Distinct roles of Nb, Ti, and V microalloying elements on the fire resistance of low-Mo steels

The high-temperature mechanical stability of structural steels is critical for fire-resistant applications, yet the individual contributions of microalloying elements remain incompletely understood. In this study, we systematically investigated the strengthening mechanisms of three key microalloying...

Full description

Saved in:
Bibliographic Details
Main Authors: Hyungkwon Park, Hyo-Haeng Jo, Seong Hoon Kim, Chiwon Kim, Joonoh Moon, Jun-Ho Chung, Bong Ho Lee, Chang-Hoon Lee
Format: Article
Language:English
Published: Elsevier 2025-07-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425015662
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849424664506400768
author Hyungkwon Park
Hyo-Haeng Jo
Seong Hoon Kim
Chiwon Kim
Joonoh Moon
Jun-Ho Chung
Bong Ho Lee
Chang-Hoon Lee
author_facet Hyungkwon Park
Hyo-Haeng Jo
Seong Hoon Kim
Chiwon Kim
Joonoh Moon
Jun-Ho Chung
Bong Ho Lee
Chang-Hoon Lee
author_sort Hyungkwon Park
collection DOAJ
description The high-temperature mechanical stability of structural steels is critical for fire-resistant applications, yet the individual contributions of microalloying elements remain incompletely understood. In this study, we systematically investigated the strengthening mechanisms of three key microalloying elements–Nb, Ti, and V–in low-Mo fire-resistant steel. Each element was independently added to a 0.15Mo-base steel at varying concentrations, and tensile tests were conducted at room temperature (RT) and 600 °C. Microstructural features were characterized in detail using atom probe tomography. Ti enhanced the yield strength (YS) at both temperatures via the formation of (Ti,Mo)(C,N) precipitates, but excessive Ti reduced the YS ratio (σ600oC/σRT) due to solute depletion and precipitate coarsening. V demonstrated minimal precipitation and limited impact at RT, but its linear contribution to high-temperature strength is attributed to secondary hardening by VC. Nb yielded the most consistent strengthening across both temperatures through the combined effects of (Nb,Mo)C precipitation, Nb–C clustering, solid solution strengthening, and bainitic transformation. These findings clarify the element-specific mechanisms governing fire-resistant behavior and suggest that optimized microalloying strategies can enable steels with superior strength retention at elevated temperatures.
format Article
id doaj-art-2dbe7024c19848a6bec661ac9a2ae4f3
institution Kabale University
issn 2238-7854
language English
publishDate 2025-07-01
publisher Elsevier
record_format Article
series Journal of Materials Research and Technology
spelling doaj-art-2dbe7024c19848a6bec661ac9a2ae4f32025-08-20T03:30:04ZengElsevierJournal of Materials Research and Technology2238-78542025-07-01372144215110.1016/j.jmrt.2025.06.144Distinct roles of Nb, Ti, and V microalloying elements on the fire resistance of low-Mo steelsHyungkwon Park0Hyo-Haeng Jo1Seong Hoon Kim2Chiwon Kim3Joonoh Moon4Jun-Ho Chung5Bong Ho Lee6Chang-Hoon Lee7Extreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of KoreaExtreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of KoreaExtreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of KoreaExtreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of KoreaDepartment of Materials Science and Engineering, Changwon National University, Republic of KoreaHyundai Steel Company, Incheon, 22525, Republic of KoreaAdvanced Analysis Team, Institute of Next-generation Semiconductor Convergence Technology, Daegu Gyeongbuk Institute of Science and Technology, Daegu, 42988, Republic of Korea; Corresponding author.Extreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of Korea; Corresponding author.The high-temperature mechanical stability of structural steels is critical for fire-resistant applications, yet the individual contributions of microalloying elements remain incompletely understood. In this study, we systematically investigated the strengthening mechanisms of three key microalloying elements–Nb, Ti, and V–in low-Mo fire-resistant steel. Each element was independently added to a 0.15Mo-base steel at varying concentrations, and tensile tests were conducted at room temperature (RT) and 600 °C. Microstructural features were characterized in detail using atom probe tomography. Ti enhanced the yield strength (YS) at both temperatures via the formation of (Ti,Mo)(C,N) precipitates, but excessive Ti reduced the YS ratio (σ600oC/σRT) due to solute depletion and precipitate coarsening. V demonstrated minimal precipitation and limited impact at RT, but its linear contribution to high-temperature strength is attributed to secondary hardening by VC. Nb yielded the most consistent strengthening across both temperatures through the combined effects of (Nb,Mo)C precipitation, Nb–C clustering, solid solution strengthening, and bainitic transformation. These findings clarify the element-specific mechanisms governing fire-resistant behavior and suggest that optimized microalloying strategies can enable steels with superior strength retention at elevated temperatures.http://www.sciencedirect.com/science/article/pii/S2238785425015662Fire-resistant steelHigh-temperature strengthMicroalloyingAtomic probe tomographyStrengthening mechanism
spellingShingle Hyungkwon Park
Hyo-Haeng Jo
Seong Hoon Kim
Chiwon Kim
Joonoh Moon
Jun-Ho Chung
Bong Ho Lee
Chang-Hoon Lee
Distinct roles of Nb, Ti, and V microalloying elements on the fire resistance of low-Mo steels
Journal of Materials Research and Technology
Fire-resistant steel
High-temperature strength
Microalloying
Atomic probe tomography
Strengthening mechanism
title Distinct roles of Nb, Ti, and V microalloying elements on the fire resistance of low-Mo steels
title_full Distinct roles of Nb, Ti, and V microalloying elements on the fire resistance of low-Mo steels
title_fullStr Distinct roles of Nb, Ti, and V microalloying elements on the fire resistance of low-Mo steels
title_full_unstemmed Distinct roles of Nb, Ti, and V microalloying elements on the fire resistance of low-Mo steels
title_short Distinct roles of Nb, Ti, and V microalloying elements on the fire resistance of low-Mo steels
title_sort distinct roles of nb ti and v microalloying elements on the fire resistance of low mo steels
topic Fire-resistant steel
High-temperature strength
Microalloying
Atomic probe tomography
Strengthening mechanism
url http://www.sciencedirect.com/science/article/pii/S2238785425015662
work_keys_str_mv AT hyungkwonpark distinctrolesofnbtiandvmicroalloyingelementsonthefireresistanceoflowmosteels
AT hyohaengjo distinctrolesofnbtiandvmicroalloyingelementsonthefireresistanceoflowmosteels
AT seonghoonkim distinctrolesofnbtiandvmicroalloyingelementsonthefireresistanceoflowmosteels
AT chiwonkim distinctrolesofnbtiandvmicroalloyingelementsonthefireresistanceoflowmosteels
AT joonohmoon distinctrolesofnbtiandvmicroalloyingelementsonthefireresistanceoflowmosteels
AT junhochung distinctrolesofnbtiandvmicroalloyingelementsonthefireresistanceoflowmosteels
AT bongholee distinctrolesofnbtiandvmicroalloyingelementsonthefireresistanceoflowmosteels
AT changhoonlee distinctrolesofnbtiandvmicroalloyingelementsonthefireresistanceoflowmosteels