Preparation of outer membrane vesicles from rabbit Bordetella bronchiseptica and their protein composition analysis

This study aimed to establish the optimal preparation method of outer membrane vesicles (OMVs) from rabbit Bordetella bronchiseptica (Bb). The FX-1 strain of rabbit Bb was used as the research object. Centrifugal ultrafiltration and ultrasonication were compared, and followed by the optimization of...

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Main Authors: NAN Li, HUANG Ye’e, XIAO Chenwen, WANG Zhipeng, WEI Qiang, JI Quan’an, LI Ke, LIU Yan, BAO Guolian
Format: Article
Language:English
Published: Zhejiang University Press 2021-04-01
Series:浙江大学学报. 农业与生命科学版
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Online Access:https://www.academax.com/doi/10.3785/j.issn.1008-9209.2020.05.190
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author NAN Li
HUANG Ye’e
XIAO Chenwen
WANG Zhipeng
WEI Qiang
JI Quan’an
LI Ke
LIU Yan
BAO Guolian
author_facet NAN Li
HUANG Ye’e
XIAO Chenwen
WANG Zhipeng
WEI Qiang
JI Quan’an
LI Ke
LIU Yan
BAO Guolian
author_sort NAN Li
collection DOAJ
description This study aimed to establish the optimal preparation method of outer membrane vesicles (OMVs) from rabbit Bordetella bronchiseptica (Bb). The FX-1 strain of rabbit Bb was used as the research object. Centrifugal ultrafiltration and ultrasonication were compared, and followed by the optimization of the preparation technics, such as culture time, antibiotic addition and filtering method. The physical and chemical properties of OMVs were examined with transmission electron microscope (TEM), scanning electron microscope (SEM) and nanoparticle tracking analysis (NTA), etc. The protein compositions were analysed with Bradford protein quantification, sodium dodecyl sulfate-polyacrylamide gel electrophoresis (SDS-PAGE) and liquid chromatography-tandem mass spectrometry (LC-MS/MS). The results showed that centrifugal ultrafiltration was a better preparation method of OMVs, and the optimum culture time, cefalexin concentration and filtering method were 18 h, 64 μg/mL and filtration though 0.45 µm membrane once, respectively. The OMVs showed a spherical shape with the diameter of 127.83 nm±0.68 nm, containing a range of proteins associated with virulence and infection mechanisms. This preparation technique could significantly promote the production of OMVs, which making industrial production possible. Furthermore, analysis of the protein composition lays a foundation for novel subunit vaccine research and development.
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series 浙江大学学报. 农业与生命科学版
spelling doaj-art-2c1db5ed43b548639961ce1129ad9c012025-08-20T03:32:05ZengZhejiang University Press浙江大学学报. 农业与生命科学版1008-92092097-51552021-04-014725126010.3785/j.issn.1008-9209.2020.05.19010089209Preparation of outer membrane vesicles from rabbit Bordetella bronchiseptica and their protein composition analysisNAN LiHUANG Ye’eXIAO ChenwenWANG ZhipengWEI QiangJI Quan’anLI KeLIU YanBAO GuolianThis study aimed to establish the optimal preparation method of outer membrane vesicles (OMVs) from rabbit Bordetella bronchiseptica (Bb). The FX-1 strain of rabbit Bb was used as the research object. Centrifugal ultrafiltration and ultrasonication were compared, and followed by the optimization of the preparation technics, such as culture time, antibiotic addition and filtering method. The physical and chemical properties of OMVs were examined with transmission electron microscope (TEM), scanning electron microscope (SEM) and nanoparticle tracking analysis (NTA), etc. The protein compositions were analysed with Bradford protein quantification, sodium dodecyl sulfate-polyacrylamide gel electrophoresis (SDS-PAGE) and liquid chromatography-tandem mass spectrometry (LC-MS/MS). The results showed that centrifugal ultrafiltration was a better preparation method of OMVs, and the optimum culture time, cefalexin concentration and filtering method were 18 h, 64 μg/mL and filtration though 0.45 µm membrane once, respectively. The OMVs showed a spherical shape with the diameter of 127.83 nm±0.68 nm, containing a range of proteins associated with virulence and infection mechanisms. This preparation technique could significantly promote the production of OMVs, which making industrial production possible. Furthermore, analysis of the protein composition lays a foundation for novel subunit vaccine research and development.https://www.academax.com/doi/10.3785/j.issn.1008-9209.2020.05.190bacterial outer membrane vesicles<italic>Bordetella bronchiseptica</italic> preparation technicprotein composition analysis
spellingShingle NAN Li
HUANG Ye’e
XIAO Chenwen
WANG Zhipeng
WEI Qiang
JI Quan’an
LI Ke
LIU Yan
BAO Guolian
Preparation of outer membrane vesicles from rabbit Bordetella bronchiseptica and their protein composition analysis
浙江大学学报. 农业与生命科学版
bacterial outer membrane vesicles
<italic>Bordetella bronchiseptica</italic>
preparation technic
protein composition analysis
title Preparation of outer membrane vesicles from rabbit Bordetella bronchiseptica and their protein composition analysis
title_full Preparation of outer membrane vesicles from rabbit Bordetella bronchiseptica and their protein composition analysis
title_fullStr Preparation of outer membrane vesicles from rabbit Bordetella bronchiseptica and their protein composition analysis
title_full_unstemmed Preparation of outer membrane vesicles from rabbit Bordetella bronchiseptica and their protein composition analysis
title_short Preparation of outer membrane vesicles from rabbit Bordetella bronchiseptica and their protein composition analysis
title_sort preparation of outer membrane vesicles from rabbit bordetella bronchiseptica and their protein composition analysis
topic bacterial outer membrane vesicles
<italic>Bordetella bronchiseptica</italic>
preparation technic
protein composition analysis
url https://www.academax.com/doi/10.3785/j.issn.1008-9209.2020.05.190
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