. Despite the substantial efforts for the design of efficient Cu‐based heterogeneous catalysts, there exist inevitable structural changes of catalysts with continuous dissolution and redeposition during CO2RR. This reconstruction modifies the as‐synthesized catalysts into an unpredictable structure and leads to changes in active site. Here, we review the reconstruction of Cu‐based catalysts during CO2RR, which occurs via continuous dissolution and redeposition process. This includes fundamental principles of reconstruction and the effect of microenvironment on reconstruction during CO2RR. We offer research progress about the reconstruction of Cu‐based electrocatalysts, analysis methodologies to track the reconstruction, and the insight to improve the activity, selectivity, and stability of CO2RR. We provide perspective to understand and harness the reconstruction for the development of efficient CO2RR catalysts.
format Article
id doaj-art-2e98c8e9793741cb92d943f0c6a404c8
institution Kabale University
issn 2766-8509
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language English
publishDate 2025-08-01
publisher Wiley
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series Exploration
spelling doaj-art-2e98c8e9793741cb92d943f0c6a404c82025-08-26T10:33:01ZengWileyExploration2766-85092766-20982025-08-0154n/an/a10.1002/EXP.20240019Advancements in Understanding Catalyst Reconstruction During Electrochemical CO2 ReductionWoosuck Kwon0Dohun Kim1Yujin Lee2Jinoh Jung3Dae‐Hyun Nam4Department of Energy Science and Engineering Daegu Gyeongbuk Institute of Science and Technology (DGIST) Daegu Republic of KoreaDepartment of Energy Science and Engineering Daegu Gyeongbuk Institute of Science and Technology (DGIST) Daegu Republic of KoreaDepartment of Materials Science and Engineering Korea University Seoul Republic of KoreaDepartment of Energy Science and Engineering Daegu Gyeongbuk Institute of Science and Technology (DGIST) Daegu Republic of KoreaDepartment of Energy Science and Engineering Daegu Gyeongbuk Institute of Science and Technology (DGIST) Daegu Republic of KoreaABSTRACT Electrochemical CO2 reduction reaction (CO2RR) has received great attention to solve CO2‐ induced global warming and carbon neutrality. It is essential to enhance the electrochemical CO2RR selectivity, activity, and long‐term stability for sustainable manufacturing of specific chemicals via CO2RR. To produce multi‐carbon (C2+) chemicals, Cu‐based heterogeneous catalysts have been developed in terms of defect engineering, morphological design, and facet control. Despite the substantial efforts for the design of efficient Cu‐based heterogeneous catalysts, there exist inevitable structural changes of catalysts with continuous dissolution and redeposition during CO2RR. This reconstruction modifies the as‐synthesized catalysts into an unpredictable structure and leads to changes in active site. Here, we review the reconstruction of Cu‐based catalysts during CO2RR, which occurs via continuous dissolution and redeposition process. This includes fundamental principles of reconstruction and the effect of microenvironment on reconstruction during CO2RR. We offer research progress about the reconstruction of Cu‐based electrocatalysts, analysis methodologies to track the reconstruction, and the insight to improve the activity, selectivity, and stability of CO2RR. We provide perspective to understand and harness the reconstruction for the development of efficient CO2RR catalysts.https://doi.org/10.1002/EXP.20240019carbon neutralityCO2 reduction reactionelectrocatalystsheterogeneous catalystsreconstruction
spellingShingle Woosuck Kwon
Dohun Kim
Yujin Lee
Jinoh Jung
Dae‐Hyun Nam
Advancements in Understanding Catalyst Reconstruction During Electrochemical CO2 Reduction
Exploration
carbon neutrality
CO2 reduction reaction
electrocatalysts
heterogeneous catalysts
reconstruction
title Advancements in Understanding Catalyst Reconstruction During Electrochemical CO2 Reduction
title_full Advancements in Understanding Catalyst Reconstruction During Electrochemical CO2 Reduction
title_fullStr Advancements in Understanding Catalyst Reconstruction During Electrochemical CO2 Reduction
title_full_unstemmed Advancements in Understanding Catalyst Reconstruction During Electrochemical CO2 Reduction
title_short Advancements in Understanding Catalyst Reconstruction During Electrochemical CO2 Reduction
title_sort advancements in understanding catalyst reconstruction during electrochemical co2 reduction
topic carbon neutrality
CO2 reduction reaction
electrocatalysts
heterogeneous catalysts
reconstruction
url https://doi.org/10.1002/EXP.20240019
work_keys_str_mv AT woosuckkwon advancementsinunderstandingcatalystreconstructionduringelectrochemicalco2reduction
AT dohunkim advancementsinunderstandingcatalystreconstructionduringelectrochemicalco2reduction
AT yujinlee advancementsinunderstandingcatalystreconstructionduringelectrochemicalco2reduction
AT jinohjung advancementsinunderstandingcatalystreconstructionduringelectrochemicalco2reduction
AT daehyunnam advancementsinunderstandingcatalystreconstructionduringelectrochemicalco2reduction