Trimethylamine Gas Sensor Based on Electrospun In<sub>2</sub>O<sub>3</sub> Nanowires with Different Grain Sizes for Fish Freshness Monitoring

Seafood, especially marine fish, is highly prone to spoilage during processing, transportation, and storage. It releases pungent trimethylamine (TMA) gas, which severely affects food quality and safety. Metal–oxide–semiconductor (MOS) gas sensors for TMA detection offer a rapid, convenient, and accu...

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Main Authors: Xiangrui Dong, Bo Zhang, Mengyao Shen, Qi Lu, Hao Shen, Yi Ni, Yuechen Liu, Haitao Song
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Chemosensors
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Online Access:https://www.mdpi.com/2227-9040/13/6/218
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author Xiangrui Dong
Bo Zhang
Mengyao Shen
Qi Lu
Hao Shen
Yi Ni
Yuechen Liu
Haitao Song
author_facet Xiangrui Dong
Bo Zhang
Mengyao Shen
Qi Lu
Hao Shen
Yi Ni
Yuechen Liu
Haitao Song
author_sort Xiangrui Dong
collection DOAJ
description Seafood, especially marine fish, is highly prone to spoilage during processing, transportation, and storage. It releases pungent trimethylamine (TMA) gas, which severely affects food quality and safety. Metal–oxide–semiconductor (MOS) gas sensors for TMA detection offer a rapid, convenient, and accurate method for assessing fish freshness. Indium oxide (In<sub>2</sub>O<sub>3</sub>) has shown potential as an effective sensing material for the detection of TMA. In this work, one-dimensional In<sub>2</sub>O<sub>3</sub> nanowires with different grain sizes and levels of crystallinity were synthetized using the electrospinning technique and underwent different thermal calcination processes. Gas-sensing tests showed that the In<sub>2</sub>O<sub>3</sub>–3 °C/min–500 °C gas sensor exhibited an outstanding performance, including a high response (R<sub>a</sub>/R<sub>g</sub> = 47.0) to 100 ppm TMA, a short response time (6 s), a low limit of detection (LOD, 0.0392 ppm), and an excellent long-term stability. Furthermore, the sensor showed promising experimental results in monitoring the freshness of <i>Larimichthys crocea</i> (<i>L. crocea</i>). By analyzing the relationship between the grain size and crystallinity of the In<sub>2</sub>O<sub>3</sub> samples, a mechanism for the enhanced gas-sensing performance was proposed. This work provides a novel strategy for designing and fabricating gas sensors for TMA detection and highlights their potential for broad applications in real-time fish freshness monitoring.
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institution Kabale University
issn 2227-9040
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publishDate 2025-06-01
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series Chemosensors
spelling doaj-art-27743c68d2fa477ea64d02cf013763e52025-08-20T03:26:26ZengMDPI AGChemosensors2227-90402025-06-0113621810.3390/chemosensors13060218Trimethylamine Gas Sensor Based on Electrospun In<sub>2</sub>O<sub>3</sub> Nanowires with Different Grain Sizes for Fish Freshness MonitoringXiangrui Dong0Bo Zhang1Mengyao Shen2Qi Lu3Hao Shen4Yi Ni5Yuechen Liu6Haitao Song7Engineering Research Center of IoT Technology Applications (Ministry of Education), School of Integrated Circuits, Jiangnan University, Wuxi 214122, ChinaEngineering Research Center of IoT Technology Applications (Ministry of Education), School of Integrated Circuits, Jiangnan University, Wuxi 214122, ChinaEngineering Research Center of IoT Technology Applications (Ministry of Education), School of Integrated Circuits, Jiangnan University, Wuxi 214122, ChinaEngineering Research Center of IoT Technology Applications (Ministry of Education), School of Integrated Circuits, Jiangnan University, Wuxi 214122, ChinaShanghai Artificial Intelligence Research Institute Co., Ltd., Shanghai 200240, ChinaEngineering Research Center of IoT Technology Applications (Ministry of Education), School of Integrated Circuits, Jiangnan University, Wuxi 214122, ChinaArtificial Intelligence Technology Center, Institute of Translational Medicine, Shanghai Jiao Tong University, Shanghai 200240, ChinaShanghai Artificial Intelligence Research Institute Co., Ltd., Shanghai 200240, ChinaSeafood, especially marine fish, is highly prone to spoilage during processing, transportation, and storage. It releases pungent trimethylamine (TMA) gas, which severely affects food quality and safety. Metal–oxide–semiconductor (MOS) gas sensors for TMA detection offer a rapid, convenient, and accurate method for assessing fish freshness. Indium oxide (In<sub>2</sub>O<sub>3</sub>) has shown potential as an effective sensing material for the detection of TMA. In this work, one-dimensional In<sub>2</sub>O<sub>3</sub> nanowires with different grain sizes and levels of crystallinity were synthetized using the electrospinning technique and underwent different thermal calcination processes. Gas-sensing tests showed that the In<sub>2</sub>O<sub>3</sub>–3 °C/min–500 °C gas sensor exhibited an outstanding performance, including a high response (R<sub>a</sub>/R<sub>g</sub> = 47.0) to 100 ppm TMA, a short response time (6 s), a low limit of detection (LOD, 0.0392 ppm), and an excellent long-term stability. Furthermore, the sensor showed promising experimental results in monitoring the freshness of <i>Larimichthys crocea</i> (<i>L. crocea</i>). By analyzing the relationship between the grain size and crystallinity of the In<sub>2</sub>O<sub>3</sub> samples, a mechanism for the enhanced gas-sensing performance was proposed. This work provides a novel strategy for designing and fabricating gas sensors for TMA detection and highlights their potential for broad applications in real-time fish freshness monitoring.https://www.mdpi.com/2227-9040/13/6/218In<sub>2</sub>O<sub>3</sub>electrospinningTMA gas sensorgrain sizefish freshness monitoring
spellingShingle Xiangrui Dong
Bo Zhang
Mengyao Shen
Qi Lu
Hao Shen
Yi Ni
Yuechen Liu
Haitao Song
Trimethylamine Gas Sensor Based on Electrospun In<sub>2</sub>O<sub>3</sub> Nanowires with Different Grain Sizes for Fish Freshness Monitoring
Chemosensors
In<sub>2</sub>O<sub>3</sub>
electrospinning
TMA gas sensor
grain size
fish freshness monitoring
title Trimethylamine Gas Sensor Based on Electrospun In<sub>2</sub>O<sub>3</sub> Nanowires with Different Grain Sizes for Fish Freshness Monitoring
title_full Trimethylamine Gas Sensor Based on Electrospun In<sub>2</sub>O<sub>3</sub> Nanowires with Different Grain Sizes for Fish Freshness Monitoring
title_fullStr Trimethylamine Gas Sensor Based on Electrospun In<sub>2</sub>O<sub>3</sub> Nanowires with Different Grain Sizes for Fish Freshness Monitoring
title_full_unstemmed Trimethylamine Gas Sensor Based on Electrospun In<sub>2</sub>O<sub>3</sub> Nanowires with Different Grain Sizes for Fish Freshness Monitoring
title_short Trimethylamine Gas Sensor Based on Electrospun In<sub>2</sub>O<sub>3</sub> Nanowires with Different Grain Sizes for Fish Freshness Monitoring
title_sort trimethylamine gas sensor based on electrospun in sub 2 sub o sub 3 sub nanowires with different grain sizes for fish freshness monitoring
topic In<sub>2</sub>O<sub>3</sub>
electrospinning
TMA gas sensor
grain size
fish freshness monitoring
url https://www.mdpi.com/2227-9040/13/6/218
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