Heteroligand copper(II), nickel(II), and cobalt(II) complexes with isonicotinic acid hydrazide and L-histidine

Complex formation in the ternary systems copper(II)/nickel(II)/cobalt(II) – isonicotinic acid hydrazide – L-histidine was studied by the methods of spectrophotometry and mathematical modeling in an aqueous solution with 0.1 mol dm–3 KNO3 as a background electrolyte. The compositions, formation const...

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Main Authors: N.V. Troshanin, T.I. Bychkova
Format: Article
Language:English
Published: Kazan Federal University 2021-03-01
Series:Учёные записки Казанского университета: Серия Естественные науки
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Online Access:https://kpfu.ru/uz-eng-ns-2021-1-4.html
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author N.V. Troshanin
T.I. Bychkova
author_facet N.V. Troshanin
T.I. Bychkova
author_sort N.V. Troshanin
collection DOAJ
description Complex formation in the ternary systems copper(II)/nickel(II)/cobalt(II) – isonicotinic acid hydrazide – L-histidine was studied by the methods of spectrophotometry and mathematical modeling in an aqueous solution with 0.1 mol dm–3 KNO3 as a background electrolyte. The compositions, formation constants, and spectral parameters of the heteroligand complexes with a metal/hydrazide/amino acid ratio of 1:1:1 were determined. It was found that the heteroligand complexes with the neutral form of isonicotinic acid hydrazide have higher stability values than those with the protonated form. The stability of bis- and tris-complexes of the same composition in the series copper(II) – nickel(II) – cobalt(II) is in agreement with the Irving–Williams order. Three isomers of the heteroligand complex of nickel(II) with the protonated form of isonicotinic acid hydrazide and histidine zwitterion were optimized by the method of molecular mechanics. In the system with cobalt(II), a reversible interaction with atmospheric oxygen was revealed.
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publisher Kazan Federal University
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series Учёные записки Казанского университета: Серия Естественные науки
spelling doaj-art-2db1d2d984064d749d665af89e9115ac2025-08-20T02:43:55ZengKazan Federal UniversityУчёные записки Казанского университета: Серия Естественные науки2542-064X2500-218X2021-03-011631456010.26907/2542-064X.2021.1.45-60Heteroligand copper(II), nickel(II), and cobalt(II) complexes with isonicotinic acid hydrazide and L-histidineN.V. Troshanin0T.I. Bychkova1Kazan Federal University, Kazan, 420008 RussiaKazan Federal University, Kazan, 420008 RussiaComplex formation in the ternary systems copper(II)/nickel(II)/cobalt(II) – isonicotinic acid hydrazide – L-histidine was studied by the methods of spectrophotometry and mathematical modeling in an aqueous solution with 0.1 mol dm–3 KNO3 as a background electrolyte. The compositions, formation constants, and spectral parameters of the heteroligand complexes with a metal/hydrazide/amino acid ratio of 1:1:1 were determined. It was found that the heteroligand complexes with the neutral form of isonicotinic acid hydrazide have higher stability values than those with the protonated form. The stability of bis- and tris-complexes of the same composition in the series copper(II) – nickel(II) – cobalt(II) is in agreement with the Irving–Williams order. Three isomers of the heteroligand complex of nickel(II) with the protonated form of isonicotinic acid hydrazide and histidine zwitterion were optimized by the method of molecular mechanics. In the system with cobalt(II), a reversible interaction with atmospheric oxygen was revealed.https://kpfu.ru/uz-eng-ns-2021-1-4.htmlspectrophotometryph-metrymathematical modelingcomplex formationcopper(ii)nickel(ii)cobalt(ii)isonicotinic acid hydrazidel-histidine
spellingShingle N.V. Troshanin
T.I. Bychkova
Heteroligand copper(II), nickel(II), and cobalt(II) complexes with isonicotinic acid hydrazide and L-histidine
Учёные записки Казанского университета: Серия Естественные науки
spectrophotometry
ph-metry
mathematical modeling
complex formation
copper(ii)
nickel(ii)
cobalt(ii)
isonicotinic acid hydrazide
l-histidine
title Heteroligand copper(II), nickel(II), and cobalt(II) complexes with isonicotinic acid hydrazide and L-histidine
title_full Heteroligand copper(II), nickel(II), and cobalt(II) complexes with isonicotinic acid hydrazide and L-histidine
title_fullStr Heteroligand copper(II), nickel(II), and cobalt(II) complexes with isonicotinic acid hydrazide and L-histidine
title_full_unstemmed Heteroligand copper(II), nickel(II), and cobalt(II) complexes with isonicotinic acid hydrazide and L-histidine
title_short Heteroligand copper(II), nickel(II), and cobalt(II) complexes with isonicotinic acid hydrazide and L-histidine
title_sort heteroligand copper ii nickel ii and cobalt ii complexes with isonicotinic acid hydrazide and l histidine
topic spectrophotometry
ph-metry
mathematical modeling
complex formation
copper(ii)
nickel(ii)
cobalt(ii)
isonicotinic acid hydrazide
l-histidine
url https://kpfu.ru/uz-eng-ns-2021-1-4.html
work_keys_str_mv AT nvtroshanin heteroligandcopperiinickeliiandcobaltiicomplexeswithisonicotinicacidhydrazideandlhistidine
AT tibychkova heteroligandcopperiinickeliiandcobaltiicomplexeswithisonicotinicacidhydrazideandlhistidine