Hybrid Adhesive Hydrogel Patch Containing Genipin-Crosslinked Gelatin–Hyaluronic Acid for Future Use in Atopic Dermatitis

Hydrogel patches have gained significant attention in wound healing applications as they are similar to hydrogel dressings due to their moisture-retentive properties, biocompatibility, and ability to promote tissue regeneration. In this study, gelatin-based hydrogels crosslinked with genipin and inc...

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Main Authors: Nurul Ain Zawawi, Manira Maarof, Nur Izzah Md Fadilah, Daniel Looi Qi Hao, Yasuhiko Tabata, Mh Busra Fauzi
Format: Article
Language:English
Published: MDPI AG 2025-05-01
Series:Journal of Functional Biomaterials
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Online Access:https://www.mdpi.com/2079-4983/16/6/195
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author Nurul Ain Zawawi
Manira Maarof
Nur Izzah Md Fadilah
Daniel Looi Qi Hao
Yasuhiko Tabata
Mh Busra Fauzi
author_facet Nurul Ain Zawawi
Manira Maarof
Nur Izzah Md Fadilah
Daniel Looi Qi Hao
Yasuhiko Tabata
Mh Busra Fauzi
author_sort Nurul Ain Zawawi
collection DOAJ
description Hydrogel patches have gained significant attention in wound healing applications as they are similar to hydrogel dressings due to their moisture-retentive properties, biocompatibility, and ability to promote tissue regeneration. In this study, gelatin-based hydrogels crosslinked with genipin and incorporated with hyaluronic acid (HA) were developed to enhance mechanical stability, swelling behavior, and structural integrity. Fourier transform infrared (FTIR), thermogravimetric (TGA), and energy-dispersive X-ray (EDX) analyses were conducted and confirmed successful crosslinking and good thermal stability, ensuring hydrogel durability under physiological conditions. The optimized hydrogel (GE_HA_GNP) exhibited a sufficient water vapor transmission rate (WVTR), swelling ratio, and contact angle, allowing for effective wound exudate absorption and hydration maintenance, which is essential for accelerated healing. The findings demonstrate that the crosslinked hydrogels were able to maintain a WVTR of 500 to 1500 gm<sup>−2</sup> day<sup>−1</sup>, a contact angle of >40°, and a swelling ratio of 700–1000%. The combination of genipin as a crosslinker and the addition of HA significantly improved the mechanical properties and biocompatibility of the hydrogels, making them promising candidates for an alternative treatment for atopic dermatitis and a potential wound dress-ing. Furthermore, the hydrogel patches show potential for future drug delivery appli-cations, with further studies required to evaluate their antimicrobial properties and long-term clinical performance.
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institution Kabale University
issn 2079-4983
language English
publishDate 2025-05-01
publisher MDPI AG
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series Journal of Functional Biomaterials
spelling doaj-art-27660ab73c6244ef841661ea0af8ddbd2025-08-20T03:27:14ZengMDPI AGJournal of Functional Biomaterials2079-49832025-05-0116619510.3390/jfb16060195Hybrid Adhesive Hydrogel Patch Containing Genipin-Crosslinked Gelatin–Hyaluronic Acid for Future Use in Atopic DermatitisNurul Ain Zawawi0Manira Maarof1Nur Izzah Md Fadilah2Daniel Looi Qi Hao3Yasuhiko Tabata4Mh Busra Fauzi5Department of Tissue Engineering & Regenerative Medicine, Faculty of Medicine, Universiti Kebangsaan Malaysia, Cheras, Kuala Lumpur 56000, MalaysiaDepartment of Tissue Engineering & Regenerative Medicine, Faculty of Medicine, Universiti Kebangsaan Malaysia, Cheras, Kuala Lumpur 56000, MalaysiaDepartment of Tissue Engineering & Regenerative Medicine, Faculty of Medicine, Universiti Kebangsaan Malaysia, Cheras, Kuala Lumpur 56000, MalaysiaMy Cytohealth Sdn Bhd, Hive 5, Taman Teknologi, MRANTI, Bukit Jalil, Kuala Lumpur 57000, MalaysiaCell Biotechnology Group, Department of Plastic and Reconstructive Surgery, Graduate School of Medicine, Kyoto University, South Research Bldg. No.1 (Institute for Life and Medical Sciences) 53 Kawara-cho Shogoin, Kyoto 606-8507, Sakyo-ku, JapanDepartment of Tissue Engineering & Regenerative Medicine, Faculty of Medicine, Universiti Kebangsaan Malaysia, Cheras, Kuala Lumpur 56000, MalaysiaHydrogel patches have gained significant attention in wound healing applications as they are similar to hydrogel dressings due to their moisture-retentive properties, biocompatibility, and ability to promote tissue regeneration. In this study, gelatin-based hydrogels crosslinked with genipin and incorporated with hyaluronic acid (HA) were developed to enhance mechanical stability, swelling behavior, and structural integrity. Fourier transform infrared (FTIR), thermogravimetric (TGA), and energy-dispersive X-ray (EDX) analyses were conducted and confirmed successful crosslinking and good thermal stability, ensuring hydrogel durability under physiological conditions. The optimized hydrogel (GE_HA_GNP) exhibited a sufficient water vapor transmission rate (WVTR), swelling ratio, and contact angle, allowing for effective wound exudate absorption and hydration maintenance, which is essential for accelerated healing. The findings demonstrate that the crosslinked hydrogels were able to maintain a WVTR of 500 to 1500 gm<sup>−2</sup> day<sup>−1</sup>, a contact angle of >40°, and a swelling ratio of 700–1000%. The combination of genipin as a crosslinker and the addition of HA significantly improved the mechanical properties and biocompatibility of the hydrogels, making them promising candidates for an alternative treatment for atopic dermatitis and a potential wound dress-ing. Furthermore, the hydrogel patches show potential for future drug delivery appli-cations, with further studies required to evaluate their antimicrobial properties and long-term clinical performance.https://www.mdpi.com/2079-4983/16/6/195hydrogel patchnatural biomaterialgelatinhyaluronic acidgenipinatopic dermatitis
spellingShingle Nurul Ain Zawawi
Manira Maarof
Nur Izzah Md Fadilah
Daniel Looi Qi Hao
Yasuhiko Tabata
Mh Busra Fauzi
Hybrid Adhesive Hydrogel Patch Containing Genipin-Crosslinked Gelatin–Hyaluronic Acid for Future Use in Atopic Dermatitis
Journal of Functional Biomaterials
hydrogel patch
natural biomaterial
gelatin
hyaluronic acid
genipin
atopic dermatitis
title Hybrid Adhesive Hydrogel Patch Containing Genipin-Crosslinked Gelatin–Hyaluronic Acid for Future Use in Atopic Dermatitis
title_full Hybrid Adhesive Hydrogel Patch Containing Genipin-Crosslinked Gelatin–Hyaluronic Acid for Future Use in Atopic Dermatitis
title_fullStr Hybrid Adhesive Hydrogel Patch Containing Genipin-Crosslinked Gelatin–Hyaluronic Acid for Future Use in Atopic Dermatitis
title_full_unstemmed Hybrid Adhesive Hydrogel Patch Containing Genipin-Crosslinked Gelatin–Hyaluronic Acid for Future Use in Atopic Dermatitis
title_short Hybrid Adhesive Hydrogel Patch Containing Genipin-Crosslinked Gelatin–Hyaluronic Acid for Future Use in Atopic Dermatitis
title_sort hybrid adhesive hydrogel patch containing genipin crosslinked gelatin hyaluronic acid for future use in atopic dermatitis
topic hydrogel patch
natural biomaterial
gelatin
hyaluronic acid
genipin
atopic dermatitis
url https://www.mdpi.com/2079-4983/16/6/195
work_keys_str_mv AT nurulainzawawi hybridadhesivehydrogelpatchcontaininggenipincrosslinkedgelatinhyaluronicacidforfutureuseinatopicdermatitis
AT maniramaarof hybridadhesivehydrogelpatchcontaininggenipincrosslinkedgelatinhyaluronicacidforfutureuseinatopicdermatitis
AT nurizzahmdfadilah hybridadhesivehydrogelpatchcontaininggenipincrosslinkedgelatinhyaluronicacidforfutureuseinatopicdermatitis
AT daniellooiqihao hybridadhesivehydrogelpatchcontaininggenipincrosslinkedgelatinhyaluronicacidforfutureuseinatopicdermatitis
AT yasuhikotabata hybridadhesivehydrogelpatchcontaininggenipincrosslinkedgelatinhyaluronicacidforfutureuseinatopicdermatitis
AT mhbusrafauzi hybridadhesivehydrogelpatchcontaininggenipincrosslinkedgelatinhyaluronicacidforfutureuseinatopicdermatitis