Reversible biobased adhesives enable closed-loop engineered composites

Abstract Ubiquitous synthetic resin adhesives based on petrochemical brings environmental burdens and health concerns. Many researchers have been focused on developing biomass-derived alternatives, and reported many strong-adhesion products with high cohesive density. However, the stabilized structu...

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Main Authors: Jin Lv, Daxin Zhang, Xinkai Li, Yinggang Miao, Yuyan Wang, Ying Wang, Xinxing Zhang
Format: Article
Language:English
Published: Nature Portfolio 2025-08-01
Series:Nature Communications
Online Access:https://doi.org/10.1038/s41467-025-62917-1
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author Jin Lv
Daxin Zhang
Xinkai Li
Yinggang Miao
Yuyan Wang
Ying Wang
Xinxing Zhang
author_facet Jin Lv
Daxin Zhang
Xinkai Li
Yinggang Miao
Yuyan Wang
Ying Wang
Xinxing Zhang
author_sort Jin Lv
collection DOAJ
description Abstract Ubiquitous synthetic resin adhesives based on petrochemical brings environmental burdens and health concerns. Many researchers have been focused on developing biomass-derived alternatives, and reported many strong-adhesion products with high cohesive density. However, the stabilized structure-dependent adhesion contributes to greater difficulty in recycling, especially hetero-layered composites. Here, a supramolecularly connected nanoconfined network strategy is proposed for ultra-strong yet switchable biobased adhesives, where cellulose nanoconfinement phases takes up 36.5–46.3 wt%. Dependent on thermally responsive disulfide bond, resulting adhesives achieve both excellent adhesion strength (6.02 MPa) that can support a 65 kg weight with 4 cm2, and instant thermo-responsive detachment with a high switching ratio over 600 (debonding adhesion ≈0 MPa, response time ≤ 10 s). Under the alternating temperature, adhesive-based composites can be disassembled into different categories and fully recycled through the destruction of dynamic crosslinked network. The full life cycle impact assessment shows this strategy is able to avoid the inherent environmental (about 7.52 * 102 PAF m3 d/kgemitted) and health (about 2.04 * 10−4 cases/kgemitted) burden. This work establishes a paradigm for closed-loop engineered composites by the substantive breakthrough of green intelligent adhesives, providing ways to alleviate environmental stress.
format Article
id doaj-art-2849015b86684dec8ca93cdd387780d9
institution Kabale University
issn 2041-1723
language English
publishDate 2025-08-01
publisher Nature Portfolio
record_format Article
series Nature Communications
spelling doaj-art-2849015b86684dec8ca93cdd387780d92025-08-24T11:39:41ZengNature PortfolioNature Communications2041-17232025-08-0116111210.1038/s41467-025-62917-1Reversible biobased adhesives enable closed-loop engineered compositesJin Lv0Daxin Zhang1Xinkai Li2Yinggang Miao3Yuyan Wang4Ying Wang5Xinxing Zhang6National Key Laboratory of Advanced Polymer Materials, Polymer Research Institute, Sichuan UniversityShaanxi Key Laboratory of Impact Dynamics and its Engineering Application, School of Aeronautics, Northwestern Polytechnical UniversityNational Key Laboratory of Advanced Polymer Materials, Polymer Research Institute, Sichuan UniversityShaanxi Key Laboratory of Impact Dynamics and its Engineering Application, School of Aeronautics, Northwestern Polytechnical UniversityMax Planck Institute for Polymer ResearchCollege of Electrical Engineering, Sichuan UniversityNational Key Laboratory of Advanced Polymer Materials, Polymer Research Institute, Sichuan UniversityAbstract Ubiquitous synthetic resin adhesives based on petrochemical brings environmental burdens and health concerns. Many researchers have been focused on developing biomass-derived alternatives, and reported many strong-adhesion products with high cohesive density. However, the stabilized structure-dependent adhesion contributes to greater difficulty in recycling, especially hetero-layered composites. Here, a supramolecularly connected nanoconfined network strategy is proposed for ultra-strong yet switchable biobased adhesives, where cellulose nanoconfinement phases takes up 36.5–46.3 wt%. Dependent on thermally responsive disulfide bond, resulting adhesives achieve both excellent adhesion strength (6.02 MPa) that can support a 65 kg weight with 4 cm2, and instant thermo-responsive detachment with a high switching ratio over 600 (debonding adhesion ≈0 MPa, response time ≤ 10 s). Under the alternating temperature, adhesive-based composites can be disassembled into different categories and fully recycled through the destruction of dynamic crosslinked network. The full life cycle impact assessment shows this strategy is able to avoid the inherent environmental (about 7.52 * 102 PAF m3 d/kgemitted) and health (about 2.04 * 10−4 cases/kgemitted) burden. This work establishes a paradigm for closed-loop engineered composites by the substantive breakthrough of green intelligent adhesives, providing ways to alleviate environmental stress.https://doi.org/10.1038/s41467-025-62917-1
spellingShingle Jin Lv
Daxin Zhang
Xinkai Li
Yinggang Miao
Yuyan Wang
Ying Wang
Xinxing Zhang
Reversible biobased adhesives enable closed-loop engineered composites
Nature Communications
title Reversible biobased adhesives enable closed-loop engineered composites
title_full Reversible biobased adhesives enable closed-loop engineered composites
title_fullStr Reversible biobased adhesives enable closed-loop engineered composites
title_full_unstemmed Reversible biobased adhesives enable closed-loop engineered composites
title_short Reversible biobased adhesives enable closed-loop engineered composites
title_sort reversible biobased adhesives enable closed loop engineered composites
url https://doi.org/10.1038/s41467-025-62917-1
work_keys_str_mv AT jinlv reversiblebiobasedadhesivesenableclosedloopengineeredcomposites
AT daxinzhang reversiblebiobasedadhesivesenableclosedloopengineeredcomposites
AT xinkaili reversiblebiobasedadhesivesenableclosedloopengineeredcomposites
AT yinggangmiao reversiblebiobasedadhesivesenableclosedloopengineeredcomposites
AT yuyanwang reversiblebiobasedadhesivesenableclosedloopengineeredcomposites
AT yingwang reversiblebiobasedadhesivesenableclosedloopengineeredcomposites
AT xinxingzhang reversiblebiobasedadhesivesenableclosedloopengineeredcomposites