Impact of B and Al on the initial and residual dissolution rate of alumino-boro-silicate glasses. Part II: gel properties

Abstract Physical and chemical properties of passivating alteration gels formed on alumino-boro-silicate glasses of interest for nuclear waste containment are reported. Opposite effects of B and Al on the gel’s propensity to restructure and become passivating were observed. Boron, primarily forming...

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Main Authors: Mélanie Taron, Stéphane Gin, Huseyin Kaya, Jean-Marc Delaye, Seong H. Kim
Format: Article
Language:English
Published: Nature Portfolio 2025-05-01
Series:npj Materials Degradation
Online Access:https://doi.org/10.1038/s41529-025-00576-9
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author Mélanie Taron
Stéphane Gin
Huseyin Kaya
Jean-Marc Delaye
Seong H. Kim
author_facet Mélanie Taron
Stéphane Gin
Huseyin Kaya
Jean-Marc Delaye
Seong H. Kim
author_sort Mélanie Taron
collection DOAJ
description Abstract Physical and chemical properties of passivating alteration gels formed on alumino-boro-silicate glasses of interest for nuclear waste containment are reported. Opposite effects of B and Al on the gel’s propensity to restructure and become passivating were observed. Boron, primarily forming Si‒O‒B bonds, fragments and weakens the silicate network if its concentration is higher than a critical value, leading to the formation of pores and Si‒OH terminations as it leaches out. The greater the number of the silanol groups, the more effective the recondensation (Si‒OH + Si‒OH ⇌ Si‒O‒Si + H2O) is, leading to reduction of pore connectivity; this facilitates passivation and thus lowers the glass alteration rate. Conversely, Al has a slowing effect on this reorganization dynamics. This work provides better insight into the role of elements in the glass alteration kinetics.
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spelling doaj-art-1e05c2e2f9124a2086a427ae60db42fb2025-08-20T02:34:15ZengNature Portfolionpj Materials Degradation2397-21062025-05-019111210.1038/s41529-025-00576-9Impact of B and Al on the initial and residual dissolution rate of alumino-boro-silicate glasses. Part II: gel propertiesMélanie Taron0Stéphane Gin1Huseyin Kaya2Jean-Marc Delaye3Seong H. Kim4CEA, DES, ISEC, DPME, SEME, University of Montpellier, MarcouleCEA, DES, ISEC, DPME, SEME, University of Montpellier, MarcouleDepartment of Materials Science & Engineering, The Pennsylvania State UniversityCEA, DES, ISEC, DPME, SEME, University of Montpellier, MarcouleDepartment of Chemical Engineering and Materials Research Institute, The Pennsylvania State UniversityAbstract Physical and chemical properties of passivating alteration gels formed on alumino-boro-silicate glasses of interest for nuclear waste containment are reported. Opposite effects of B and Al on the gel’s propensity to restructure and become passivating were observed. Boron, primarily forming Si‒O‒B bonds, fragments and weakens the silicate network if its concentration is higher than a critical value, leading to the formation of pores and Si‒OH terminations as it leaches out. The greater the number of the silanol groups, the more effective the recondensation (Si‒OH + Si‒OH ⇌ Si‒O‒Si + H2O) is, leading to reduction of pore connectivity; this facilitates passivation and thus lowers the glass alteration rate. Conversely, Al has a slowing effect on this reorganization dynamics. This work provides better insight into the role of elements in the glass alteration kinetics.https://doi.org/10.1038/s41529-025-00576-9
spellingShingle Mélanie Taron
Stéphane Gin
Huseyin Kaya
Jean-Marc Delaye
Seong H. Kim
Impact of B and Al on the initial and residual dissolution rate of alumino-boro-silicate glasses. Part II: gel properties
npj Materials Degradation
title Impact of B and Al on the initial and residual dissolution rate of alumino-boro-silicate glasses. Part II: gel properties
title_full Impact of B and Al on the initial and residual dissolution rate of alumino-boro-silicate glasses. Part II: gel properties
title_fullStr Impact of B and Al on the initial and residual dissolution rate of alumino-boro-silicate glasses. Part II: gel properties
title_full_unstemmed Impact of B and Al on the initial and residual dissolution rate of alumino-boro-silicate glasses. Part II: gel properties
title_short Impact of B and Al on the initial and residual dissolution rate of alumino-boro-silicate glasses. Part II: gel properties
title_sort impact of b and al on the initial and residual dissolution rate of alumino boro silicate glasses part ii gel properties
url https://doi.org/10.1038/s41529-025-00576-9
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