Morphology-controlled nickel oxide nanostructures: unlocking high-performance supercapacitor applications

Nickel oxide (NiO) has garnered significant attention as a high-performance electrode material for energy storage devices due to its excellent electrochemical activity and high theoretical capacity. In this study, well crystalline cubic structure NiO with diverse morphologies-three-dimensional spher...

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Main Authors: Govindhasamy Murugadoss, Narthana Kandhasamy, Irina V. Zaporotskova, Nachimuthu Venkatesh, Sunitha Salla, Sakthivel Pandurengan
Format: Article
Language:English
Published: Elsevier 2025-06-01
Series:Chemical Physics Impact
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Online Access:http://www.sciencedirect.com/science/article/pii/S2667022425000751
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author Govindhasamy Murugadoss
Narthana Kandhasamy
Irina V. Zaporotskova
Nachimuthu Venkatesh
Sunitha Salla
Sakthivel Pandurengan
author_facet Govindhasamy Murugadoss
Narthana Kandhasamy
Irina V. Zaporotskova
Nachimuthu Venkatesh
Sunitha Salla
Sakthivel Pandurengan
author_sort Govindhasamy Murugadoss
collection DOAJ
description Nickel oxide (NiO) has garnered significant attention as a high-performance electrode material for energy storage devices due to its excellent electrochemical activity and high theoretical capacity. In this study, well crystalline cubic structure NiO with diverse morphologies-three-dimensional spherical (NiO-3D-S), two-dimensional sheet-like structure (NiO-2D), and three-dimensional asymmetric structure (NiO-3D-A) were synthesized via a simple hydrothermal method. The surface morphology was effectively tailored using polyvinylpyrrolidone (PVP) in combination with various surfactants, including ethylene glycol (EG), cetyltrimethylammonium bromide (CTAB), and glycerol. Among the synthesized structures, the 2D sheet-like porous NiO (NiO-2D) exhibited superior electrochemical performance, achieving a high specific capacitance of 853.17 F g⁻¹ at a current density of 1 mA g⁻¹. It also demonstrated excellent cycling stability, retaining approximately 92 % of its initial capacitance after 3000 charge–discharge cycles. This enhanced performance is attributed to its unique porous architecture composed of ultra-fine grains self-assembled into uniform 2D sheets, which facilitate rapid ion diffusion and efficient charge transport. To evaluate practical applicability, an asymmetric two-electrode device was fabricated using NiO-2D as the positive electrode. The device delivered an energy density of 3.2 Wh kg⁻¹ and a power density of 360 W kg⁻¹, and successfully powered a red light-emitting diode (LED), demonstrating its potential for real-world applications. These findings underscore the promise of 2D sheet-like porous NiO as an advanced electrode material for high-performance and durable electrochemical energy storage systems.
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spelling doaj-art-23b3a0f403c1446b9f2c9ca51994e89d2025-08-20T02:07:40ZengElsevierChemical Physics Impact2667-02242025-06-011010088810.1016/j.chphi.2025.100888Morphology-controlled nickel oxide nanostructures: unlocking high-performance supercapacitor applicationsGovindhasamy Murugadoss0Narthana Kandhasamy1Irina V. Zaporotskova2Nachimuthu Venkatesh3Sunitha Salla4Sakthivel Pandurengan5Centre for Nanoscience and Nanotechnology, Sathyabama Institute of Science and Technology, Chennai, 600 119, Tamil Nadu, India; Corresponding authors.Centre for Nanoscience and Nanotechnology, Sathyabama Institute of Science and Technology, Chennai, 600 119, Tamil Nadu, IndiaFederal State Educational Institution of Higher Education ''Volgograd State University'', ave. Universitetskiy, 100, Volgograd, Volgograd region, 400062, RussiaCentre for Nanoscience and Nanotechnology, Sathyabama Institute of Science and Technology, Chennai, 600 119, Tamil Nadu, IndiaDepartment of Chemistry, Sathyabama Institute of Science and Technology, Chennai, 600 119, Tamil Nadu, IndiaDepartment of Physics, Manipal University Jaipur, Jaipur, 303 007, Rajasthan, India; Corresponding authors.Nickel oxide (NiO) has garnered significant attention as a high-performance electrode material for energy storage devices due to its excellent electrochemical activity and high theoretical capacity. In this study, well crystalline cubic structure NiO with diverse morphologies-three-dimensional spherical (NiO-3D-S), two-dimensional sheet-like structure (NiO-2D), and three-dimensional asymmetric structure (NiO-3D-A) were synthesized via a simple hydrothermal method. The surface morphology was effectively tailored using polyvinylpyrrolidone (PVP) in combination with various surfactants, including ethylene glycol (EG), cetyltrimethylammonium bromide (CTAB), and glycerol. Among the synthesized structures, the 2D sheet-like porous NiO (NiO-2D) exhibited superior electrochemical performance, achieving a high specific capacitance of 853.17 F g⁻¹ at a current density of 1 mA g⁻¹. It also demonstrated excellent cycling stability, retaining approximately 92 % of its initial capacitance after 3000 charge–discharge cycles. This enhanced performance is attributed to its unique porous architecture composed of ultra-fine grains self-assembled into uniform 2D sheets, which facilitate rapid ion diffusion and efficient charge transport. To evaluate practical applicability, an asymmetric two-electrode device was fabricated using NiO-2D as the positive electrode. The device delivered an energy density of 3.2 Wh kg⁻¹ and a power density of 360 W kg⁻¹, and successfully powered a red light-emitting diode (LED), demonstrating its potential for real-world applications. These findings underscore the promise of 2D sheet-like porous NiO as an advanced electrode material for high-performance and durable electrochemical energy storage systems.http://www.sciencedirect.com/science/article/pii/S2667022425000751Surface modificationHydrothermal2d sheetSupercapacitorEnergy storage
spellingShingle Govindhasamy Murugadoss
Narthana Kandhasamy
Irina V. Zaporotskova
Nachimuthu Venkatesh
Sunitha Salla
Sakthivel Pandurengan
Morphology-controlled nickel oxide nanostructures: unlocking high-performance supercapacitor applications
Chemical Physics Impact
Surface modification
Hydrothermal
2d sheet
Supercapacitor
Energy storage
title Morphology-controlled nickel oxide nanostructures: unlocking high-performance supercapacitor applications
title_full Morphology-controlled nickel oxide nanostructures: unlocking high-performance supercapacitor applications
title_fullStr Morphology-controlled nickel oxide nanostructures: unlocking high-performance supercapacitor applications
title_full_unstemmed Morphology-controlled nickel oxide nanostructures: unlocking high-performance supercapacitor applications
title_short Morphology-controlled nickel oxide nanostructures: unlocking high-performance supercapacitor applications
title_sort morphology controlled nickel oxide nanostructures unlocking high performance supercapacitor applications
topic Surface modification
Hydrothermal
2d sheet
Supercapacitor
Energy storage
url http://www.sciencedirect.com/science/article/pii/S2667022425000751
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AT irinavzaporotskova morphologycontrollednickeloxidenanostructuresunlockinghighperformancesupercapacitorapplications
AT nachimuthuvenkatesh morphologycontrollednickeloxidenanostructuresunlockinghighperformancesupercapacitorapplications
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