Effects of difference in heating sources on ammonia reactivity: Possibility for photolysis-assisted ammonia combustion

Ammonia (NH3) reactivity in a micro flow reactor with a controlled temperature profile (MFR) is reexamined through species measurements utilizing two heating sources in the MFR: an H2/air flat flame and an electric heater. The maximum wall temperatures (Tw,max) formed in the reactor vary in a range...

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Main Authors: Kenta Tamaoki, Yoshito Ishida, Takuya Tezuka, Hisashi Nakamura
Format: Article
Language:English
Published: Elsevier 2024-12-01
Series:Fuel Communications
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Online Access:http://www.sciencedirect.com/science/article/pii/S2666052024000256
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author Kenta Tamaoki
Yoshito Ishida
Takuya Tezuka
Hisashi Nakamura
author_facet Kenta Tamaoki
Yoshito Ishida
Takuya Tezuka
Hisashi Nakamura
author_sort Kenta Tamaoki
collection DOAJ
description Ammonia (NH3) reactivity in a micro flow reactor with a controlled temperature profile (MFR) is reexamined through species measurements utilizing two heating sources in the MFR: an H2/air flat flame and an electric heater. The maximum wall temperatures (Tw,max) formed in the reactor vary in a range of Tw,max = 1100–1400 K. A stoichiometric NH3/air mixture is tested, and exhaust NH3 is detected by a quadrupole mass spectrometer (QMS). Unexpectedly, NH3 is completely consumed at temperatures at least 100 K lower in the H2/air flat flame case compared to the electric furnace case, despite nearly identical conditions of a MFR characteristic residence time estimated by the wall temperature profiles and the convective flow velocity. Considering the non-thermal characteristics of the two heating sources that the H2/air flat flame emits ultraviolet light, whereas infrared light as thermal radiation is emitted within the electric furnace, the possibility of NH3 photolysis in the H2/air flat flame case is discussed based on literature regarding emissions from the H2/air flames, the transmittance of the quartz tube, and the photodissociation of NH3 in the ultraviolet region. When ultraviolet light emitted from the H2/air flat flame passes through the quartz tube and decomposes NH3 into NH2 and H radicals, these produced radicals enhance the growth of OH radicals, resulting in increased NH3 reactivity. These findings suggest the possibility of photolysis-assisted ammonia combustion, which could be an additional method to overcome the low reactivity of NH3.
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spelling doaj-art-1bcda9540a4041c0be284bcc7e9e398a2025-08-20T01:58:22ZengElsevierFuel Communications2666-05202024-12-012110013010.1016/j.jfueco.2024.100130Effects of difference in heating sources on ammonia reactivity: Possibility for photolysis-assisted ammonia combustionKenta Tamaoki0Yoshito Ishida1Takuya Tezuka2Hisashi Nakamura3Institute of Fluid Science, Tohoku University, 2-1-1 Katahira, Aoba, Sendai, Miyagi 980-8577, Japan; Department of Mechanical Systems Engineering, Graduate School of Engineering, Tohoku University, 6-6 Aramaki Aza Aoba, Aoba, Sendai, Miyagi 980-8579, JapanInstitute of Fluid Science, Tohoku University, 2-1-1 Katahira, Aoba, Sendai, Miyagi 980-8577, Japan; Department of Mechanical Systems Engineering, Graduate School of Engineering, Tohoku University, 6-6 Aramaki Aza Aoba, Aoba, Sendai, Miyagi 980-8579, JapanInstitute of Fluid Science, Tohoku University, 2-1-1 Katahira, Aoba, Sendai, Miyagi 980-8577, JapanInstitute of Fluid Science, Tohoku University, 2-1-1 Katahira, Aoba, Sendai, Miyagi 980-8577, Japan; Corresponding author.Ammonia (NH3) reactivity in a micro flow reactor with a controlled temperature profile (MFR) is reexamined through species measurements utilizing two heating sources in the MFR: an H2/air flat flame and an electric heater. The maximum wall temperatures (Tw,max) formed in the reactor vary in a range of Tw,max = 1100–1400 K. A stoichiometric NH3/air mixture is tested, and exhaust NH3 is detected by a quadrupole mass spectrometer (QMS). Unexpectedly, NH3 is completely consumed at temperatures at least 100 K lower in the H2/air flat flame case compared to the electric furnace case, despite nearly identical conditions of a MFR characteristic residence time estimated by the wall temperature profiles and the convective flow velocity. Considering the non-thermal characteristics of the two heating sources that the H2/air flat flame emits ultraviolet light, whereas infrared light as thermal radiation is emitted within the electric furnace, the possibility of NH3 photolysis in the H2/air flat flame case is discussed based on literature regarding emissions from the H2/air flames, the transmittance of the quartz tube, and the photodissociation of NH3 in the ultraviolet region. When ultraviolet light emitted from the H2/air flat flame passes through the quartz tube and decomposes NH3 into NH2 and H radicals, these produced radicals enhance the growth of OH radicals, resulting in increased NH3 reactivity. These findings suggest the possibility of photolysis-assisted ammonia combustion, which could be an additional method to overcome the low reactivity of NH3.http://www.sciencedirect.com/science/article/pii/S2666052024000256AmmoniaMicrocombustionCarbon-free fuelPhotolysis
spellingShingle Kenta Tamaoki
Yoshito Ishida
Takuya Tezuka
Hisashi Nakamura
Effects of difference in heating sources on ammonia reactivity: Possibility for photolysis-assisted ammonia combustion
Fuel Communications
Ammonia
Microcombustion
Carbon-free fuel
Photolysis
title Effects of difference in heating sources on ammonia reactivity: Possibility for photolysis-assisted ammonia combustion
title_full Effects of difference in heating sources on ammonia reactivity: Possibility for photolysis-assisted ammonia combustion
title_fullStr Effects of difference in heating sources on ammonia reactivity: Possibility for photolysis-assisted ammonia combustion
title_full_unstemmed Effects of difference in heating sources on ammonia reactivity: Possibility for photolysis-assisted ammonia combustion
title_short Effects of difference in heating sources on ammonia reactivity: Possibility for photolysis-assisted ammonia combustion
title_sort effects of difference in heating sources on ammonia reactivity possibility for photolysis assisted ammonia combustion
topic Ammonia
Microcombustion
Carbon-free fuel
Photolysis
url http://www.sciencedirect.com/science/article/pii/S2666052024000256
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AT takuyatezuka effectsofdifferenceinheatingsourcesonammoniareactivitypossibilityforphotolysisassistedammoniacombustion
AT hisashinakamura effectsofdifferenceinheatingsourcesonammoniareactivitypossibilityforphotolysisassistedammoniacombustion