Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
A new ethylenediaminetetraacetic acid- (EDTA-) mediated hydrothermal route to prepare chrysanthemum-shaped samarium orthovanadate (SmVO4) nanocrystals with decavanadate (K6V10O28·9H2O) as vanadium source has been developed. The present hydrothermal approach is simple and reproducible and employs a r...
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| Format: | Article |
| Language: | English |
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Wiley
2013-01-01
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| Series: | The Scientific World Journal |
| Online Access: | http://dx.doi.org/10.1155/2013/127816 |
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| author | Quanguo Li Wenli Zuo Feng Li |
| author_facet | Quanguo Li Wenli Zuo Feng Li |
| author_sort | Quanguo Li |
| collection | DOAJ |
| description | A new ethylenediaminetetraacetic acid- (EDTA-) mediated hydrothermal route to prepare chrysanthemum-shaped samarium orthovanadate (SmVO4) nanocrystals with decavanadate (K6V10O28·9H2O) as vanadium source has been developed. The present hydrothermal approach is simple and reproducible and employs a relatively mild reaction temperature. The EDTA, pH value, and temperature of the reaction systems play important roles in determining the morphologies and growth process of the SmVO4 products. The products have been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), photoluminescence spectra (PL), and UV-Vis spectroscopy. |
| format | Article |
| id | doaj-art-2ce02a04053d4c2b8e2378f80bf20eed |
| institution | Kabale University |
| issn | 1537-744X |
| language | English |
| publishDate | 2013-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | The Scientific World Journal |
| spelling | doaj-art-2ce02a04053d4c2b8e2378f80bf20eed2025-08-20T03:55:16ZengWileyThe Scientific World Journal1537-744X2013-01-01201310.1155/2013/127816127816Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium SourceQuanguo Li0Wenli Zuo1Feng Li2College of Chemistry, Key Lab of Environment Friendly Chemistry and Application in Ministry of Education, Xiangtan University, Xiangtan 411105, ChinaCollege of Chemistry, Key Lab of Environment Friendly Chemistry and Application in Ministry of Education, Xiangtan University, Xiangtan 411105, ChinaCollege of Chemistry, Key Lab of Environment Friendly Chemistry and Application in Ministry of Education, Xiangtan University, Xiangtan 411105, ChinaA new ethylenediaminetetraacetic acid- (EDTA-) mediated hydrothermal route to prepare chrysanthemum-shaped samarium orthovanadate (SmVO4) nanocrystals with decavanadate (K6V10O28·9H2O) as vanadium source has been developed. The present hydrothermal approach is simple and reproducible and employs a relatively mild reaction temperature. The EDTA, pH value, and temperature of the reaction systems play important roles in determining the morphologies and growth process of the SmVO4 products. The products have been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), photoluminescence spectra (PL), and UV-Vis spectroscopy.http://dx.doi.org/10.1155/2013/127816 |
| spellingShingle | Quanguo Li Wenli Zuo Feng Li Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source The Scientific World Journal |
| title | Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source |
| title_full | Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source |
| title_fullStr | Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source |
| title_full_unstemmed | Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source |
| title_short | Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source |
| title_sort | chelating ligand mediated hydrothermal synthesis of samarium orthovanadate with decavanadate as vanadium source |
| url | http://dx.doi.org/10.1155/2013/127816 |
| work_keys_str_mv | AT quanguoli chelatingligandmediatedhydrothermalsynthesisofsamariumorthovanadatewithdecavanadateasvanadiumsource AT wenlizuo chelatingligandmediatedhydrothermalsynthesisofsamariumorthovanadatewithdecavanadateasvanadiumsource AT fengli chelatingligandmediatedhydrothermalsynthesisofsamariumorthovanadatewithdecavanadateasvanadiumsource |