Raman evaluation of graphene oxide dispersed in naphthenic oil

Abstract Graphene oxide is a revolutionary material that enhances properties in electronics, automotive, civil construction, aerospace, and industrial sectors. Even added in low levels (0.1 – 5.0%), properly dispersed in polymer composites, it results in significant differences in mechanical, therma...

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Main Authors: ALAN PASSERO, TAYNARA A. DE CARVALHO, NATALIA B. SANCHES, LIDIA M.S. MURAKAMI, JORGE CARLOS N. DUTRA, RITA DE CÁSSIA L. DUTRA
Format: Article
Language:English
Published: Academia Brasileira de Ciências 2025-03-01
Series:Anais da Academia Brasileira de Ciências
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Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0001-37652025000201702&lng=en&tlng=en
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author ALAN PASSERO
TAYNARA A. DE CARVALHO
NATALIA B. SANCHES
LIDIA M.S. MURAKAMI
JORGE CARLOS N. DUTRA
RITA DE CÁSSIA L. DUTRA
author_facet ALAN PASSERO
TAYNARA A. DE CARVALHO
NATALIA B. SANCHES
LIDIA M.S. MURAKAMI
JORGE CARLOS N. DUTRA
RITA DE CÁSSIA L. DUTRA
author_sort ALAN PASSERO
collection DOAJ
description Abstract Graphene oxide is a revolutionary material that enhances properties in electronics, automotive, civil construction, aerospace, and industrial sectors. Even added in low levels (0.1 – 5.0%), properly dispersed in polymer composites, it results in significant differences in mechanical, thermal, chemical, and electrical properties. Often, a suitable dispersant facilitate homogenization and provides stability in the fabrication process. However, there are few studies in the literature that assess graphene oxide dispersion. This paper presents methodologies for determining the graphene oxide content and its dispersion in naphthenic plasticizer in the presence of surfactant. A multivariate method, based on partial least squares regression and Raman spectroscopy, was used to determine the particle size and graphene oxide content in the graphene oxide /plasticizer system, with linearity (R2 > 0.99) and analytical error (> 0.29%). A laser diffraction methodology was developed for the dispersibility study. The results contribute to the state of the art of researching industrial aerospace solutions for polymeric systems containing graphene oxide.
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spelling doaj-art-1b11365e2bca4477b66f18bf099fd9d42025-08-20T03:17:14ZengAcademia Brasileira de CiênciasAnais da Academia Brasileira de Ciências1678-26902025-03-0197210.1590/0001-3765202520240617Raman evaluation of graphene oxide dispersed in naphthenic oilALAN PASSEROhttps://orcid.org/0000-0003-1938-8458TAYNARA A. DE CARVALHOhttps://orcid.org/0000-0003-4420-2299NATALIA B. SANCHEShttps://orcid.org/0000-0002-3545-119XLIDIA M.S. MURAKAMIhttps://orcid.org/0000-0001-9180-1089JORGE CARLOS N. DUTRAhttps://orcid.org/0000-0002-0923-620XRITA DE CÁSSIA L. DUTRAhttps://orcid.org/0000-0001-9958-1279Abstract Graphene oxide is a revolutionary material that enhances properties in electronics, automotive, civil construction, aerospace, and industrial sectors. Even added in low levels (0.1 – 5.0%), properly dispersed in polymer composites, it results in significant differences in mechanical, thermal, chemical, and electrical properties. Often, a suitable dispersant facilitate homogenization and provides stability in the fabrication process. However, there are few studies in the literature that assess graphene oxide dispersion. This paper presents methodologies for determining the graphene oxide content and its dispersion in naphthenic plasticizer in the presence of surfactant. A multivariate method, based on partial least squares regression and Raman spectroscopy, was used to determine the particle size and graphene oxide content in the graphene oxide /plasticizer system, with linearity (R2 > 0.99) and analytical error (> 0.29%). A laser diffraction methodology was developed for the dispersibility study. The results contribute to the state of the art of researching industrial aerospace solutions for polymeric systems containing graphene oxide.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0001-37652025000201702&lng=en&tlng=enDispersiongraphene oxidelaser diffractionRaman
spellingShingle ALAN PASSERO
TAYNARA A. DE CARVALHO
NATALIA B. SANCHES
LIDIA M.S. MURAKAMI
JORGE CARLOS N. DUTRA
RITA DE CÁSSIA L. DUTRA
Raman evaluation of graphene oxide dispersed in naphthenic oil
Anais da Academia Brasileira de Ciências
Dispersion
graphene oxide
laser diffraction
Raman
title Raman evaluation of graphene oxide dispersed in naphthenic oil
title_full Raman evaluation of graphene oxide dispersed in naphthenic oil
title_fullStr Raman evaluation of graphene oxide dispersed in naphthenic oil
title_full_unstemmed Raman evaluation of graphene oxide dispersed in naphthenic oil
title_short Raman evaluation of graphene oxide dispersed in naphthenic oil
title_sort raman evaluation of graphene oxide dispersed in naphthenic oil
topic Dispersion
graphene oxide
laser diffraction
Raman
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0001-37652025000201702&lng=en&tlng=en
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