Mussel-Inspired Hydrogels Incorporating Graphite Derivatives for Soft Tissue Regeneration

Hyaluronic acid (HA)-based hydrogels offer a promising approach for soft tissue application due to their biocompatibility, tunable mechanical properties, ability to mimic the extracellular matrix, and capacity to support cell adhesion and proliferation. In this work, bioadhesive composite hydrogels...

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Main Authors: Filipa Fernandes, Daniela Peixoto, Cátia Correia, Magda Silva, Maria C. Paiva, Natália M. Alves
Format: Article
Language:English
Published: MDPI AG 2025-02-01
Series:Nanomaterials
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Online Access:https://www.mdpi.com/2079-4991/15/4/276
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author Filipa Fernandes
Daniela Peixoto
Cátia Correia
Magda Silva
Maria C. Paiva
Natália M. Alves
author_facet Filipa Fernandes
Daniela Peixoto
Cátia Correia
Magda Silva
Maria C. Paiva
Natália M. Alves
author_sort Filipa Fernandes
collection DOAJ
description Hyaluronic acid (HA)-based hydrogels offer a promising approach for soft tissue application due to their biocompatibility, tunable mechanical properties, ability to mimic the extracellular matrix, and capacity to support cell adhesion and proliferation. In this work, bioadhesive composite hydrogels were developed by integrating graphite derivatives (EG) into a dopamine-modified HA matrix (HA-Cat), which enhances tissue adhesion through catechol groups that mimic mussel-inspired adhesion mechanisms. The EG was functionalized via 1,3-dipolar cycloaddition reaction (f-EG), that allowed the anchoring of silver nanoparticles (f-EG-Ag) and grafting of hydrocaffeic acid (f-EG-Cat) on the functionalized EG surfaces. The hydrogels were produced by oxidative crosslinking of HA-Cat under mild basic pH conditions using sodium periodate. Indirect in vitro assays using L929 fibroblast cells showed high biocompatibility and enhanced cell proliferation at optimized composite hydrogel concentrations. These findings suggest that composite hydrogels could find an application as bioactive, adhesive scaffolds for the regeneration of soft tissues, where they can facilitate localized agent delivery and integration with the host tissue.
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series Nanomaterials
spelling doaj-art-2a9e32bce9ab453a887966cd28af5ab52025-08-20T03:12:19ZengMDPI AGNanomaterials2079-49912025-02-0115427610.3390/nano15040276Mussel-Inspired Hydrogels Incorporating Graphite Derivatives for Soft Tissue RegenerationFilipa Fernandes0Daniela Peixoto1Cátia Correia2Magda Silva3Maria C. Paiva4Natália M. Alves53B’s Research Group, I3Bs—Research Institute on Biomaterials, Biodegradables and Biomimetics, University of Minho Headquarters of the European Institute of Excellence on Tissue Engineering and Regenerative Medicine, Avepark, 4805-694 Guimarães, Portugal3B’s Research Group, I3Bs—Research Institute on Biomaterials, Biodegradables and Biomimetics, University of Minho Headquarters of the European Institute of Excellence on Tissue Engineering and Regenerative Medicine, Avepark, 4805-694 Guimarães, Portugal3B’s Research Group, I3Bs—Research Institute on Biomaterials, Biodegradables and Biomimetics, University of Minho Headquarters of the European Institute of Excellence on Tissue Engineering and Regenerative Medicine, Avepark, 4805-694 Guimarães, PortugalDepartment of Polymer Engineering, Institute for Polymers and Composites, University of Minho, 4800-058 Guimarães, PortugalDepartment of Polymer Engineering, Institute for Polymers and Composites, University of Minho, 4800-058 Guimarães, Portugal3B’s Research Group, I3Bs—Research Institute on Biomaterials, Biodegradables and Biomimetics, University of Minho Headquarters of the European Institute of Excellence on Tissue Engineering and Regenerative Medicine, Avepark, 4805-694 Guimarães, PortugalHyaluronic acid (HA)-based hydrogels offer a promising approach for soft tissue application due to their biocompatibility, tunable mechanical properties, ability to mimic the extracellular matrix, and capacity to support cell adhesion and proliferation. In this work, bioadhesive composite hydrogels were developed by integrating graphite derivatives (EG) into a dopamine-modified HA matrix (HA-Cat), which enhances tissue adhesion through catechol groups that mimic mussel-inspired adhesion mechanisms. The EG was functionalized via 1,3-dipolar cycloaddition reaction (f-EG), that allowed the anchoring of silver nanoparticles (f-EG-Ag) and grafting of hydrocaffeic acid (f-EG-Cat) on the functionalized EG surfaces. The hydrogels were produced by oxidative crosslinking of HA-Cat under mild basic pH conditions using sodium periodate. Indirect in vitro assays using L929 fibroblast cells showed high biocompatibility and enhanced cell proliferation at optimized composite hydrogel concentrations. These findings suggest that composite hydrogels could find an application as bioactive, adhesive scaffolds for the regeneration of soft tissues, where they can facilitate localized agent delivery and integration with the host tissue.https://www.mdpi.com/2079-4991/15/4/276hyaluronic acidgraphitebiomimetic approach
spellingShingle Filipa Fernandes
Daniela Peixoto
Cátia Correia
Magda Silva
Maria C. Paiva
Natália M. Alves
Mussel-Inspired Hydrogels Incorporating Graphite Derivatives for Soft Tissue Regeneration
Nanomaterials
hyaluronic acid
graphite
biomimetic approach
title Mussel-Inspired Hydrogels Incorporating Graphite Derivatives for Soft Tissue Regeneration
title_full Mussel-Inspired Hydrogels Incorporating Graphite Derivatives for Soft Tissue Regeneration
title_fullStr Mussel-Inspired Hydrogels Incorporating Graphite Derivatives for Soft Tissue Regeneration
title_full_unstemmed Mussel-Inspired Hydrogels Incorporating Graphite Derivatives for Soft Tissue Regeneration
title_short Mussel-Inspired Hydrogels Incorporating Graphite Derivatives for Soft Tissue Regeneration
title_sort mussel inspired hydrogels incorporating graphite derivatives for soft tissue regeneration
topic hyaluronic acid
graphite
biomimetic approach
url https://www.mdpi.com/2079-4991/15/4/276
work_keys_str_mv AT filipafernandes musselinspiredhydrogelsincorporatinggraphitederivativesforsofttissueregeneration
AT danielapeixoto musselinspiredhydrogelsincorporatinggraphitederivativesforsofttissueregeneration
AT catiacorreia musselinspiredhydrogelsincorporatinggraphitederivativesforsofttissueregeneration
AT magdasilva musselinspiredhydrogelsincorporatinggraphitederivativesforsofttissueregeneration
AT mariacpaiva musselinspiredhydrogelsincorporatinggraphitederivativesforsofttissueregeneration
AT nataliamalves musselinspiredhydrogelsincorporatinggraphitederivativesforsofttissueregeneration