Microtubule polymerization induced by iridium‐fullerene photosensitizers for cancer immunotherapy via dual‐reactive oxygen species regulation strategy

Abstract Microtubules (MTs) are key players in cell division, migration, and signaling, and they are regarded as important targets for cancer treatment. In this work, two fullerene (C60)‐functionalized Ir(III) complexes (Ir‐C601 and Ir‐C602) are rationally designed as dual reactive oxygen species (R...

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Main Authors: Xiao‐Xiao Chen, Kun Peng, Xi Chen, Zheng‐Yin Pan, Qing‐Hua Shen, Yu‐Yi Ling, Jian‐Zhang Zhao, Cai‐Ping Tan
Format: Article
Language:English
Published: Wiley 2024-12-01
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Online Access:https://doi.org/10.1002/agt2.623
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author Xiao‐Xiao Chen
Kun Peng
Xi Chen
Zheng‐Yin Pan
Qing‐Hua Shen
Yu‐Yi Ling
Jian‐Zhang Zhao
Cai‐Ping Tan
author_facet Xiao‐Xiao Chen
Kun Peng
Xi Chen
Zheng‐Yin Pan
Qing‐Hua Shen
Yu‐Yi Ling
Jian‐Zhang Zhao
Cai‐Ping Tan
author_sort Xiao‐Xiao Chen
collection DOAJ
description Abstract Microtubules (MTs) are key players in cell division, migration, and signaling, and they are regarded as important targets for cancer treatment. In this work, two fullerene (C60)‐functionalized Ir(III) complexes (Ir‐C601 and Ir‐C602) are rationally designed as dual reactive oxygen species (ROS) regulators and MT‐targeted Type I/II photosensitizers. In the dark, Ir‐C601 and Ir‐C602 serve as ROS scavengers to eliminate O2•− and •OH, consequently reducing the dark cytotoxicity and reversing dysfunctional T cells. Due to the efficiently populated C60‐localized intraligand triplet state, Ir‐C601 and Ir‐C602 can be excited by green light (525 nm) to produce O2•− and •OONO− (Type I) and 1O2 (Type II) to overcome tumor hypoxia. Moreover, Ir‐C601 is also able to photooxidize tubulin, consequently interfering with the cellular cytoskeleton structures, inducing immunogenic cell death and inhibiting cell proliferation and migration. Finally, Ir‐C601 exhibits promising photo‐immunotherapeutic effects both in vitro and in vivo. In all, we report here the first MT stabilizing photosensitizer performing through Type I/II photodynamic therapy pathways, which provides insights into the rational design of new photo‐immunotherapeutic agents targeting specific biomolecules.
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spelling doaj-art-1e9cb229e7bb48169c680982bced8a8c2025-08-20T02:35:41ZengWileyAggregate2692-45602024-12-0156n/an/a10.1002/agt2.623Microtubule polymerization induced by iridium‐fullerene photosensitizers for cancer immunotherapy via dual‐reactive oxygen species regulation strategyXiao‐Xiao Chen0Kun Peng1Xi Chen2Zheng‐Yin Pan3Qing‐Hua Shen4Yu‐Yi Ling5Jian‐Zhang Zhao6Cai‐Ping Tan7MOE Key Laboratory of Bioinorganic and Synthetic Chemistry, School of Chemistry Sun Yat‐Sen University Guangzhou P. R. ChinaMOE Key Laboratory of Bioinorganic and Synthetic Chemistry, School of Chemistry Sun Yat‐Sen University Guangzhou P. R. ChinaState Key Laboratory of Fine Chemicals, Frontiers Science Center for Smart Materials, School of Chemical Engineering Dalian University of Technology Dalian P. R. ChinaMOE Key Laboratory of Bioinorganic and Synthetic Chemistry, School of Chemistry Sun Yat‐Sen University Guangzhou P. R. ChinaMOE Key Laboratory of Bioinorganic and Synthetic Chemistry, School of Chemistry Sun Yat‐Sen University Guangzhou P. R. ChinaMOE Key Laboratory of Bioinorganic and Synthetic Chemistry, School of Chemistry Sun Yat‐Sen University Guangzhou P. R. ChinaState Key Laboratory of Fine Chemicals, Frontiers Science Center for Smart Materials, School of Chemical Engineering Dalian University of Technology Dalian P. R. ChinaMOE Key Laboratory of Bioinorganic and Synthetic Chemistry, School of Chemistry Sun Yat‐Sen University Guangzhou P. R. ChinaAbstract Microtubules (MTs) are key players in cell division, migration, and signaling, and they are regarded as important targets for cancer treatment. In this work, two fullerene (C60)‐functionalized Ir(III) complexes (Ir‐C601 and Ir‐C602) are rationally designed as dual reactive oxygen species (ROS) regulators and MT‐targeted Type I/II photosensitizers. In the dark, Ir‐C601 and Ir‐C602 serve as ROS scavengers to eliminate O2•− and •OH, consequently reducing the dark cytotoxicity and reversing dysfunctional T cells. Due to the efficiently populated C60‐localized intraligand triplet state, Ir‐C601 and Ir‐C602 can be excited by green light (525 nm) to produce O2•− and •OONO− (Type I) and 1O2 (Type II) to overcome tumor hypoxia. Moreover, Ir‐C601 is also able to photooxidize tubulin, consequently interfering with the cellular cytoskeleton structures, inducing immunogenic cell death and inhibiting cell proliferation and migration. Finally, Ir‐C601 exhibits promising photo‐immunotherapeutic effects both in vitro and in vivo. In all, we report here the first MT stabilizing photosensitizer performing through Type I/II photodynamic therapy pathways, which provides insights into the rational design of new photo‐immunotherapeutic agents targeting specific biomolecules.https://doi.org/10.1002/agt2.623anticancerfullereneiridium complexesmicrotubulephoto‐immunotherapy
spellingShingle Xiao‐Xiao Chen
Kun Peng
Xi Chen
Zheng‐Yin Pan
Qing‐Hua Shen
Yu‐Yi Ling
Jian‐Zhang Zhao
Cai‐Ping Tan
Microtubule polymerization induced by iridium‐fullerene photosensitizers for cancer immunotherapy via dual‐reactive oxygen species regulation strategy
Aggregate
anticancer
fullerene
iridium complexes
microtubule
photo‐immunotherapy
title Microtubule polymerization induced by iridium‐fullerene photosensitizers for cancer immunotherapy via dual‐reactive oxygen species regulation strategy
title_full Microtubule polymerization induced by iridium‐fullerene photosensitizers for cancer immunotherapy via dual‐reactive oxygen species regulation strategy
title_fullStr Microtubule polymerization induced by iridium‐fullerene photosensitizers for cancer immunotherapy via dual‐reactive oxygen species regulation strategy
title_full_unstemmed Microtubule polymerization induced by iridium‐fullerene photosensitizers for cancer immunotherapy via dual‐reactive oxygen species regulation strategy
title_short Microtubule polymerization induced by iridium‐fullerene photosensitizers for cancer immunotherapy via dual‐reactive oxygen species regulation strategy
title_sort microtubule polymerization induced by iridium fullerene photosensitizers for cancer immunotherapy via dual reactive oxygen species regulation strategy
topic anticancer
fullerene
iridium complexes
microtubule
photo‐immunotherapy
url https://doi.org/10.1002/agt2.623
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