Application of a number of physical and chemical analysis methods the assessment of a multicomponent sample composition of natural water

The authors present experimental data on the development of a special sample in the form of a dispersed material that simulates the mineral macro-component composition of natural surface water. The results of the study obtained by a number of physico-chemical analysis methods were compared to determ...

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Main Authors: L. V. Trubacheva, S. Yu. Lohaninа, T. I. Belova
Format: Article
Language:Russian
Published: Ural Research Institute of Metrology 2020-09-01
Series:Стандартные образцы
Subjects:
Online Access:https://www.rmjournal.ru/jour/article/view/247
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author L. V. Trubacheva
S. Yu. Lohaninа
T. I. Belova
author_facet L. V. Trubacheva
S. Yu. Lohaninа
T. I. Belova
author_sort L. V. Trubacheva
collection DOAJ
description The authors present experimental data on the development of a special sample in the form of a dispersed material that simulates the mineral macro-component composition of natural surface water. The results of the study obtained by a number of physico-chemical analysis methods were compared to determine the mass concentration of the micro-component - manganese (II) in the sample. Determination of the mass concentration of manganese (II) was carried out by the methods of spectrophotometry for PND F 14.1:2.61, x-ray fluorometry for PND F 14.1:2:4.130, inversion voltammetry for PND F 14.1:24.217.Procedures for establishing the metrological characteristics of a special sample to control the accuracy of the results of measurements of the mass concentration of manganese (II) using a number of physicо-chemical analysis methods have been carried out.A number of advantages and disadvantages of certified measurement methods that are widely used in chemical laboratories for determining the content of manganese in natural surface water are noted. The necessity of carrying out the procedure of certification of the spectrophotometric method with the use of manganese (II) ions - sodium periodate as an oxidizer is shown.
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issn 2077-1177
language Russian
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publisher Ural Research Institute of Metrology
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series Стандартные образцы
spelling doaj-art-272bdb1c600e45599d5ece6eff2815a72025-08-20T02:43:59ZrusUral Research Institute of MetrologyСтандартные образцы2077-11772020-09-01162415610.20915/2687-0886-2020-16-2-41-55213Application of a number of physical and chemical analysis methods the assessment of a multicomponent sample composition of natural waterL. V. Trubacheva0S. Yu. Lohaninа1T. I. Belova2Udmurt State UniversityUdmurt State UniversityUdmurt State UniversityThe authors present experimental data on the development of a special sample in the form of a dispersed material that simulates the mineral macro-component composition of natural surface water. The results of the study obtained by a number of physico-chemical analysis methods were compared to determine the mass concentration of the micro-component - manganese (II) in the sample. Determination of the mass concentration of manganese (II) was carried out by the methods of spectrophotometry for PND F 14.1:2.61, x-ray fluorometry for PND F 14.1:2:4.130, inversion voltammetry for PND F 14.1:24.217.Procedures for establishing the metrological characteristics of a special sample to control the accuracy of the results of measurements of the mass concentration of manganese (II) using a number of physicо-chemical analysis methods have been carried out.A number of advantages and disadvantages of certified measurement methods that are widely used in chemical laboratories for determining the content of manganese in natural surface water are noted. The necessity of carrying out the procedure of certification of the spectrophotometric method with the use of manganese (II) ions - sodium periodate as an oxidizer is shown.https://www.rmjournal.ru/jour/article/view/247multicomponent composition samplessamples for controlmeasurement techniquesin-laboratory quality control of measurement resultsimplementation of measurement techniques in the laboratory
spellingShingle L. V. Trubacheva
S. Yu. Lohaninа
T. I. Belova
Application of a number of physical and chemical analysis methods the assessment of a multicomponent sample composition of natural water
Стандартные образцы
multicomponent composition samples
samples for control
measurement techniques
in-laboratory quality control of measurement results
implementation of measurement techniques in the laboratory
title Application of a number of physical and chemical analysis methods the assessment of a multicomponent sample composition of natural water
title_full Application of a number of physical and chemical analysis methods the assessment of a multicomponent sample composition of natural water
title_fullStr Application of a number of physical and chemical analysis methods the assessment of a multicomponent sample composition of natural water
title_full_unstemmed Application of a number of physical and chemical analysis methods the assessment of a multicomponent sample composition of natural water
title_short Application of a number of physical and chemical analysis methods the assessment of a multicomponent sample composition of natural water
title_sort application of a number of physical and chemical analysis methods the assessment of a multicomponent sample composition of natural water
topic multicomponent composition samples
samples for control
measurement techniques
in-laboratory quality control of measurement results
implementation of measurement techniques in the laboratory
url https://www.rmjournal.ru/jour/article/view/247
work_keys_str_mv AT lvtrubacheva applicationofanumberofphysicalandchemicalanalysismethodstheassessmentofamulticomponentsamplecompositionofnaturalwater
AT syulohanina applicationofanumberofphysicalandchemicalanalysismethodstheassessmentofamulticomponentsamplecompositionofnaturalwater
AT tibelova applicationofanumberofphysicalandchemicalanalysismethodstheassessmentofamulticomponentsamplecompositionofnaturalwater