Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire

The elastic limit is a critical parameter in spring design, which has a significant impact on the spring characteristic. The influence of cold drawing on the strength, elastic limit, elastic after-effect, and microstructure of 07Cr17Ni7Al ultrafine wire with a diameter of 0.3 mm for valve springs is...

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Main Authors: HE Qinsheng, WANG Jianqiao, ZHAO Zhen, LI Fang, ZHANG Shiqing, WANG Hong, ZOU Xingzheng, TANG Yuanshou, HUANG Min, LI Jing
Format: Article
Language:zho
Published: Journal of Materials Engineering 2025-03-01
Series:Cailiao gongcheng
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Online Access:https://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2023.000785
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author HE Qinsheng
WANG Jianqiao
ZHAO Zhen
LI Fang
ZHANG Shiqing
WANG Hong
ZOU Xingzheng
TANG Yuanshou
HUANG Min
LI Jing
author_facet HE Qinsheng
WANG Jianqiao
ZHAO Zhen
LI Fang
ZHANG Shiqing
WANG Hong
ZOU Xingzheng
TANG Yuanshou
HUANG Min
LI Jing
author_sort HE Qinsheng
collection DOAJ
description The elastic limit is a critical parameter in spring design, which has a significant impact on the spring characteristic. The influence of cold drawing on the strength, elastic limit, elastic after-effect, and microstructure of 07Cr17Ni7Al ultrafine wire with a diameter of 0.3 mm for valve springs is investigated using room temperature tensile tests, single arm bending method, optical microscope(OM), X-ray diffraction(XRD) and scanning electron microscope(SEM). Different mathematical models are used to fit and analyze the deformation and martensite content, deformation-elastic limit, and stress-elastic after-effect. The results show that the solid solution 07Cr17Ni7Al wire is composed of austenite and a small amount of ferrite. Cold drawing transforms austenite into martensite, the content of deformation-induced martensite (DIM) increases with increasing deformation. The relationship between DIM content and cold-drawn equivalent strain (η) conforms to the Olson-Cohen model. When η reaches 1.64, the DIM content is about 92%, and the DIM reaches saturation. The tensile strength of wire exhibits a linear relationship with η, and the larger the deformation, the higher the tensile strength. The relationship between the elastic limit and the η follows an “S” shaped curve and conforms to the DoseResp model. The elastic limit increases with increasing deformation. When the η reaches 1.64 or more, the elastic limit tends to be gentle. The elastic after-effect increases with increasing stress, which conforms to the PWL2 model. There exists a “critical stress for elastic after-effect”. When the stress exceeds this critical value, the rate of elastic after-effect increases by 2-11 times with increasing stress. When the η is 1.64-2.41, the 07Cr17Ni7Al wire has good mechanical and elastic properties.
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publisher Journal of Materials Engineering
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spelling doaj-art-2b7039df94704b39b47aff3adc8d7a4b2025-08-20T03:17:32ZzhoJournal of Materials EngineeringCailiao gongcheng1001-43812025-03-01533839410.11868/j.issn.1001-4381.2023.0007851001-4381(2025)03-0083-12Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wireHE Qinsheng0WANG Jianqiao1ZHAO Zhen2LI Fang3ZHANG Shiqing4WANG Hong5ZOU Xingzheng6TANG Yuanshou7HUANG Min8LI Jing9Department of Functional Materials and Components,Chongqing Materials Research Institute Co.,Ltd.,Chongqing 400707,ChinaDepartment of Functional Materials and Components,Chongqing Materials Research Institute Co.,Ltd.,Chongqing 400707,ChinaDepartment of Functional Materials and Components,Chongqing Materials Research Institute Co.,Ltd.,Chongqing 400707,ChinaDepartment of Functional Materials and Components,Chongqing Materials Research Institute Co.,Ltd.,Chongqing 400707,ChinaDepartment of Functional Materials and Components,Chongqing Materials Research Institute Co.,Ltd.,Chongqing 400707,ChinaDepartment of Functional Materials and Components,Chongqing Materials Research Institute Co.,Ltd.,Chongqing 400707,ChinaDepartment of Functional Materials and Components,Chongqing Materials Research Institute Co.,Ltd.,Chongqing 400707,ChinaDepartment of Functional Materials and Components,Chongqing Materials Research Institute Co.,Ltd.,Chongqing 400707,ChinaDepartment of Functional Materials and Components,Chongqing Materials Research Institute Co.,Ltd.,Chongqing 400707,ChinaCollege of Materials Sciences and Engineering,Chongqing School,University of Chinese Academy of Sciences,Chongqing 400714, ChinaThe elastic limit is a critical parameter in spring design, which has a significant impact on the spring characteristic. The influence of cold drawing on the strength, elastic limit, elastic after-effect, and microstructure of 07Cr17Ni7Al ultrafine wire with a diameter of 0.3 mm for valve springs is investigated using room temperature tensile tests, single arm bending method, optical microscope(OM), X-ray diffraction(XRD) and scanning electron microscope(SEM). Different mathematical models are used to fit and analyze the deformation and martensite content, deformation-elastic limit, and stress-elastic after-effect. The results show that the solid solution 07Cr17Ni7Al wire is composed of austenite and a small amount of ferrite. Cold drawing transforms austenite into martensite, the content of deformation-induced martensite (DIM) increases with increasing deformation. The relationship between DIM content and cold-drawn equivalent strain (η) conforms to the Olson-Cohen model. When η reaches 1.64, the DIM content is about 92%, and the DIM reaches saturation. The tensile strength of wire exhibits a linear relationship with η, and the larger the deformation, the higher the tensile strength. The relationship between the elastic limit and the η follows an “S” shaped curve and conforms to the DoseResp model. The elastic limit increases with increasing deformation. When the η reaches 1.64 or more, the elastic limit tends to be gentle. The elastic after-effect increases with increasing stress, which conforms to the PWL2 model. There exists a “critical stress for elastic after-effect”. When the stress exceeds this critical value, the rate of elastic after-effect increases by 2-11 times with increasing stress. When the η is 1.64-2.41, the 07Cr17Ni7Al wire has good mechanical and elastic properties.https://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2023.000785stainless steeldeformation-induced martensiteelastic limitelastic after-effectmechanical propertyultrafine wirecold drawing
spellingShingle HE Qinsheng
WANG Jianqiao
ZHAO Zhen
LI Fang
ZHANG Shiqing
WANG Hong
ZOU Xingzheng
TANG Yuanshou
HUANG Min
LI Jing
Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire
Cailiao gongcheng
stainless steel
deformation-induced martensite
elastic limit
elastic after-effect
mechanical property
ultrafine wire
cold drawing
title Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire
title_full Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire
title_fullStr Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire
title_full_unstemmed Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire
title_short Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire
title_sort evolution of microstructure and properties of cold drawn 07cr17ni7al ultrafine wire
topic stainless steel
deformation-induced martensite
elastic limit
elastic after-effect
mechanical property
ultrafine wire
cold drawing
url https://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2023.000785
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