Structural Changes in Copper Slags During Slow Cooling

The objects of the study were converter slags from the Balkhash copper plant in their initial state and after heat treatment. Using mineralogical and X-ray phase analysis, scanning electron microscopy (SEM), and electron probe microanalysis (EPMA), it was found that the initial converter slag and it...

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Main Authors: Bulat Sukurov, Sergey Kvyatkovskiy, Sultanbek Kozhakhmetov, Anastassiya Semenova, Maral Dyussebekova, Marina Kvyatkovskaya
Format: Article
Language:English
Published: MDPI AG 2024-10-01
Series:Metals
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Online Access:https://www.mdpi.com/2075-4701/14/10/1187
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author Bulat Sukurov
Sergey Kvyatkovskiy
Sultanbek Kozhakhmetov
Anastassiya Semenova
Maral Dyussebekova
Marina Kvyatkovskaya
author_facet Bulat Sukurov
Sergey Kvyatkovskiy
Sultanbek Kozhakhmetov
Anastassiya Semenova
Maral Dyussebekova
Marina Kvyatkovskaya
author_sort Bulat Sukurov
collection DOAJ
description The objects of the study were converter slags from the Balkhash copper plant in their initial state and after heat treatment. Using mineralogical and X-ray phase analysis, scanning electron microscopy (SEM), and electron probe microanalysis (EPMA), it was found that the initial converter slag and its thermally treated samples have identical matrices with almost complete coincidence in mineral and phase compositions. The distinguishing feature is the quantitative ratio of mineral components in the slag mass. Almost all of the iron is oxidized and present in the form of fayalite, magnetite, and magnetite, with other elements (silicon, copper, zinc, and aluminum) incorporated into its lattice. The structure of all slag samples indicates an association of sulfur exclusively with copper. Copper in the slags was identified in both metallic and sulfide forms. Slow cooling of the converter slag after its remelting contributes to the reduction in the sulfide–metal suspension in the volume of the melt and its coarsening. During slow cooling, structural changes occur not only in the main oxide part of the slag but also in the polymetallic globules.
format Article
id doaj-art-21547365d7dd4ebbb66b3e56115bd544
institution OA Journals
issn 2075-4701
language English
publishDate 2024-10-01
publisher MDPI AG
record_format Article
series Metals
spelling doaj-art-21547365d7dd4ebbb66b3e56115bd5442025-08-20T02:11:15ZengMDPI AGMetals2075-47012024-10-011410118710.3390/met14101187Structural Changes in Copper Slags During Slow CoolingBulat Sukurov0Sergey Kvyatkovskiy1Sultanbek Kozhakhmetov2Anastassiya Semenova3Maral Dyussebekova4Marina Kvyatkovskaya5Institute of Metallurgy and Ore Beneficiation, Satbayev University, Almaty 050013, KazakhstanInstitute of Metallurgy and Ore Beneficiation, Satbayev University, Almaty 050013, KazakhstanInstitute of Metallurgy and Ore Beneficiation, Satbayev University, Almaty 050013, KazakhstanInstitute of Metallurgy and Ore Beneficiation, Satbayev University, Almaty 050013, KazakhstanInstitute of Metallurgy and Ore Beneficiation, Satbayev University, Almaty 050013, KazakhstanInstitute of Metallurgy and Ore Beneficiation, Satbayev University, Almaty 050013, KazakhstanThe objects of the study were converter slags from the Balkhash copper plant in their initial state and after heat treatment. Using mineralogical and X-ray phase analysis, scanning electron microscopy (SEM), and electron probe microanalysis (EPMA), it was found that the initial converter slag and its thermally treated samples have identical matrices with almost complete coincidence in mineral and phase compositions. The distinguishing feature is the quantitative ratio of mineral components in the slag mass. Almost all of the iron is oxidized and present in the form of fayalite, magnetite, and magnetite, with other elements (silicon, copper, zinc, and aluminum) incorporated into its lattice. The structure of all slag samples indicates an association of sulfur exclusively with copper. Copper in the slags was identified in both metallic and sulfide forms. Slow cooling of the converter slag after its remelting contributes to the reduction in the sulfide–metal suspension in the volume of the melt and its coarsening. During slow cooling, structural changes occur not only in the main oxide part of the slag but also in the polymetallic globules.https://www.mdpi.com/2075-4701/14/10/1187metallurgical slagsdepletion of slagsslow coolingmicrostructurepolymetallic globuleshigh-dynamic formation of Pb microdroplets
spellingShingle Bulat Sukurov
Sergey Kvyatkovskiy
Sultanbek Kozhakhmetov
Anastassiya Semenova
Maral Dyussebekova
Marina Kvyatkovskaya
Structural Changes in Copper Slags During Slow Cooling
Metals
metallurgical slags
depletion of slags
slow cooling
microstructure
polymetallic globules
high-dynamic formation of Pb microdroplets
title Structural Changes in Copper Slags During Slow Cooling
title_full Structural Changes in Copper Slags During Slow Cooling
title_fullStr Structural Changes in Copper Slags During Slow Cooling
title_full_unstemmed Structural Changes in Copper Slags During Slow Cooling
title_short Structural Changes in Copper Slags During Slow Cooling
title_sort structural changes in copper slags during slow cooling
topic metallurgical slags
depletion of slags
slow cooling
microstructure
polymetallic globules
high-dynamic formation of Pb microdroplets
url https://www.mdpi.com/2075-4701/14/10/1187
work_keys_str_mv AT bulatsukurov structuralchangesincopperslagsduringslowcooling
AT sergeykvyatkovskiy structuralchangesincopperslagsduringslowcooling
AT sultanbekkozhakhmetov structuralchangesincopperslagsduringslowcooling
AT anastassiyasemenova structuralchangesincopperslagsduringslowcooling
AT maraldyussebekova structuralchangesincopperslagsduringslowcooling
AT marinakvyatkovskaya structuralchangesincopperslagsduringslowcooling