Synthesis and Application of Bis[1,2-(4-aryl-2-alkyl-1H- inden-1-yl)]Ethane as an Efficient`Ligand for Preparation of Olefin Polymerization Catalysts

In this study, a class of bis-1,2-(4-aryl-2-alkyl-1H- inden-1-yl) ethane was synthesized and characterized by spectroscopic methods such as 1HNMR, 13CNMR, melting point and FTIR. bis-1,2-(4-aryl-2-alkyl-1H- inden-1-yl) ethane was synthesized by the reaction of butyl­lithium, arylindenes and dibromoe...

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Main Authors: v. Lotfi, B. Emamgholi, S. T. Bahrami, E. poorakbar
Format: Article
Language:English
Published: University of Tehran 2019-04-01
Series:Journal of Sciences, Islamic Republic of Iran
Subjects:
Online Access:https://jsciences.ut.ac.ir/article_71749_b93b48fa58d212e0abfc55b6fe67d295.pdf
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author v. Lotfi
B. Emamgholi
S. T. Bahrami
E. poorakbar
author_facet v. Lotfi
B. Emamgholi
S. T. Bahrami
E. poorakbar
author_sort v. Lotfi
collection DOAJ
description In this study, a class of bis-1,2-(4-aryl-2-alkyl-1H- inden-1-yl) ethane was synthesized and characterized by spectroscopic methods such as 1HNMR, 13CNMR, melting point and FTIR. bis-1,2-(4-aryl-2-alkyl-1H- inden-1-yl) ethane was synthesized by the reaction of butyl­lithium, arylindenes and dibromoethane in a facile, one-pot strategy. It’s shown that these methods have a wide scope to afford libraries of aryl-substituted indenes. The prepared compounds was then applied as a ligand for the fabrication of a number of metal complexes which can be used as catalyst for the polymerization of the olefins.
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institution OA Journals
issn 1016-1104
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language English
publishDate 2019-04-01
publisher University of Tehran
record_format Article
series Journal of Sciences, Islamic Republic of Iran
spelling doaj-art-2e06cf17f73e4c9b88508e14bbf6d3662025-08-20T02:25:54ZengUniversity of TehranJournal of Sciences, Islamic Republic of Iran1016-11042345-69142019-04-0130213514210.22059/jsciences.2019.7174971749Synthesis and Application of Bis[1,2-(4-aryl-2-alkyl-1H- inden-1-yl)]Ethane as an Efficient`Ligand for Preparation of Olefin Polymerization Catalystsv. Lotfi0B. Emamgholi1S. T. Bahrami2E. poorakbar3Department of Chemistry, Faculty of Sciences, University of Tehran, Tehran, Islamic Republic of IranDepartment of Chemistry, Faculty of Sciences, Imam Khomeini International University, Qazvin, Islamic Republic of IranDepartment of Chemistry, Faculty of Sciences, Islamic Azad University, Qaemshahr Branch, Qaemshahr, Islamic Republic of IranDepartment of Biology, Faculty of Sciences,University of Payame Noor, Tehran, Islamic Republic of IranIn this study, a class of bis-1,2-(4-aryl-2-alkyl-1H- inden-1-yl) ethane was synthesized and characterized by spectroscopic methods such as 1HNMR, 13CNMR, melting point and FTIR. bis-1,2-(4-aryl-2-alkyl-1H- inden-1-yl) ethane was synthesized by the reaction of butyl­lithium, arylindenes and dibromoethane in a facile, one-pot strategy. It’s shown that these methods have a wide scope to afford libraries of aryl-substituted indenes. The prepared compounds was then applied as a ligand for the fabrication of a number of metal complexes which can be used as catalyst for the polymerization of the olefins.https://jsciences.ut.ac.ir/article_71749_b93b48fa58d212e0abfc55b6fe67d295.pdforganometallic compoundmetallocenebis-arylalkyl ethane ligandcatalysis
spellingShingle v. Lotfi
B. Emamgholi
S. T. Bahrami
E. poorakbar
Synthesis and Application of Bis[1,2-(4-aryl-2-alkyl-1H- inden-1-yl)]Ethane as an Efficient`Ligand for Preparation of Olefin Polymerization Catalysts
Journal of Sciences, Islamic Republic of Iran
organometallic compound
metallocene
bis-arylalkyl ethane ligand
catalysis
title Synthesis and Application of Bis[1,2-(4-aryl-2-alkyl-1H- inden-1-yl)]Ethane as an Efficient`Ligand for Preparation of Olefin Polymerization Catalysts
title_full Synthesis and Application of Bis[1,2-(4-aryl-2-alkyl-1H- inden-1-yl)]Ethane as an Efficient`Ligand for Preparation of Olefin Polymerization Catalysts
title_fullStr Synthesis and Application of Bis[1,2-(4-aryl-2-alkyl-1H- inden-1-yl)]Ethane as an Efficient`Ligand for Preparation of Olefin Polymerization Catalysts
title_full_unstemmed Synthesis and Application of Bis[1,2-(4-aryl-2-alkyl-1H- inden-1-yl)]Ethane as an Efficient`Ligand for Preparation of Olefin Polymerization Catalysts
title_short Synthesis and Application of Bis[1,2-(4-aryl-2-alkyl-1H- inden-1-yl)]Ethane as an Efficient`Ligand for Preparation of Olefin Polymerization Catalysts
title_sort synthesis and application of bis 1 2 4 aryl 2 alkyl 1h inden 1 yl ethane as an efficient ligand for preparation of olefin polymerization catalysts
topic organometallic compound
metallocene
bis-arylalkyl ethane ligand
catalysis
url https://jsciences.ut.ac.ir/article_71749_b93b48fa58d212e0abfc55b6fe67d295.pdf
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AT bemamgholi synthesisandapplicationofbis124aryl2alkyl1hinden1ylethaneasanefficientligandforpreparationofolefinpolymerizationcatalysts
AT stbahrami synthesisandapplicationofbis124aryl2alkyl1hinden1ylethaneasanefficientligandforpreparationofolefinpolymerizationcatalysts
AT epoorakbar synthesisandapplicationofbis124aryl2alkyl1hinden1ylethaneasanefficientligandforpreparationofolefinpolymerizationcatalysts