Design of Ultra-Stable Solid Amine Adsorbents and Mechanisms of Hydroxyl Group-Dependent Deactivation for Reversible CO2 Capture from Flue Gas

Highlights We reveal that the nature of the hydrogen bonding networks formed by surface hydroxyl groups plays a key role in the deactivation mechanisms of supported polyethylenimine (PEI), which exhibits contrasting oxidative and anti-urea properties when supported on Al–OH- and Si–OH-containing sub...

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Main Authors: Meng Zhao, Liang Huang, Yanshan Gao, Ziling Wang, Shuyu Liang, Xuancan Zhu, Qiang Wang, Hong He, Dermot O’Hare
Format: Article
Language:English
Published: SpringerOpen 2025-02-01
Series:Nano-Micro Letters
Subjects:
Online Access:https://doi.org/10.1007/s40820-025-01664-w
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author Meng Zhao
Liang Huang
Yanshan Gao
Ziling Wang
Shuyu Liang
Xuancan Zhu
Qiang Wang
Hong He
Dermot O’Hare
author_facet Meng Zhao
Liang Huang
Yanshan Gao
Ziling Wang
Shuyu Liang
Xuancan Zhu
Qiang Wang
Hong He
Dermot O’Hare
author_sort Meng Zhao
collection DOAJ
description Highlights We reveal that the nature of the hydrogen bonding networks formed by surface hydroxyl groups plays a key role in the deactivation mechanisms of supported polyethylenimine (PEI), which exhibits contrasting oxidative and anti-urea properties when supported on Al–OH- and Si–OH-containing substrates. PEG modification helps reduce urea formation for PEI supported on Si–OH-containing substrates, but does not prevent oxidation of the Al–OH-containing support. The resulted ultra-stable 40PEI-20PEG-SBA-15 showing outstanding stability over 1000 adsorption–desorption cycles (2.45 mmol g−1) and negligible capacity loss after one month in simulated flue gas.
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institution Kabale University
issn 2311-6706
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language English
publishDate 2025-02-01
publisher SpringerOpen
record_format Article
series Nano-Micro Letters
spelling doaj-art-1ac58cef3bc149ba95b89c6d460669c42025-08-20T03:46:19ZengSpringerOpenNano-Micro Letters2311-67062150-55512025-02-0117111910.1007/s40820-025-01664-wDesign of Ultra-Stable Solid Amine Adsorbents and Mechanisms of Hydroxyl Group-Dependent Deactivation for Reversible CO2 Capture from Flue GasMeng Zhao0Liang Huang1Yanshan Gao2Ziling Wang3Shuyu Liang4Xuancan Zhu5Qiang Wang6Hong He7Dermot O’Hare8College of Environmental Science and Engineering, Beijing Forestry UniversityCollege of Environmental Science and Engineering, Beijing Forestry UniversityCollege of Environmental Science and Engineering, Beijing Forestry UniversityCollege of Environmental Science and Engineering, Beijing Forestry UniversityCollege of Environmental Science and Engineering, Beijing Forestry UniversityResearch Center of Solar Power and Refrigeration, Institute of Refrigeration and Cryogenics, Shanghai Jiao Tong UniversityCollege of Environmental Science and Engineering, Beijing Forestry UniversityState Key Joint Laboratory of Environment Simulation and Pollution Control, Research Centre for Eco-Environmental Sciences, Chinese Academy of SciencesChemistry Research Laboratory, Department of Chemistry, University of OxfordHighlights We reveal that the nature of the hydrogen bonding networks formed by surface hydroxyl groups plays a key role in the deactivation mechanisms of supported polyethylenimine (PEI), which exhibits contrasting oxidative and anti-urea properties when supported on Al–OH- and Si–OH-containing substrates. PEG modification helps reduce urea formation for PEI supported on Si–OH-containing substrates, but does not prevent oxidation of the Al–OH-containing support. The resulted ultra-stable 40PEI-20PEG-SBA-15 showing outstanding stability over 1000 adsorption–desorption cycles (2.45 mmol g−1) and negligible capacity loss after one month in simulated flue gas.https://doi.org/10.1007/s40820-025-01664-wCO2 captureSolid amine adsorbentLong-term stabilityOxidative degradationUrea formation
spellingShingle Meng Zhao
Liang Huang
Yanshan Gao
Ziling Wang
Shuyu Liang
Xuancan Zhu
Qiang Wang
Hong He
Dermot O’Hare
Design of Ultra-Stable Solid Amine Adsorbents and Mechanisms of Hydroxyl Group-Dependent Deactivation for Reversible CO2 Capture from Flue Gas
Nano-Micro Letters
CO2 capture
Solid amine adsorbent
Long-term stability
Oxidative degradation
Urea formation
title Design of Ultra-Stable Solid Amine Adsorbents and Mechanisms of Hydroxyl Group-Dependent Deactivation for Reversible CO2 Capture from Flue Gas
title_full Design of Ultra-Stable Solid Amine Adsorbents and Mechanisms of Hydroxyl Group-Dependent Deactivation for Reversible CO2 Capture from Flue Gas
title_fullStr Design of Ultra-Stable Solid Amine Adsorbents and Mechanisms of Hydroxyl Group-Dependent Deactivation for Reversible CO2 Capture from Flue Gas
title_full_unstemmed Design of Ultra-Stable Solid Amine Adsorbents and Mechanisms of Hydroxyl Group-Dependent Deactivation for Reversible CO2 Capture from Flue Gas
title_short Design of Ultra-Stable Solid Amine Adsorbents and Mechanisms of Hydroxyl Group-Dependent Deactivation for Reversible CO2 Capture from Flue Gas
title_sort design of ultra stable solid amine adsorbents and mechanisms of hydroxyl group dependent deactivation for reversible co2 capture from flue gas
topic CO2 capture
Solid amine adsorbent
Long-term stability
Oxidative degradation
Urea formation
url https://doi.org/10.1007/s40820-025-01664-w
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