Experimental study on preparation of mine-used filling cementitious material from multi-source coal-based solid wastes

In order to reduce the cost of coal mine filling and mining, and achieve the synergistic utilization of multi-source coal based solid waste, special filling cementitious material is prepared using solid waste such as fly ash, gasification slag, and desulfurization gypsum as the main raw materials. B...

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Main Authors: Zhifei LIU, Wei WU, Zhongwei BI, Xingyu FU, Yeqing LANG, Qingli HOU, Xinguo JIA
Format: Article
Language:zho
Published: Editorial Office of Safety in Coal Mines 2024-12-01
Series:Meikuang Anquan
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Online Access:https://www.mkaqzz.com/cn/article/doi/10.13347/j.cnki.mkaq.20240615
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author Zhifei LIU
Wei WU
Zhongwei BI
Xingyu FU
Yeqing LANG
Qingli HOU
Xinguo JIA
author_facet Zhifei LIU
Wei WU
Zhongwei BI
Xingyu FU
Yeqing LANG
Qingli HOU
Xinguo JIA
author_sort Zhifei LIU
collection DOAJ
description In order to reduce the cost of coal mine filling and mining, and achieve the synergistic utilization of multi-source coal based solid waste, special filling cementitious material is prepared using solid waste such as fly ash, gasification slag, and desulfurization gypsum as the main raw materials. By conducting orthogonal test, the optimal ratio of each component in the cementitious material was determined, and the Tesser five-step method was used to study the occurrence and leaching characteristics of heavy metal elements in the cementitious material. The results show that the optimal ratio of cementitious material, fly ash∶furnace bottom ash∶gasification slag∶cement clinker∶desulfurization gypsum∶quicklime, is 39.1%∶23.4%∶15.6%∶10.9%∶4.7%∶6.3%; after curing for 7 days, the hydration products mainly exist in the form of needles and are connected by flocculent and filamentous products; the curing age reaches 28 days, and the hydration products mainly exist in the form of clumps or blocks. The hydration products bind tightly, and the net slurry strength of the cementitious material reaches 1.83 MPa and 2.44 MPa at 7 and 28 days, respectively. The filling cementitious material prepared from solid waste such as fly ash can effectively solidify heavy metals and has no risk of heavy metal pollution to the underground environment.
format Article
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institution OA Journals
issn 1003-496X
language zho
publishDate 2024-12-01
publisher Editorial Office of Safety in Coal Mines
record_format Article
series Meikuang Anquan
spelling doaj-art-29093ab6c5364c4db6ec19ff2e9819bc2025-08-20T01:58:11ZzhoEditorial Office of Safety in Coal MinesMeikuang Anquan1003-496X2024-12-015512223010.13347/j.cnki.mkaq.20240615zMKAQ20240615Experimental study on preparation of mine-used filling cementitious material from multi-source coal-based solid wastesZhifei LIU0Wei WU1Zhongwei BI2Xingyu FU3Yeqing LANG4Qingli HOU5Xinguo JIA6China Coal Research Institute, Beijing 100013, ChinaChina Coal Research Institute, Beijing 100013, ChinaChina Coal Research Institute, Beijing 100013, ChinaChina Coal Research Institute, Beijing 100013, ChinaSucun Coal Mine of Lingchuan Chong’an Group, Jincheng 048000, ChinaSucun Coal Mine of Lingchuan Chong’an Group, Jincheng 048000, ChinaChina Coal Research Institute, Beijing 100013, ChinaIn order to reduce the cost of coal mine filling and mining, and achieve the synergistic utilization of multi-source coal based solid waste, special filling cementitious material is prepared using solid waste such as fly ash, gasification slag, and desulfurization gypsum as the main raw materials. By conducting orthogonal test, the optimal ratio of each component in the cementitious material was determined, and the Tesser five-step method was used to study the occurrence and leaching characteristics of heavy metal elements in the cementitious material. The results show that the optimal ratio of cementitious material, fly ash∶furnace bottom ash∶gasification slag∶cement clinker∶desulfurization gypsum∶quicklime, is 39.1%∶23.4%∶15.6%∶10.9%∶4.7%∶6.3%; after curing for 7 days, the hydration products mainly exist in the form of needles and are connected by flocculent and filamentous products; the curing age reaches 28 days, and the hydration products mainly exist in the form of clumps or blocks. The hydration products bind tightly, and the net slurry strength of the cementitious material reaches 1.83 MPa and 2.44 MPa at 7 and 28 days, respectively. The filling cementitious material prepared from solid waste such as fly ash can effectively solidify heavy metals and has no risk of heavy metal pollution to the underground environment.https://www.mkaqzz.com/cn/article/doi/10.13347/j.cnki.mkaq.20240615cementitious materialcoal-based solid wastefilling miningheavy metal elementorthogonal test
spellingShingle Zhifei LIU
Wei WU
Zhongwei BI
Xingyu FU
Yeqing LANG
Qingli HOU
Xinguo JIA
Experimental study on preparation of mine-used filling cementitious material from multi-source coal-based solid wastes
Meikuang Anquan
cementitious material
coal-based solid waste
filling mining
heavy metal element
orthogonal test
title Experimental study on preparation of mine-used filling cementitious material from multi-source coal-based solid wastes
title_full Experimental study on preparation of mine-used filling cementitious material from multi-source coal-based solid wastes
title_fullStr Experimental study on preparation of mine-used filling cementitious material from multi-source coal-based solid wastes
title_full_unstemmed Experimental study on preparation of mine-used filling cementitious material from multi-source coal-based solid wastes
title_short Experimental study on preparation of mine-used filling cementitious material from multi-source coal-based solid wastes
title_sort experimental study on preparation of mine used filling cementitious material from multi source coal based solid wastes
topic cementitious material
coal-based solid waste
filling mining
heavy metal element
orthogonal test
url https://www.mkaqzz.com/cn/article/doi/10.13347/j.cnki.mkaq.20240615
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