Studying Reactivity Relationships of Copolymers N-naphthylacrylamide with (Acrylicacid and Methylacrylate)

The organation ⁄monomer N-naphthylacrylamide (NAA) was prepared; subsequently the synthesized monomer was successfully copolymerized with acrylicacid (AA) and methylacrylate (MA) by free radical technique using dry benzene as solvent and benzoyl peroxide (BPO) as initiator. The overall conversion wa...

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Main Author: Ameen Hadi Mohammed
Format: Article
Language:English
Published: University of Baghdad, College of Science for Women 2019-06-01
Series:مجلة بغداد للعلوم
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Online Access:http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/3466
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author Ameen Hadi Mohammed
author_facet Ameen Hadi Mohammed
author_sort Ameen Hadi Mohammed
collection DOAJ
description The organation ⁄monomer N-naphthylacrylamide (NAA) was prepared; subsequently the synthesized monomer was successfully copolymerized with acrylicacid (AA) and methylacrylate (MA) by free radical technique using dry benzene as solvent and benzoyl peroxide (BPO) as initiator. The overall conversion was kept low (≤ 10% wt/wt) for all studies copolymers samples. The synthesized monomer and copolymers were characterized using Fourier transform infrared spectroscopy (FT-IR), and their thermal properties were studied by DSC and TGA. The copolymers compositions were determined by elemental analysis. Kelen-Tudes and Finmman-Ross graphical procedures were employed to determine the monomers reactivity ratios. The derived reactivity ratios (r1, r2) are: (0.048, 0.687) for (NAA-co-AA) and (0.066, 0.346) for (NAA-co-MA). Based on the average reactivity ratios, sequence distribution of monomers in the copolymers and the microstructure of copolymers were calculated by statistical method and found that these values are in agreement with the derived reactivity ratios.
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series مجلة بغداد للعلوم
spelling doaj-art-1d08798efd224615a341fbd0b58e1b912025-08-20T03:34:05ZengUniversity of Baghdad, College of Science for Womenمجلة بغداد للعلوم2078-86652411-79862019-06-0116210.21123/bsj.16.2.0345Studying Reactivity Relationships of Copolymers N-naphthylacrylamide with (Acrylicacid and Methylacrylate)Ameen Hadi MohammedThe organation ⁄monomer N-naphthylacrylamide (NAA) was prepared; subsequently the synthesized monomer was successfully copolymerized with acrylicacid (AA) and methylacrylate (MA) by free radical technique using dry benzene as solvent and benzoyl peroxide (BPO) as initiator. The overall conversion was kept low (≤ 10% wt/wt) for all studies copolymers samples. The synthesized monomer and copolymers were characterized using Fourier transform infrared spectroscopy (FT-IR), and their thermal properties were studied by DSC and TGA. The copolymers compositions were determined by elemental analysis. Kelen-Tudes and Finmman-Ross graphical procedures were employed to determine the monomers reactivity ratios. The derived reactivity ratios (r1, r2) are: (0.048, 0.687) for (NAA-co-AA) and (0.066, 0.346) for (NAA-co-MA). Based on the average reactivity ratios, sequence distribution of monomers in the copolymers and the microstructure of copolymers were calculated by statistical method and found that these values are in agreement with the derived reactivity ratios.http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/3466Acrylic acid, Methyl acrylate, N-naphthylacrylamide, Reactivity relationships
spellingShingle Ameen Hadi Mohammed
Studying Reactivity Relationships of Copolymers N-naphthylacrylamide with (Acrylicacid and Methylacrylate)
مجلة بغداد للعلوم
Acrylic acid, Methyl acrylate, N-naphthylacrylamide, Reactivity relationships
title Studying Reactivity Relationships of Copolymers N-naphthylacrylamide with (Acrylicacid and Methylacrylate)
title_full Studying Reactivity Relationships of Copolymers N-naphthylacrylamide with (Acrylicacid and Methylacrylate)
title_fullStr Studying Reactivity Relationships of Copolymers N-naphthylacrylamide with (Acrylicacid and Methylacrylate)
title_full_unstemmed Studying Reactivity Relationships of Copolymers N-naphthylacrylamide with (Acrylicacid and Methylacrylate)
title_short Studying Reactivity Relationships of Copolymers N-naphthylacrylamide with (Acrylicacid and Methylacrylate)
title_sort studying reactivity relationships of copolymers n naphthylacrylamide with acrylicacid and methylacrylate
topic Acrylic acid, Methyl acrylate, N-naphthylacrylamide, Reactivity relationships
url http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/3466
work_keys_str_mv AT ameenhadimohammed studyingreactivityrelationshipsofcopolymersnnaphthylacrylamidewithacrylicacidandmethylacrylate