Achieving the synergistic strength and wear resistance in TiC/Fe matrix composites by spark plasma sintering and hot isostatic pressing

The iron matrix composites reinforced with titanium carbide particles (TiC/Fe MCs) with high strength and excellent wear resistance had been fabricated through spark plasma sintering (SPS) and hot isostatic pressing (HIP) post-treatment in this study. The effects of different HIP temperatures on the...

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Main Authors: Chuan Wang, Yi Xiao, Wanpeng Zhang, Tianwen Zhao, Huiqiao Du, Yong Li
Format: Article
Language:English
Published: Elsevier 2025-05-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425011202
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author Chuan Wang
Yi Xiao
Wanpeng Zhang
Tianwen Zhao
Huiqiao Du
Yong Li
author_facet Chuan Wang
Yi Xiao
Wanpeng Zhang
Tianwen Zhao
Huiqiao Du
Yong Li
author_sort Chuan Wang
collection DOAJ
description The iron matrix composites reinforced with titanium carbide particles (TiC/Fe MCs) with high strength and excellent wear resistance had been fabricated through spark plasma sintering (SPS) and hot isostatic pressing (HIP) post-treatment in this study. The effects of different HIP temperatures on the porosity, microstructure, interface, and mechanical properties of the composites had been systematically investigated. The results indicated that the microstructure of both the composites fabricated by SPS and HIP post-treatment consists of TiC, FeCr, (Ti, Mo)C, Al2Mo3C, and Cr21Mo2C6 phases. Under HIP post-treatment conditions at 1410 °C, the composite exhibited a hardness of 628 HV0.5, a bending strength of 1006 MPa, a coefficient of friction (COF) of 0.56, and a wear rate of only 4.6 × 10−5 mm3/m. Compared to samples fabricated by SPS alone, the porosity decreased from 3.85 % to 0.08 %, the hardness increased by 5.5 %, the bending strength improved by 52.0 %, the COF decreased by 24.3 %, and the wear rate decreased by 61.7 %. After SPS process, the fracture surfaces of the samples exhibited a higher prevalence of intergranular fracture, whereas transgranular fracture was predominant following HIP post-treatment at 1250 °C. The primary strengthening mechanisms of the composite included fine-grain strengthening and enhanced densification. During friction and wear testing, fatigue wear, oxidative wear, and plastic deformation predominantly affected the SPS samples and the samples treated with HIP post-treatment below 1250 °C. However, abrasive wear, plastic deformation, and oxidative wear primarily influenced the samples with HIP post-treatment above 1250 °C.
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publisher Elsevier
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spelling doaj-art-28e244f0c0f441d5a1730ffa46272c062025-08-20T02:15:58ZengElsevierJournal of Materials Research and Technology2238-78542025-05-01367228724310.1016/j.jmrt.2025.04.299Achieving the synergistic strength and wear resistance in TiC/Fe matrix composites by spark plasma sintering and hot isostatic pressingChuan Wang0Yi Xiao1Wanpeng Zhang2Tianwen Zhao3Huiqiao Du4Yong Li5School of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, ChinaSchool of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, China; Corresponding author.School of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, ChinaSchool of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, ChinaSchool of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, ChinaSchool of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, China; National Key Laboratory of Precision Welding & Joining of Materials and Structures, Harbin, 150001, China; Corresponding author. School of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, China.The iron matrix composites reinforced with titanium carbide particles (TiC/Fe MCs) with high strength and excellent wear resistance had been fabricated through spark plasma sintering (SPS) and hot isostatic pressing (HIP) post-treatment in this study. The effects of different HIP temperatures on the porosity, microstructure, interface, and mechanical properties of the composites had been systematically investigated. The results indicated that the microstructure of both the composites fabricated by SPS and HIP post-treatment consists of TiC, FeCr, (Ti, Mo)C, Al2Mo3C, and Cr21Mo2C6 phases. Under HIP post-treatment conditions at 1410 °C, the composite exhibited a hardness of 628 HV0.5, a bending strength of 1006 MPa, a coefficient of friction (COF) of 0.56, and a wear rate of only 4.6 × 10−5 mm3/m. Compared to samples fabricated by SPS alone, the porosity decreased from 3.85 % to 0.08 %, the hardness increased by 5.5 %, the bending strength improved by 52.0 %, the COF decreased by 24.3 %, and the wear rate decreased by 61.7 %. After SPS process, the fracture surfaces of the samples exhibited a higher prevalence of intergranular fracture, whereas transgranular fracture was predominant following HIP post-treatment at 1250 °C. The primary strengthening mechanisms of the composite included fine-grain strengthening and enhanced densification. During friction and wear testing, fatigue wear, oxidative wear, and plastic deformation predominantly affected the SPS samples and the samples treated with HIP post-treatment below 1250 °C. However, abrasive wear, plastic deformation, and oxidative wear primarily influenced the samples with HIP post-treatment above 1250 °C.http://www.sciencedirect.com/science/article/pii/S2238785425011202TiC/Fe matrix compositesSPSHIPMechanical propertiesWear resistance
spellingShingle Chuan Wang
Yi Xiao
Wanpeng Zhang
Tianwen Zhao
Huiqiao Du
Yong Li
Achieving the synergistic strength and wear resistance in TiC/Fe matrix composites by spark plasma sintering and hot isostatic pressing
Journal of Materials Research and Technology
TiC/Fe matrix composites
SPS
HIP
Mechanical properties
Wear resistance
title Achieving the synergistic strength and wear resistance in TiC/Fe matrix composites by spark plasma sintering and hot isostatic pressing
title_full Achieving the synergistic strength and wear resistance in TiC/Fe matrix composites by spark plasma sintering and hot isostatic pressing
title_fullStr Achieving the synergistic strength and wear resistance in TiC/Fe matrix composites by spark plasma sintering and hot isostatic pressing
title_full_unstemmed Achieving the synergistic strength and wear resistance in TiC/Fe matrix composites by spark plasma sintering and hot isostatic pressing
title_short Achieving the synergistic strength and wear resistance in TiC/Fe matrix composites by spark plasma sintering and hot isostatic pressing
title_sort achieving the synergistic strength and wear resistance in tic fe matrix composites by spark plasma sintering and hot isostatic pressing
topic TiC/Fe matrix composites
SPS
HIP
Mechanical properties
Wear resistance
url http://www.sciencedirect.com/science/article/pii/S2238785425011202
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