Characterization of defective coffee beans and blends differentiation based on 1H qNMR technique

Defective coffee beans (DCB) are one of the main reasons for poor coffee quality. In the current research, chemical difference of three common DCB including sour beans (SCB), black beans (BCB), and mold beans (MCB) were clarified using 1H qNMR method and compared with that of non-defective beans (ND...

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Main Authors: Gui-Lin Hu, Chen-Xi Quan, Hao-Peng Dai, Ming-Hua Qiu
Format: Article
Language:English
Published: Elsevier 2024-01-01
Series:Current Research in Food Science
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2665927124001965
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author Gui-Lin Hu
Chen-Xi Quan
Hao-Peng Dai
Ming-Hua Qiu
author_facet Gui-Lin Hu
Chen-Xi Quan
Hao-Peng Dai
Ming-Hua Qiu
author_sort Gui-Lin Hu
collection DOAJ
description Defective coffee beans (DCB) are one of the main reasons for poor coffee quality. In the current research, chemical difference of three common DCB including sour beans (SCB), black beans (BCB), and mold beans (MCB) were clarified using 1H qNMR method and compared with that of non-defective beans (NDCB). The results indicated that DCB has lower sugar and lipid content compared to NDCB, yet it boasts a higher acetate concentration. The 1H NMR from water-soluble content was shown to be more effective than that of oil fraction for qualitative of DCB blends, regardless of whether partial least squares discriminant analysis (PLS-DA) or machine learning (ML) algorithms were used. Support vector machine (SVM) was proved to be excellent for distinguishing DCB blends. Finally, a partial least squares regression (PLS) model was built for quantitative analysis of DCB blends. In summary, current research will not only help to reveal the material basis of DCB and their impact on coffee flavor, but also provide feasible strategies for the identification of DCB.
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publishDate 2024-01-01
publisher Elsevier
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series Current Research in Food Science
spelling doaj-art-1eb866b9b8b949b9bd2e3046405a490e2025-08-20T02:49:49ZengElsevierCurrent Research in Food Science2665-92712024-01-01910087010.1016/j.crfs.2024.100870Characterization of defective coffee beans and blends differentiation based on 1H qNMR techniqueGui-Lin Hu0Chen-Xi Quan1Hao-Peng Dai2Ming-Hua Qiu3State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming, 650201, Yunnan, ChinaState Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming, 650201, Yunnan, ChinaState Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming, 650201, Yunnan, ChinaCorresponding author.; State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming, 650201, Yunnan, ChinaDefective coffee beans (DCB) are one of the main reasons for poor coffee quality. In the current research, chemical difference of three common DCB including sour beans (SCB), black beans (BCB), and mold beans (MCB) were clarified using 1H qNMR method and compared with that of non-defective beans (NDCB). The results indicated that DCB has lower sugar and lipid content compared to NDCB, yet it boasts a higher acetate concentration. The 1H NMR from water-soluble content was shown to be more effective than that of oil fraction for qualitative of DCB blends, regardless of whether partial least squares discriminant analysis (PLS-DA) or machine learning (ML) algorithms were used. Support vector machine (SVM) was proved to be excellent for distinguishing DCB blends. Finally, a partial least squares regression (PLS) model was built for quantitative analysis of DCB blends. In summary, current research will not only help to reveal the material basis of DCB and their impact on coffee flavor, but also provide feasible strategies for the identification of DCB.http://www.sciencedirect.com/science/article/pii/S2665927124001965Arabica coffeeDefective coffee beansChemometricsMachine learningSupport vector machine
spellingShingle Gui-Lin Hu
Chen-Xi Quan
Hao-Peng Dai
Ming-Hua Qiu
Characterization of defective coffee beans and blends differentiation based on 1H qNMR technique
Current Research in Food Science
Arabica coffee
Defective coffee beans
Chemometrics
Machine learning
Support vector machine
title Characterization of defective coffee beans and blends differentiation based on 1H qNMR technique
title_full Characterization of defective coffee beans and blends differentiation based on 1H qNMR technique
title_fullStr Characterization of defective coffee beans and blends differentiation based on 1H qNMR technique
title_full_unstemmed Characterization of defective coffee beans and blends differentiation based on 1H qNMR technique
title_short Characterization of defective coffee beans and blends differentiation based on 1H qNMR technique
title_sort characterization of defective coffee beans and blends differentiation based on 1h qnmr technique
topic Arabica coffee
Defective coffee beans
Chemometrics
Machine learning
Support vector machine
url http://www.sciencedirect.com/science/article/pii/S2665927124001965
work_keys_str_mv AT guilinhu characterizationofdefectivecoffeebeansandblendsdifferentiationbasedon1hqnmrtechnique
AT chenxiquan characterizationofdefectivecoffeebeansandblendsdifferentiationbasedon1hqnmrtechnique
AT haopengdai characterizationofdefectivecoffeebeansandblendsdifferentiationbasedon1hqnmrtechnique
AT minghuaqiu characterizationofdefectivecoffeebeansandblendsdifferentiationbasedon1hqnmrtechnique