Microstructural Characterization of Martensitic Stainless Steel Blades Manufactured by Directed Energy Deposition (DED)

This study explores the feasibility of manufacturing martensitic stainless steel turbine blades via a directed energy deposition (DED) process using a powder precursor. Five different blade geometries were fabricated using AISI 431 L martensitic stainless steel deposited onto an AISI 304 L austeniti...

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Main Authors: Caroline Cristine de Andrade Ferreira, Rafael Humberto Mota de Siqueira, Johan Grass Nuñez, Fábio Edson Mariani, Reginaldo Teixeira Coelho, Daolun Chen, Milton Sérgio Fernandes de Lima
Format: Article
Language:English
Published: MDPI AG 2025-05-01
Series:Metals
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Online Access:https://www.mdpi.com/2075-4701/15/6/612
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author Caroline Cristine de Andrade Ferreira
Rafael Humberto Mota de Siqueira
Johan Grass Nuñez
Fábio Edson Mariani
Reginaldo Teixeira Coelho
Daolun Chen
Milton Sérgio Fernandes de Lima
author_facet Caroline Cristine de Andrade Ferreira
Rafael Humberto Mota de Siqueira
Johan Grass Nuñez
Fábio Edson Mariani
Reginaldo Teixeira Coelho
Daolun Chen
Milton Sérgio Fernandes de Lima
author_sort Caroline Cristine de Andrade Ferreira
collection DOAJ
description This study explores the feasibility of manufacturing martensitic stainless steel turbine blades via a directed energy deposition (DED) process using a powder precursor. Five different blade geometries were fabricated using AISI 431 L martensitic stainless steel deposited onto an AISI 304 L austenitic stainless steel substrate. The produced components were characterized in terms of microstructure, surface roughness, porosity, hardness, and residual stresses in both the as-processed condition and after heat treatment at 260 and 593 °C. Optical and scanning electron microscopy (SEM) analyses revealed a predominantly martensitic microstructure with well-defined grain boundaries. Heat treatment influenced the phase distribution and grain size, but did not have a significant impact on the surface roughness or modulus of elasticity. Tomographic assessments confirmed the absence of aligned or coalesced pores, which are critical sites for crack initiation. Residual stress analysis indicated the presence of compressive stresses in all blade geometries, which were effectively relieved by heat treatment. In addition, salt spray corrosion tests demonstrated that the corrosion resistance of the manufactured blades was similar to that of the base material. These findings suggest that DED is a viable technique for producing and repairing turbine blades, providing structural integrity and mechanical properties suitable for high-performance applications.
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spelling doaj-art-286be11764ec4ed6bbeec2631bf9215c2025-08-20T03:27:35ZengMDPI AGMetals2075-47012025-05-0115661210.3390/met15060612Microstructural Characterization of Martensitic Stainless Steel Blades Manufactured by Directed Energy Deposition (DED)Caroline Cristine de Andrade Ferreira0Rafael Humberto Mota de Siqueira1Johan Grass Nuñez2Fábio Edson Mariani3Reginaldo Teixeira Coelho4Daolun Chen5Milton Sérgio Fernandes de Lima6Graduate Program in Space Sciences and Technologies, Technological Institute of Aeronautics, Praca Eduardo Gomes 50, Sao Jose dos Campos 12228-901, SP, BrazilPhotonics Division, Institute for Advanced Studies, Trevo Amarante 1, Sao Jose dos Campos 12228-001, SP, BrazilLaboratory for Advanced Process and Sustainability, Department of Production Engineering, School of Engineering at Sao Carlos, University of Sao Paulo, Sao Carlos 13566-590, SP, BrazilLaboratory for Advanced Process and Sustainability, Department of Production Engineering, School of Engineering at Sao Carlos, University of Sao Paulo, Sao Carlos 13566-590, SP, BrazilLaboratory for Advanced Process and Sustainability, Department of Production Engineering, School of Engineering at Sao Carlos, University of Sao Paulo, Sao Carlos 13566-590, SP, BrazilDepartment of Mechanical, Industrial and Mechatronics Engineering, Toronto Metropolitan University, Toronto, ON M5B 2K3, CanadaGraduate Program in Space Sciences and Technologies, Technological Institute of Aeronautics, Praca Eduardo Gomes 50, Sao Jose dos Campos 12228-901, SP, BrazilThis study explores the feasibility of manufacturing martensitic stainless steel turbine blades via a directed energy deposition (DED) process using a powder precursor. Five different blade geometries were fabricated using AISI 431 L martensitic stainless steel deposited onto an AISI 304 L austenitic stainless steel substrate. The produced components were characterized in terms of microstructure, surface roughness, porosity, hardness, and residual stresses in both the as-processed condition and after heat treatment at 260 and 593 °C. Optical and scanning electron microscopy (SEM) analyses revealed a predominantly martensitic microstructure with well-defined grain boundaries. Heat treatment influenced the phase distribution and grain size, but did not have a significant impact on the surface roughness or modulus of elasticity. Tomographic assessments confirmed the absence of aligned or coalesced pores, which are critical sites for crack initiation. Residual stress analysis indicated the presence of compressive stresses in all blade geometries, which were effectively relieved by heat treatment. In addition, salt spray corrosion tests demonstrated that the corrosion resistance of the manufactured blades was similar to that of the base material. These findings suggest that DED is a viable technique for producing and repairing turbine blades, providing structural integrity and mechanical properties suitable for high-performance applications.https://www.mdpi.com/2075-4701/15/6/612directed energy depositionmartensitic stainless steelmicrostructural characterizationturbine blades
spellingShingle Caroline Cristine de Andrade Ferreira
Rafael Humberto Mota de Siqueira
Johan Grass Nuñez
Fábio Edson Mariani
Reginaldo Teixeira Coelho
Daolun Chen
Milton Sérgio Fernandes de Lima
Microstructural Characterization of Martensitic Stainless Steel Blades Manufactured by Directed Energy Deposition (DED)
Metals
directed energy deposition
martensitic stainless steel
microstructural characterization
turbine blades
title Microstructural Characterization of Martensitic Stainless Steel Blades Manufactured by Directed Energy Deposition (DED)
title_full Microstructural Characterization of Martensitic Stainless Steel Blades Manufactured by Directed Energy Deposition (DED)
title_fullStr Microstructural Characterization of Martensitic Stainless Steel Blades Manufactured by Directed Energy Deposition (DED)
title_full_unstemmed Microstructural Characterization of Martensitic Stainless Steel Blades Manufactured by Directed Energy Deposition (DED)
title_short Microstructural Characterization of Martensitic Stainless Steel Blades Manufactured by Directed Energy Deposition (DED)
title_sort microstructural characterization of martensitic stainless steel blades manufactured by directed energy deposition ded
topic directed energy deposition
martensitic stainless steel
microstructural characterization
turbine blades
url https://www.mdpi.com/2075-4701/15/6/612
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